4-Hydroxy-2-butanone 590-90-9

Details:

590-90-9 - Names and Identifiers

Name	4-Hydroxy-2-butanone
Synonyms	AI3-11747 NSC 41219 3-Oxobutanol 4-Butanol-2-one Methylolacetone 3-Oxo-1-butanol 3-Ketobutan-1-ol 4-hydroxy-2-butanon Monomethylolacetone 4-Hydroxybutan-2-one 4-Hydroxy-2-butanone 2-Butanone,4-hydroxy- 2-Butanone, 4-hydroxy- H**4-HYDROXY-2-BUTANONE
CAS	590-90-9
EINECS	209-693-6
InChI	InChI=1/C4H8O2/c1-4(6)2-3-5/h5H,2-3H2,1H3

590-90-9 - Physico-chemical Properties

Molecular Formula	C4H8O2
Molar Mass	88.11
Density	1.023 g/mL at 25 °C (lit.)
Melting Point	15°C (estimate)
Boling Point	73-76 °C/12 mmHg (lit.)
Flash Point	91°F
Water Solubility	Miscible with water, alcohol, ethanol and ether.
Solubility	Chloroform, Methanol (Slightly)
Vapor Presure	1.05mmHg at 25°C
Appearance	Transparent liquid
Color	Clear Colourless
BRN	1737666
pKa	14.43±0.10(Predicted)
Storage Condition	under inert gas (nitrogen or Argon) at 2-8°C
Sensitive	Sensitive to air
Refractive Index	1.430
MDL	MFCD00059005
Physical and Chemical Properties	colorless liquid with aromatic odor. Volatile components present in licorice and cigarette smoke solubility miscible with water, ethanol, ether, acetone Other properties typical reactions of alcohols and ketones can occur. The hydroxyl and carbonyl groups in the molecule can form cyclic half ketals
Use	Pharmaceutical Intermediates

590-90-9 - Risk and Safety

Risk Codes	10 - Flammable
Safety Description	S16 - Keep away from sources of ignition. S24/25 - Avoid contact with skin and eyes.
UN IDs	UN 1993
WGK Germany	3
TSCA	Yes
HS Code	29144000

590-90-9 - Introduction

Miscible with water, ethanol, ether, acetone. The product exists in the tobacco smoke.

 

590-90-9 - Reference Information

LogP	-1.209 at 25℃
NIST chemical information	information provided by: webbook.nist.gov (external link)
EPA chemical substance information	information provided by: ofmpeb.epa.gov (external link)
Introduction	4-hydroxy-2-butanone, a component used to trap bark beetle powder, ziegler-Natta catalyst and Ziegler- Natta catalyst form a complex for the Stereospecific Polymerization of butadiene as a catalyst and an organic synthesis intermediate, which is an intermediate for the synthesis of spice raspberry ketone and anethoxyacetone.
preparation	a synthesis method of 4-hydroxy-2-butanone, comprising the following steps:(1) add a certain amount of 1.3 butanediol, Catalyst, water and water-carrying agent to the reaction vessel, stir evenly to form a mixed solution, and raise the temperature to 60-75 °c;(2) continue stirring, to the mixed solution, hydrogen peroxide with a mass concentration of 25-35% is added dropwise, and the mixture is distilled and dehydrated while dropping;(3) when it is detected that the content of 1.3 butanediol in the reaction vessel is less than 5% of the initial content, the dropwise addition of hydrogen peroxide is stopped and stirring is continued for 0.5-1.5h;(4) the temperature in the reaction vessel is controlled, the water-carrying agent was distilled off;(5) the temperature in the reaction vessel was lowered to 60-65 ° C., and the target product 4-hydroxy-2-butanone was distilled.
Use	pharmaceutical intermediates.
production method	from the reaction of acetone and formaldehyde. The formaldehyde solution is mixed with acetone at 1:30 by weight and fed to a pipeline reactor at a temperature of 51-53 °c for a residence time of 3-4min. In the production of methyl ketene, which is an intermediate of vitamin A, the resulting 4-hydroxy-2-butanone reaction solution is directly used in the next step to obtain methyl ketene by dehydration with oxalic acid.

Our company specializes in processing and selling chemical raw materials, chemical products, pharmaceutical intermediates, veterinary medicine intermediates, dye intermediates, pigments, cosmetics raw materials and chemical reagents,  

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As a reliable partner for Chinese market, we are specialized in chemical raw materials; consolidate sourcing, marketing, sales, distribution and after-sale services, providing our partners with sourcing evaluation, technology supports, toll/contract manufacture, investment solution and suitable partnership establishment in China.
Service we can provide:
1. provide costomers with "one-stop"packaging service,from manufacture ,research,development,production,export and so on
2. Quality control, before shipment.
3. Prompt shipment with professional documents
4. Packing as your request, with photo before shipment
5.Mix and different products in ONE PCL,increase the working efficiency for customers.
6.We can export from many China main ports,convenient for the customes provide logistics services.
Our advantages: 

1, High quality with competitive price:

1) Standard:BP/USP/EP/Enterprise standard

2) All Purity≥99%

3) We are manufacturer and can provide high quality products with factory price.

 2, Fast and safe delivery

1) Parcel can be sent out in 24 hours after payment.Tracking number available

2) Secure and discreet shipment.Various transportation methods for your choice.

3) Customs pass rate ≥99%

4) We have our own agent/remailer/distributor who can help us ship our products very fast and safe,

and we have stock in there for transferring.

Product Packaging：

1) 1kg/bag (1kg net weight, 1.1kg gross weight, packed in an aluminum foil bag)

2) 25kg/drum (25kg net weight, 28kg gross weight; Packed in a cardboard-drum with two plastic-bags inside; Drum Size: 510mm high, 360mm diameter)

 Storage：

Stored in a cool and dry well-closed container. Keep away from moisture and strong light/heat.

Delivery：

Usually within3-5 working days after full payment.

transport：

EMS,DHL, TNT, UPS ,FEDEX, BY AIR, BY SEA

DHL Express, FedEx and EMS for quantity less than 50KG, usually called as DDU service; 

Sea shipping for quantity over 500KG; And air shipping is available for 50KG above;

For high value products, please select air shipping and DHL express for safe;

Our Service:
1. Fast Delivery: We can delivery within 24 hours upon receipt of your payment.
2. Quality can be promised. Hot sell to Worldwide.
3. Payment Terms: T/T,, t/t
4. Free Sample available at any time.
5. Tracking your order at any time. Inform your order's further new situation at any time.
6. Package: Professional packing with professional materials.

FAQ: 
1.Are you a trade company or factory   
We are a  factory with our own trading company.  

2.How do you control the quality   
Our factory is equipped with professional technicians to control quality, out inspectors take sample for testing every 2 hours to ensure the quality of our production. We also accept BV, SGS or any other Third-party inspection.   

3.How long is lead time  
We deliver goods within 3 days for small order, 7-10 days for bulk order.   

4. Where is your factory located How can I visit the factory   
 Our factory located in HEBEI, China.

5.Can i get some samples 
  Yes, we can supply free sample, but the shipping cost be paid by our customers. 

6.How to start orders or make payments 
  Proforma invoice will be sent first after confirmation of order, enclosed our bank information.Payment by T/T,  

7. How to confirm the Product Quality before placing orders 
  You can get free samples for some products,you only need to pay the shipping cost or arrange a courier to us and take the samples. 
8. How long is lead time

We deliver goods within 3 days for small order, 7-10 days for bulk order.

9.How do you treat quality complaint

First of all, our quality control will reduce the quality problem to near zero. If there is a realquality problem caused by us, we will send you free goods for replacement or refund your loss.