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Benzene,pentafluoro(trifluoromethyl)- (9CI) Trifluoromethyl)pentafluorobenzene Toluene, octafluoro- (6CI,7CI,8CI)
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(R)-2-METHYLSUCCINIC ACID 4-TERT-BUTYL ESTER is an organic compound commonly abbreviated as TMSA. The following is an introduction to its nature, use, preparation and safety information:
Nature:
(R)-2-METHYLSUCCINIC ACID 4-TERT-BUTYL ESTER is a colorless liquid with good solubility in water and most organic solvents. Its molecular formula is C9H16O4 and its molecular weight is 188.22g/mol. It has a density of about 0.995 g/mL and a boiling point of about 198-200 ° C.
Use:
(R)-2-METHYLSUCCINIC ACID 4-TERT-BUTYL ESTER is a commonly used organic synthesis intermediate. It can be used as a substrate, reducing agent and ligand for chiral catalysts. In addition, it can also be used to prepare organic compounds such as drugs, fragrances and dyes.
Method: The preparation of
(R)-2-METHYLSUCCINIC ACID 4-TERT-BUTYL ESTER usually involves specific synthetic routes and chemical reactions. A common synthetic method is to obtain (R)-2-methyl-3-methylthiopropionate by oxidation of methyl propyl mercaptan (MPTS), followed by methyl esterification with acetic anhydride to obtain the desired product. Specific synthesis steps and conditions can be adjusted according to needs and experimental conditions.
Safety Information:
(R)-2-METHYLSUCCINIC ACID 4-TERT-BUTYL ESTER is a chemical, so you need to pay attention to safety when using and handling it. It is combustible and should be kept away from fire and flame. Wear protective gloves, goggles and protective clothing during operation. Avoid contact with skin, eyes and respiratory tract. In case of accidental contact, rinse immediately with water and seek medical assistance. In addition, it should be kept away from children and animals, stored in sealed containers, and placed in a cool, dry place.
Molar Mass | 236.06 |
Density | 1.666 g/mL at 25 °C (lit.) |
Melting Point | -65.6 °C |
Boling Point | 104 °C (lit.) |
Flash Point | 69°F |
Solubility | Chloroform (Soluble), Methanol (Slightly) |
Appearance | A liquid |
Specific Gravity | 1.666 |
Color | Colourless |
BRN | 2057072 |
Storage Condition | Flammables area |
Refractive Index | n20/D 1.368(lit.) |
MDL | MFCD00000375 |
introduction | octafluorotoluene, English name: Octaflurotoluene; Alias: perfluorotoluene. Perfluorinated compounds are a class of elemental organic compounds in which the hydrogen connected to carbon atoms in the molecules of organic compounds is replaced by fluorine. The compound in which all the hydrocarbon bonds in the molecule are converted into fluorocarbon bonds is called perfluoroorganic compounds, and the partially substituted compounds are called monofluoro or polyfluoro organic compounds. |
application | as fluorine is the most electronegative element, polyfluorinated organic compounds have broad application prospects in chemical industry, medicine and liquid crystal materials due to their chemical stability, thermal stability, high surface activity and hydrophobic and oleophobic properties. |
preparation | (1) preparation of fluorination catalyst: by weight, 100 parts of thiourea resin are swelled in 700 parts of sodium hydroxide solution and soaked for 2 hours, the weight percentage concentration of sodium hydroxide solution is 7%, washed with deionized water to PH = 7, 300 parts of cuprous chloride solution (weight percentage concentration is 8%) are added, Add 0.05 parts of ethylene glycol bis (β-hydroxyethyl ether); Add 0.04 parts of 1-ethylmethyl ether -3-methylimidazole tetrafluoroborate, 3 parts of hydrogen peroxide, stir and react at 40 ℃ for 8 hours, finish the reaction, filter and dry to obtain fluorination catalyst;(2) Preparation of octafluorotoluene: 100 parts of octachlorotoluene are added by weight, 200 parts of dried KF,500 parts of diphenyl ether and 8 parts of fluorination catalyst are put into the reaction kettle. The system gradually heats up to react. The reaction temperature is 420 ℃, the reaction pressure is 3MP, and the reaction time is 3h. After the reaction is over, the gas phase crude in the kettle is separated from gas and solid and then enters the crude condenser for condensation. The condensate is collected in the crude tank. The residue at the bottom of the kettle is treated for production of active potassium fluoride;(3) Refining of octafluorotoluene: The crude octafluorotoluene in the crude product tank enters the octafluorotoluene rectification tower kettle, is rectified by octafluorotoluene rectification tower, and the product octafluorotoluene is separated from the top of the tower and flows through an adsorption tower equipped with 2-chloromethylchloro resin at a flow rate of 3BV/h and a temperature of 40 ℃ to obtain purified octafluorotoluene product. |
1) Standard:BP/USP/EP/Enterprise standard
2) All Purity≥99%
3) We are manufacturer and can provide high quality products with factory price.
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1) Parcel can be sent out in 24 hours after payment.Tracking number available
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3) Customs pass rate ≥99%
4) We have our own agent/remailer/distributor who can help us ship our products very fast and safe,
and we have stock in there for transferring.
Product Packaging:
1) 1kg/bag (1kg net weight, 1.1kg gross weight, packed in an aluminum foil bag)
2) 25kg/drum (25kg net weight, 28kg gross weight; Packed in a cardboard-drum with two plastic-bags inside; Drum Size: 510mm high, 360mm diameter)
Storage:
Stored in a cool and dry well-closed container. Keep away from moisture and strong light/heat.
Delivery:
Usually within3-5 working days after full payment.
transport:
EMS,DHL, TNT, UPS ,FEDEX, BY AIR, BY SEA
DHL Express, FedEx and EMS for quantity less than 50KG, usually called as DDU service;
Sea shipping for quantity over 500KG; And air shipping is available for 50KG above;
For high value products, please select air shipping and DHL express for safe;
Our Service:
1. Fast Delivery: We can delivery within 24 hours upon receipt of your payment.
2. Quality can be promised. Hot sell to Worldwide.
3. Payment Terms: T/T,, t/t
4. Free Sample available at any time.
5. Tracking your order at any time. Inform your order's further new situation at any time.
6. Package: Professional packing with professional materials.
Packing:
1. Inner double plastic bags----25kg/Fiber drum (35*35*45cm, GW: 28kg, NW: 25kg);
2. Inner double plastic bags----5kg/Aluminum foil bag (GW: 6.5kg, NW: 5kg).
3. Inner double plastic bags----1kg/Aluminum foil bag (GW: 1.5kg, NW: 1kg).
P.S.: we accept packaging customization.
Delivery:
1. Stock products are normally shipping within 3 working days.
2. For rush delivery, please contact our sales team for particular arrangement.
Shipping Details:
1. We ship goods via DHL, Fedex, UPS, TNT, China post, NL Post and other couriers, weight from 10g to 1000kg or even bulker.
2. Shipping details & shipping documents will be provided and sent by email.
3. We keep tracking the shippment until clients well received.
4. After years export shipping experience, with professional and experienced cooperated forwarders, we ensure that goods can be delivered in multiple ways safetly and efficiently.
About us
Our company specializes in processing and selling chemical raw materials, chemical products, pharmaceutical intermediates, veterinary medicine intermediates, dye intermediates, pigments, cosmetics raw materials and chemical reagents,
We have compalete sales and service team , information feedback vertical integration of a sound marketing network, products are sold throughout the country and exported to South Asia, Europe, America, Africa and other more than 20 countries and regions.
Companies adhering to the "pursuit of quality, innovation and development" business philosophy, to serve as a foundation, for the survival by the quality, seek development by science and technology, adhere to quilty comes first,fair price,good sense of customer service and responsibility. in the future hebei Nengqian import and export trade Co.,Ltd will always hold "integrity, innovation" business philosophy, to achieve honesty management, on the way of specialization, internationalization, Keep moving!
FAQ:
1. Are you a trade company or factory
We are a factory with our own trading company.
2.How do you control the quality
Our factory is equipped with professional technicians to control quality, out inspectors take sample for testing every 2 hours to ensure the quality of our production. We also accept BV, SGS or any other Third-party inspection.
3. How long is lead time
We deliver goods within 3 days for small order, 7-10 days for bulk order.
4. Where is your factory located How can I visit the factory
Our factory located in HEBEI, China.
5. Can i get some samples
Yes, we can supply free sample, but the shipping cost be paid by our customers.
6. How to start orders or make payments
Proforma invoice will be sent first after confirmation of order, enclosed our bank information.Payment by T/T,
7. How to confirm the Product Quality before placing orders
You can get free samples for some products,you only need to pay the shipping cost or arrange a courier to us and take the samples.
You can send us your product specifications and requests,we will manufacture the products according to your requests.
8. How long is lead time
We deliver goods within 3 days for small order, 7-10 days for bulk order.
9. How do you treat quality complaint
First of all, our quality control will reduce the quality problem to near zero. If there is a realquality problem caused by us, we will send you free goods for replacement or refund your loss.
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