calciol Vigorsan Ricketon
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67-97-0 - Purpose
Vitamin fortifier. Can be used in drinks, juice, candy, bread, canned food, baby food, high iron cereals and other products. China stipulates that it can be used to strengthen margarine, the amount of use is 125~156ug/kg; Use 63 ~ 125ug/kg in fortified dairy products; in
The amount used in fortified milk and milk drinks is 50-lOOug/kgI and 10-401'G/kg; The amount used in fortified solid drinks and ice cream is 10-20ug/kg.
Nature
White columnar crystal or crystalline powder, odorless and tasteless. Highly soluble in chloroform, soluble in ethanol, ether, cyclohexane and acetone, slightly soluble in vegetable oil, insoluble in water. Good heat resistance, but unstable to light, easy to oxidize in air.
Items |
Standards |
Results |
|
Color |
Colorless or white |
White |
|
Odor |
Odorless, no off -flavor |
Odoress, no off -flavor |
|
State |
Acicular crystals or crystalline powder |
Crystalline powder |
|
Specific Rotation (20°C, D) / (°)·dm²·kg?¹ |
+105.0 to +112.0 |
+109.6 (°)·dm²·kg?¹ |
|
ldentification |
Color Reaction with Acetic Anhydride and Sulfuric Acid |
Initially yellow, gradually tums red, then rapidly becomespurple, blue -green, and finally green |
Meets the regulations |
|
Infrared Spectroscopy Test |
The infrared spectrum of the sample should be consistentwith the standard infrared spectrum |
Meets the regulations |
Absorption Coefficient ∑1%1cm at 265nm |
465 -495 |
483 |
|
Lead (Pb)* |
≤2.0 mg/kg |
<2.0 mg/kg |
|
Total Arsenic (calculated as As) |
≤2.0 mg/kg |
<2.0 mg/kg |
|
Related Substances (Pre - vitamin D?, Trans - vitamin D?, Lumisterol D?, 7 - Dehydrocholesterol) |
Except for pre - vitamin D?, the area of a single impurity peak should not be greater than 0.5 times the main peak area of the control solution, and the sum of the areas of all impurity peaks should not be greater than the main peak area of the control solution |
Except for pre - vitamin D?, no single impurity peak was detected (<0.02%), total impurities 0.04% |
|
Assay |
97.0%-103.0% |
100.00% |
|
Conclusion |
This product complies with the quality standard regulations of QS - FP - FOD - 005 for Cholecalciferol (Vitamin D?) as a food additive. It also complies with the requirements of GB1903.50 - 2020. |
||
Tested once every six months |
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