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130693-82-2 Dorzolomide hydrochloride 99%
Items |
Specification |
Results |
Description |
White or almost white crystalline powder |
Complies |
Identification |
a) IR spectrum b) By HPLC |
Complies |
Solubility |
Soluble in water |
Complies |
Water |
Not more than 0.5% |
0.12% |
Residue on ignition |
Not more than 0.1% |
Complies |
Specific Rotation |
-7.3 - -9.3°(C=1, methanol, 25 °C |
-8.2° |
Heavy metals |
Not more than 10ppm |
Complies |
Related compound A |
Not more than 0.5% |
0.02% |
Chromatographic purity |
Any individual impurity: Not more than 0.1% Total impurities: Not more than 0.5% |
0.02% 0.10% |
Organic volatile impurities |
THF: not more than 720ppm Ethyl acetate: note more than 5000ppm DCM: not more than 600ppm Methanol: not more than 3000ppm |
N/A N/A N/A N/A |
Purity (HPLC) |
NLT 99.0% |
99.85% |
Assay (On anhydrous basis) |
99.0% ~ 101.0% (C10H16N2O4S3.HCl) |
100.31% |
Items |
Specification |
Results |
Description |
White or almost white crystalline powder |
Complies |
Identification |
a) IR spectrum b) By HPLC |
Complies |
Solubility |
Soluble in water |
Complies |
Water |
Not more than 0.5% |
0.12% |
Residue on ignition |
Not more than 0.1% |
Complies |
Specific Rotation |
-7.3 - -9.3°(C=1, methanol, 25 °C |
-8.2° |
Heavy metals |
Not more than 10ppm |
Complies |
Related compound A |
Not more than 0.5% |
0.02% |
Chromatographic purity |
Any individual impurity: Not more than 0.1% Total impurities: Not more than 0.5% |
0.02% 0.10% |
Organic volatile impurities |
THF: not more than 720ppm Ethyl acetate: note more than 5000ppm DCM: not more than 600ppm Methanol: not more than 3000ppm |
N/A N/A N/A N/A |
Purity (HPLC) |
NLT 99.0% |
99.85% |
Assay (On anhydrous basis) |
99.0% ~ 101.0% (C10H16N2O4S3.HCl) |
100.31% |
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