Add time:07/25/2019         Source:sciencedirect.com

Phase‐sensitive ac polarography was applied to the simultaneous quantitative determination of 4‐nitroanisole, 4‐nitrophenol and 4‐nitrocatechol in alkaline solutions. Certain experimental precautions are necessary to determine each compound in the presence of the other two. Thus, 4‐nitrocatechol is determined indirectly by forming a yellow ratio chelate with cupric ions, whereas 4‐nitroanisole is determined directly by the reduction waves of the nitro group. For the determination of 4‐nitrophenol, the interference by the simultaneously present 4‐nitrocatechol must be eliminated by masking it by the addition of magnesium ions. The method described permits a qualitative and quantitative analysis of all three compounds in one solution since linear calibration curves are obtained.

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