Add time:07/21/2019         Source:sciencedirect.com

The dioximes of 1,3- and 1,4-diacetylbenzene readily undergo regioselective double cyclopalladation on reaction with lithium tetrachloropalladate. 1,5-Bis(dimethylamino)naphthalene has been singly and doubly cyclopalladated; attempts to prepare heterodicyclometallated derivatives of this ligand were not successful. An X-ray crystal structure of the singly cyclometallated Pd(acac) complex of 1,5-bis(dimethylamino)naphthalene has been determined.

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