Add time:07/20/2019 Source:sciencedirect.com
The loss of ethylenediamine from [Cr(en)3]Cl3 has been studied using differential scanning calorimetry and thermogravimetric analysis. The effectiveness of NH4Cl as a catalyst has been evaluated. In all cases, the loss of one molecule of ethylenediamine per molecule of complex is observed, but it occurs in two steps. Unlike the deamination of [Cr(en)3](NCS)3 in the presence of NH4SCN, there is no evidence that the amount of NH4Cl present changes the final product. Kinetic and thermodynamic parameters for the reactions have been determined.
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