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  • Three dimensional organic framework of 2-amino 4, 6 dimethoxypyrimidine p-Toluenesulfonic acid monohydrate (cas 104-150-4): synthesis, single crystal growth and its properties
  • Add time:07/24/2019         Source:sciencedirect.com

    A new organic crystal, 2-amino 4, 6 dimethoxypyrimidine p-toluenesulfonic acid monohydrate (2ADPTS) was synthesized and crystals were grown from ethanolic solution by the slow evaporation method. Formation of the new crystalline compound was confirmed by a single crystal X-ray diffraction study. The species (2ADPTS) crystallizes in the triclinic crystal system with space group P-1. High resolution X-ray diffraction study (HRXRD) revealed that the 2ADPTS is free from structural grain boundaries. The thermal stability of 2ADPTS is found to be 93 °C by thermogravimetric and differential thermal (TG–DTA) analyses. UV–vis–NIR spectral study showed that the grown crystal is transparent in the entire visible region with the lower cut-off wavelength of 296 nm. The laser induced surface damage threshold of grown crystal was measured to be 2.6 GW/cm2 for 1064 nm Nd:YAG laser radiation. Nonlinear refractive index (n2), absorption coefficient (β) and third order nonlinear susceptibility (χ(3)) were measured by a Z-scan technique.

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    Prev:Quantum chemical study of p-toluenesulfonic acid, p-toluenesulfonate anion and the water–p-toluenesulfonic acid complex. Comparison with experimental spectroscopic data
    Next: Lactones. Part 16: Lactonization of γ,δ-epoxy esters with p-Toluenesulfonic acid monohydrate (cas 104-150-4))

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