Add time:08/06/2019         Source:sciencedirect.com

Recovery of lithium from lithium-rich electrolytes has attracted worldwide attention because of issues related to the electrolytic production of aluminum and its environmental impacts. Lithium carbonate preparation from a lithium-rich electrolyte by H2SO4 leaching, followed by removal of impurities and lithium precipitation with Na2CO3 was investigated. About 98% Li leaching efficiency was achieved in 1 h using 6% H2SO4 at 80 °C while maintaining a liquid-to- solid ratio of 2:1. Li2SO4 in the resulting leach solution was sequentially purified by NaOH addition to an end pH of 11 and then addition of 3 g/L ethylenediaminetetraacetic acid. Li2CO3 of 99.5% purity was then obtained by precipitation with addition of 290 g/L Na2CO3 at 95 °C for 50 min. This research is expected to improve understanding of requirements for the stable operation of electrolytic aluminum production and to potentially design processes for recycling of industrial lithium-rich electrolytes with high viability.

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