Add time:08/02/2019 Source:sciencedirect.com
The title compound has been prepared by high temperature techniques. A single crystal X-ray study has identified the structure type and composition of Tm15S22 with space group C2m, Z = 2, a = 38.395(4) Å, b = 3.8421(5) Å, c = 11.141(2) Å, β = 91.02(1)°; RRw = (2.56/2.95)% for 1072 independent reflections.
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