Add time:08/01/2019         Source:sciencedirect.com

Ammonia borane (NH3BH3), as a source material for energy generation and hydrogen storage, has attracted growing interest due to its high hydrogen content. We have investigated the synthesis of ammonia borane from Diborane (cas 19287-45-7) (B2H6) and ammonia (NH3) utilizing a low-temperature process. From our results, a maximum synthetic yield of 92.2% was obtained, for an ammonia borane complex of 0.35 M. The diammoniate diborane (DADB) was detected in about 5–10 mol% within the solid ammonia borane by solid-state 11B-NMR analysis. The synthesized solid ammonia borane products were studied to characterize hydrogen release upon thermal dehydrogenation.

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