Add time:08/07/2019         Source:sciencedirect.com

The co-crystal, Mo8O26 2(C8H9N3O)·4(C2H8N) consists of Octamolybdate, (Mo8O26)−4 an anionic cluster surrounded by four dimethylammonium ions (C2H8N)+ and (E)-N'-(pyridin-2-ylmethylene)acetohydrazide 2(C8H9N3O) has been synthesized and characterized by FT-IR and UV–Vis spectroscopic methods. Single crystal X-ray diffraction analysis reveals that complex (C24H50Mo8N10O28) contains, Octamolybdate, (Mo8O26)4- an anionic cluster surrounded by four dimethylammonium ions (C2H8N)+ along with (E)-N'-(pyridin-2-ylmethylene)acetohydrazide 2(C8H9N3O), in the unit cell. Further a series of N'-[(E)-pyridin-2-ylmethylene]acetohydrazide molecules holding the octa-molybdate units forming three dimensional supramolecular networks through number of C–H⋯O and N–H ⋯ O interactions. The Hirshfeld surfaces and two-dimensional fingerprint plots were generated to visualize the intermolecular interactions quantitatively for their relative contributions.

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