Add time:08/12/2019         Source:sciencedirect.com

The Fe–Cl boracite is prepared by a procedure, consisting of solution mixing, heating, grinding and H2 reduction. The high valence metal ion Fe3+ reacts with H2 to form the low valence metal ion Fe2+, so that the corresponding boracite can be synthesized. The lattice parameters and the phase transition temperatures are determined by means of X-ray diffraction, transmission electron microscopy and differential scanning calorimetry. The hydrogen not only plays a role in reduction, but also prevents the oxidation of the mixture. The ferroelectric property at room temperature of the sample has been substantially demonstrated.

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