Add time:08/14/2019 Source:sciencedirect.com
The electrolysis of cinnamoyl chloride in dry acetone anhydrous lithium perchlorate is carried out under controlled cathodic potential on a preparative scale. The ketonic reaction products are identified and their formation is rationalized through the electrogeneration of cinnamoyl free radical, hydrogen abstraction and dimerization of the aldoketene intermediate.
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