Regular paperInteractions in crystals. LXXXIII. The structures of 1,2,4,5-tetrakis(trimethylsilyl)benzene and of its solvent-separated radical anion salt [Na⊕(H3COCH2CHn2OCH3)3] [((H3C)3Si)4H2C6·⊖]☆-Science-Chemical Encyclopedia-lookchem

Regular paperInteractions in crystals. LXXXIII. The structures of 1,2,4,5-tetrakis(trimethylsilyl)benzene and of its solvent-separated radical anion salt [Na⊕(H3COCH2CHn2OCH3)3] [((H3C)3Si)4H2C6·⊖]☆
Add time:08/14/2019 Source:sciencedirect.com

Reduction of 1,2,4,5-Tetrakis(trimethylsilyl)benzene (cas 17156-61-5) at a sodium-metal mirror under aprotic conditions and an argon atmosphere yields red needles of its solvent-separated radical anion salt. The structure, determined in a 150 K cold N2 flow, is discussed in comparison with that of the neutral starting molecule, literature examples and results of MNDO calculations.

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