Add time:08/16/2019         Source:sciencedirect.com

Substituted acrylonitrile and ethyl acrylate bearing a masked α-hydroxyaldehyde were easily synthesised by a Barbier type reaction between the monoacetal of glyoxal and bromomethyl acrylonitrile or ethyl bromomethyl acrylate. We prepared these interesting synthons in an enantiomerically pure form by enzymatic resolution with Candida rugosa lipase, or by microbial reduction of the corresponding ketones using Aspergillus niger and Lactobacillus kefir.

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