Add time:08/17/2019         Source:sciencedirect.com

A solid-phase radioiodination technique for ω-iodophenyl fatty acids using ammonium sulfate is described. The radioiodinations are (1) regioselective, (2) high in yield (95%), (3) short in reaction time (1 h) and (4) capable of yielding high specific activity products although at lower yields. Purification is exceptionally simple: a single passage through an ion exchange column to remove unreacted ∗I− is all that is required. Syntheses of several ω-iodophenyl fatty acids are also described.

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