Add time:08/26/2019         Source:sciencedirect.com

Inulin was pyrolyzed in air to produce di-d-fructose dianhydrides (DFDAs) in ∼26% yield, three of which were identified by MS, NMR, and comparison with literature data. The mass spectra of the per-O-trimethylsilyl derivatives of the DFDAs are discussed. A mechanism is proposed for the formation of DFDAs from inulin during pyrolysis.

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