Add time:08/23/2019         Source:sciencedirect.com

The 3-[5-methyl-1-(4-methylphenyl)-1,2,3-triazol-4-yl]-s-triazolo[3,4-b]-1,3,4-thiadiazole was synthesized from p-methylaniline to 5 with formic acid. The yielded product 6 was investigated with X-ray crystallography, NMR, MS and IR techniques. Compound 6, C13H11N7S·CHCl3, Mr=416.72, crystallizes in the triclinic space group with unit cell parameters a=9.049(2), b=10.486(3), c=10.843(2) Å, α=116.79(2), β=93.83(2), γ=100.64(3)°. V=889.3(4) Å3, Z=2, Dx=1.556 mg m−3. The final R was 0.0533.

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