Add time:08/26/2019 Source:sciencedirect.com
Synthetic route to the methyl ester of methyl glycoside of 3-deoxy-D-lyxo-heptulosaric acid (13) starting from 1-cyanogalactal 2 is described. The latter substance was prepared by direct elimination of acetic acid from 1 using 1,8-diazabicyclo[5.4.0]undec-7-ene in dichloromethane.
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