The total synthesis of (+)-pectinatone: An iterative alkylation approach based on the SAMP-hydrazone method-Science-Chemical Encyclopedia-lookchem

The total synthesis of (+)-pectinatone: An iterative alkylation approach based on the SAMP-hydrazone method
Add time:09/04/2019 Source:sciencedirect.com

The marine natural product (+)-pectinatone containing ‘skip’ 1,3-dimethyl stereocentres was synthesised via the iterative alkylation of propanal SAMP-hydrazone with β-branched iodides. Factors affecting the selectivity of the alkylation reaction and the in situ formation of volatile β-branched iodides are described.

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