Add time:09/05/2019 Source:sciencedirect.com
A convenient method has been developed for the diastereoselective synthesis of methyl 5-deoxy-5-(dialkylphosphono)-5-(dialkylphosphorylamido)-2,3-O-isopropylidene-β-d-ribofuranosides under mild conditions, namely the reaction of a dialkyl phosphoramidate with a dialkyl phosphite and methyl 2,3-O-isopropylidene-β-d-ribo-pentodialdo-1,4-furanoside in acetyl chloride in a one-pot procedure.
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