Add time:09/03/2019 Source:sciencedirect.com
A strategy for the preparation of 4,4-disubstituted-3-amino-2-azetidinones, which are useful intermediates for the synthesis of analogues of monosulfactam Tigemonam, was developed. It employs D-serine as chiral starting material and involves, as key steps, the diastereoselective addition of organometal compounds to ketones 9 and the stereospecific cyclization of tertiary alcohols 7 to the β-lactams 6.
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