Add time:09/05/2019 Source:sciencedirect.com
Several methyl(allyl)thallium derivatives have been prepared for the first time. The IR and PMR spectra of these compounds indicate the presence of σ-allylthallium bonds. In the cleavage reactions of these compounds with tetramethyltin in methanol or with metal salts such as Hg(OCOCH3)2, PdX2 (X OCOC2H5 and Cl) and RhCl3·3H2O, preferential cleavage of the allylthallium bond occurs to give propylene in the case of tetramethyltin and allylic derivatives of the metals in the other cases.
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