Add time:09/24/2019 Source:sciencedirect.com
Triethyl phosphite (cas 122-52-1) and elemental iodine in solution give transient iodotriethyl-phosphonium iodide which eliminates ethyl iodide to form diethyl phosphoroiodidate. An examination of the 31P NMR and IR spectra over the temperature range −100° − 0°C fails to disclose any evidence for triethoxydi-iodophosphorane, contrary to a previous claim.
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