Add time:09/06/2019 Source:sciencedirect.com
The crystal and molecular structure of [(p-chlorophenylthio)methyl]tricyclohexylstannane (II) has been determined. In the two independent molecules of monoclinic II there are slightly distorted tetrahedral geometries about tin with intramolecular SnS distances of 3.29(1) and 3.26(1) Å. Compound II reacts with N-bromosuccinimide, I2, Pb(OAc)4 or CF3CO2H to give XCH2SC6H4Cl-p (X = Br, I, AcO or H) and the appropriate tricyclohexyltin species; II is less reactive than Cy3SnCH2SeC6H4Cl-p towards I2. Oxidative cleavage of II by m-ClC6H4CO·O·OH provides mainly CH3S(O)C6H4Cl-p. The absorption maximum for the charge transfer complex of II and (NC)2CC(CN)2 is reported.
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