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The organolanthanide fluoride [(η 5 -C 5 H t 4 Bu) 2 Sm(μ-F)] 3 (1) was generated by oxidation of [(η 5 -C 5 H t 4 Bu) 2 Sm(THF) 2 ] with Me 3 SnF. The X-ray structural analysis of 1 showed the trimeric compound to be monoclinic space groupC 2/c, Z = 4, witha = 1844.6(6), b = 1537.5(3), c = 1871.2(9) pm, β = 104.55(4)° and D c a l c = 1.597 g cm - 3 . The structure was solved from 3942 observed reflections with F o > 4σ(F o ) and refined to a final R = 0.0735.
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