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Europium borate fluoride, Eu5(BO3)3F, was synthesised as a single‐phase crystalline powder starting from europium oxide, europium fluoride and boron oxide at 1370 K. Eu5(BO3)3F crystallises in the space group Pnma. Optical spectroscopy (emission and absorption) on Eu5(BO3)3F confirms the presence of Eu2+ and delivered no evidence for Eu3+. The vibrational spectra of Eu5(BO3)3F are also reported.
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