Add time:07/15/2019         Source:sciencedirect.com

Crystals of the molybdenum(III) metaphosphate Mo(PO3)3 were grown by chemical vapor transport with iodine (1173 K → 1073 K). The structure was determined by single crystal X-ray diffraction. Mo(PO3)3 crystallizes in the monoclinic space group Ia , with a = 10.819(1) Å, b = 19.515(3) Å, c = 9.609(1) Å, β = 97.74(1)°, and Z = 12. Mo(PO3)3, and has a structure consisting of infinite chains of corner-sharing PO4 tetrahedra running along [001], bridged by isolated MoO6 octahedra. The octahedra are regular, with an average Mo-O distance of 2.084 Å. The structure can also be viewed as containing infinite MoP3O14 chains along [102], which are linked so as to define small tunnels running in the same direction.

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