Add time:07/16/2019 Source:sciencedirect.com
Cadmium(II) dithiocarbamates [Cd(dtc)2] (d tc=4-carboxamidopiperidine-1-carbodithioate, morpholine-l-carbodithioate or 4-(2-hydroxyethyl)piperazine-1-carbodithioate) and [Cd(dtc)2]·H2O (dtc=4-hydroxypiperidine-1-carbodithioate} have been prepared and characterized by thermal analysis and IR and NMR (13C, 113Cd) spectrometry. Two of these ligands have previously been shown capable of removing cadmium from its aged in vivo storage sites. The use of solid state 13C NMR measurements to establish the coordination mode of the dithiocarbamate ligands is also examined and the difficulties which arise are discussed.
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