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inquiryProduct Description Product website: http://www.finerchem.com/pro01en/id/1010.html Product Name Methyl cyclohexylphenylglycolate CAS No. 103
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inquiryMethyl cyclohexylphenylglycolate CAS:10399-13-0 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality
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inquiry10399-13-0--Methyl cyclohexylphenylglycolate Appearance:White Powder Storage:Room temperature Package:according to customers' requirements Application:Pharmaceutical intermediates Transportation:By air(EMS or EUB or FedEx or TNT ect...) or by sea(F
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Min.Order:1 Gram
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inquirySuperior quality, moderate price & quick delivery. Appearance:colourless or light yellow liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum, or as per your request. Application:Used as Pharm
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inquiryProduct Name: Methyl cyclohexylphenylglycolate Synonyms: Oxybutynin Impurity 6(Oxybutynin USP RC B);METHYL ALPHA-CYCLOHEXYLMANDELATE;METHYL CYCLOHEXYLPHENYLGLYCOLATE;METHYL 2-CYCLOHEXYL-2-HYDROXY-PHENYLACET
Cas:10399-13-0
Min.Order:5 Metric Ton
FOB Price: $1.0 / 2.0
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Cas:10399-13-0
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inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
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inquirygood quality, competitive price, thoughtful after sale serviceAppearance:white powder Storage:Keep it in dry,shady and cool place Package:25kg,50kg,180kg,200kg,250kg,1000kg,customization Application:Pharma;Industry;Agricultural;chemical reaserch Tran
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inquiryWe are committed to providing our customers with the best products and services at the most competitive prices.Appearance:white to yellow powder Storage:Room temperature with sealed well Package:according to the clients requirement Application:Use as
Methyl cyclohexylphenylglycolate cas 10399-13-0Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
Cas:10399-13-0
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inquirymethyl 2-(2'-cyclohexen-1'-yl)-2-hydroxy-2-phenylacetate
methyl 2-cyclohexyl-2-hydroxy-2-phenylacetate
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In methanol under 2625.26 Torr; for 10h; | 69.1% |
With triethylamine; palladium-carbon In methanol; hydrogen | 64.8% |
With hydrogen; triethylamine; palladium on activated charcoal In methanol at 40℃; under 11401.1 Torr; for 10h; | 64.8% |
1-bromocyclohexane
methyl 2-oxo-2-phenylacetate
methyl 2-cyclohexyl-2-hydroxy-2-phenylacetate
Conditions | Yield |
---|---|
Stage #1: 1-bromocyclohexane With cyclohexyl chloride; iodine; magnesium In tetrahydrofuran at 25 - 75℃; for 2.5h; Stage #2: methyl 2-oxo-2-phenylacetate In tetrahydrofuran at 6 - 14℃; for 2h; Stage #3: With hydrogenchloride In water; toluene at 5 - 38℃; | 58% |
Stage #1: 1-bromocyclohexane With magnesium; iodine In diethyl ether at 20℃; Inert atmosphere; Reflux; Stage #2: methyl 2-oxo-2-phenylacetate In tetrahydrofuran; diethyl ether at 0 - 20℃; Inert atmosphere; Stage #3: With ammonium chloride In tetrahydrofuran; diethyl ether at 0℃; | 57% |
With magnesium In diethyl ether |
methyl 2-oxo-2-phenylacetate
cyclohexylmagnesium bromide
methyl 2-cyclohexyl-2-hydroxy-2-phenylacetate
Conditions | Yield |
---|---|
49% |
methyl benzilate
methyl 2-cyclohexyl-2-hydroxy-2-phenylacetate
Conditions | Yield |
---|---|
With acetic acid; platinum Hydrogenation; |
methyl O-acetyl-α-cyclohexyl-α-phenylglycolate
A
methyl 2-cyclohexyl-2-hydroxy-2-phenylacetate
B
Cyclohexyl-hydroxy-(4-hydroxy-phenyl)-acetic acid methyl ester
C
Hydroxy-(4-hydroxy-cyclohexyl)-phenyl-acetic acid methyl ester
Hydroxy-((1R,3R)-3-hydroxy-cyclohexyl)-phenyl-acetic acid methyl ester
Hydroxy-((1R,3S)-3-hydroxy-cyclohexyl)-phenyl-acetic acid methyl ester
Conditions | Yield |
---|---|
With diazomethane; potassium hydroxide; ethanol; dihydrogen peroxide; acetic anhydride Product distribution; Different molar ratio; |
1-bromocyclohexane
(RS)-methyl mandelate
methyl 2-cyclohexyl-2-hydroxy-2-phenylacetate
Conditions | Yield |
---|---|
With lithium diisopropyl amide |
1-iodocyclohexane
(RS)-methyl mandelate
methyl 2-cyclohexyl-2-hydroxy-2-phenylacetate
Conditions | Yield |
---|---|
With lithium diisopropyl amide |
cyclohexylmandelic acid
methyl iodide
methyl 2-cyclohexyl-2-hydroxy-2-phenylacetate
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In N,N-dimethyl-formamide for 24h; Ambient temperature; |
(RS)-methyl mandelate
methyl 2-cyclohexyl-2-hydroxy-2-phenylacetate
Conditions | Yield |
---|---|
With lithium diisopropyl amide In tetrahydrofuran at -78 - 20℃; |
Benzilic acid
methyl 2-cyclohexyl-2-hydroxy-2-phenylacetate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: H2, glacial AcOH / PtO2 / 28 h / 80 °C / 3102.9 Torr 2: NaHCO3 / dimethylformamide / 24 h / Ambient temperature View Scheme |
methyl 2-oxo-2-phenylacetate
methyl 2-cyclohexyl-2-hydroxy-2-phenylacetate
Conditions | Yield |
---|---|
palladium-carbon In methanol; hydrogen; cyclohexene |
1-bromocyclohexane
methyl 2-oxo-2-phenylacetate
cyclohexyl chloride
methyl 2-cyclohexyl-2-hydroxy-2-phenylacetate
Conditions | Yield |
---|---|
With hydrogenchloride; iodine; magnesium In tetrahydrofuran; toluene | 58% (42% was by-product other than the objective product) |
cyclohexylmandelic acid
diazomethyl-trimethyl-silane
methyl 2-cyclohexyl-2-hydroxy-2-phenylacetate
Conditions | Yield |
---|---|
In methanol; hexane; dichloromethane | 13.7 mg |
cyclohexylboronic acid
methyl 2-cyclohexyl-2-hydroxy-2-phenylacetate
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: methanol; water / 2 h / 20 °C / Inert atmosphere 2: dichloromethane; water / 24 h / 25 °C / Inert atmosphere; Sealed tube; Irradiation 3: dichloromethane; methanol; hexane View Scheme |
cyclohexyltrifluoro-λ4-borane potassium salt
methyl 2-cyclohexyl-2-hydroxy-2-phenylacetate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: dichloromethane; water / 24 h / 25 °C / Inert atmosphere; Sealed tube; Irradiation 2: dichloromethane; methanol; hexane View Scheme |
methyl 2-cyclohexyl-2-hydroxy-2-phenylacetate
cyclohexylmandelic acid
Conditions | Yield |
---|---|
Stage #1: methyl 2-cyclohexyl-2-hydroxy-2-phenylacetate With methanol; water; sodium hydroxide for 2h; Reflux; Stage #2: With hydrogenchloride; water at 0℃; pH=3 - 4; | 77% |
Stage #1: methyl 2-cyclohexyl-2-hydroxy-2-phenylacetate With sodium hydroxide In methanol; water at 65 - 75℃; for 3h; Stage #2: With hydrogenchloride at 60 - 70℃; pH=1; Stage #3: at 0 - 5℃; for 2h; | 44% |
With sodium hydroxide | |
With potassium hydroxide In ethanol at 20℃; |
(5-dimethylaminomethyl-furan-2-yl)-methanol
methyl 2-cyclohexyl-2-hydroxy-2-phenylacetate
Conditions | Yield |
---|---|
With sodium methylate In cyclohexane for 24h; Heating; | 65% |
methyl 2-cyclohexyl-2-hydroxy-2-phenylacetate
{5-[(Cyclohexyl-methyl-amino)-methyl]-furan-2-yl}-methanol
Conditions | Yield |
---|---|
With sodium methylate In cyclohexane for 24h; Heating; | 65% |
methyl 2-cyclohexyl-2-hydroxy-2-phenylacetate
{5-[(Isopropyl-methyl-amino)-methyl]-furan-2-yl}-methanol
Conditions | Yield |
---|---|
With sodium methylate In cyclohexane for 24h; Heating; | 60% |
methyl 2-cyclohexyl-2-hydroxy-2-phenylacetate
(4a,6a-dimethyl-tetrahydro-1,4-dioxa-6b-aza-cyclopenta[cd]pentalen-2a-yl)-methanol
Conditions | Yield |
---|---|
(i) Na, heptane, (ii) /BRN= 2699068/; Multistep reaction; |
1-(2,2-dimethyl-1,3-dioxolan-4-ylmethyl)-4-piperidinol
methyl 2-cyclohexyl-2-hydroxy-2-phenylacetate
Cyclohexyl-hydroxy-phenyl-acetic acid 1-(2,2-dimethyl-[1,3]dioxolan-4-ylmethyl)-piperidin-4-yl ester
Conditions | Yield |
---|---|
With sodium hydride 1.) oil, 80 deg C; Yield given. Multistep reaction; |
methyl 2-cyclohexyl-2-hydroxy-2-phenylacetate
1-(1,3-dioxolan-2-ylmethyl)-4-piperidinol
4-(α-cyclohexyl-α-phenylglycoloyloxy)-1-(1,3-dioxolan-2-ylmethyl)piperidine
Conditions | Yield |
---|---|
With sodium hydride 1.) oil, 80 deg C, 2.) 3 h; Yield given. Multistep reaction; |
methyl 2-cyclohexyl-2-hydroxy-2-phenylacetate
Cyclohexyl phenyl ketone
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: KOH / ethanol / 20 °C 2: 94 percent / (NMe4)Co(III)Me2opba*2H2O*CH3CN; pivalaldehyde; O2 / acetonitrile / 3 h View Scheme | |
Multi-step reaction with 2 steps 1: NaOH 2: 94 percent / O2, pivalaldehyde, (NMe4)*2H2O*CH3CN (L = ortho-phenylenebis(N'-methyloxamidate)) / acetonitrile / 2 h / Ambient temperature View Scheme |
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