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inquiryProduct Description Product website: http://www.finerchem.com/pro01en/id/1001.html Product Name 3-Ethynylphenol CAS No. 10401-11-3
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inquiryhigh quality with lower quotation. and enough stockAppearance:Light yellow liquid Storage:Low temperature dry and shady Package:10g/pack Application:only for research Transportation:By Air,By TNT,EMS,Fedex Port:Shanghai Port
3-Hydroxyphenylacetylene CAS:10401-11-3 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic
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Cas:10401-11-3
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Cas:10401-11-3
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3-hydroxy phenylacetylene
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride In tetrahydrofuran at 20℃; for 1h; Inert atmosphere; | 95% |
3-[2-(trimethylsilylethynyl)]phenol
3-hydroxy phenylacetylene
Conditions | Yield |
---|---|
With methanol; potassium hydroxide In tetrahydrofuran at 20℃; for 10h; Inert atmosphere; | 88% |
Stage #1: 3-[2-(trimethylsilylethynyl)]phenol With potassium hydroxide In tetrahydrofuran; methanol; water for 2h; Stage #2: With hydrogenchloride In tetrahydrofuran; methanol; water | 70% |
With potassium carbonate In methanol at 20℃; for 3h; Inert atmosphere; |
3-hydroxy phenylacetylene
Conditions | Yield |
---|---|
at 800℃; under 0.000750075 Torr; | 87% |
3-hydroxy phenylacetylene
Conditions | Yield |
---|---|
With potassium hydroxide In toluene for 3h; Heating; | 43% |
(1S,2R)-3-Trimethylsilanylethynyl-cyclohexa-3,5-diene-1,2-diol
3-hydroxy phenylacetylene
Conditions | Yield |
---|---|
With potassium carbonate In methanol for 12h; |
A
2-ethynyl-phenol
B
3-hydroxy phenylacetylene
Conditions | Yield |
---|---|
With perchloric acid at 25℃; Rate constant; |
3-Bromophenol
3-hydroxy phenylacetylene
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: bis(triphenylphosphine)palladium(II) dichloride; copper(l) iodide; triethylamine / tetrahydrofuran / 24 h / 20 °C / Inert atmosphere 2: potassium carbonate / methanol / 3 h / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 2 steps 1: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triphenylphosphine / 1,4-dioxane / 1.33 h / 70 °C / Inert atmosphere; Microwave irradiation 2: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere View Scheme |
meta-hydroxybenzaldehyde
3-hydroxy phenylacetylene
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: chloroform / 24 h / Cooling with ice; Inert atmosphere; Darkness 2: 800 °C / 0 Torr View Scheme |
3-hydroxy phenylacetylene
Conditions | Yield |
---|---|
With potassium fluoride; 18-crown-6 ether; Methyl thioglycolate In water; acetonitrile at 50℃; |
3-hydroxy phenylacetylene
3-Hydroxyacetophenone
Conditions | Yield |
---|---|
With gold(III) tribromide; water at 200℃; for 0.333333h; microwave irradiation; | 100% |
With tropylium tetrafluoroborate; water; acetic acid at 130℃; for 1h; Catalytic behavior; Temperature; Microwave irradiation; Inert atmosphere; | 92% |
With trifluorormethanesulfonic acid; water In 2,2,2-trifluoroethanol at 25℃; for 24h; Sealed tube; regioselective reaction; | 87% |
With water at 60℃; for 20h; Sealed tube; | 63% |
With methanesulfonic acid; iron(II) chloride tetrahydrate In 1,2-dichloro-ethane at 60℃; for 2h; Inert atmosphere; | 49% |
2,2‘,4,4’,5,5‘,6,6‘-hexa-O-acetyl-3,3‘-diazido-3,3‘-dideoxy-1,1‘-sulfanediyl-di-β-D-galactopyranoside
3-hydroxy phenylacetylene
bis-{2,4,6-tri-O-acetyl-3-deoxy-3-[4-(3-hydroxyphenyl)-1H-1,2,3-triazol-1-yl]-β-D-galactopyranosyl}sulfane
Conditions | Yield |
---|---|
With copper(ll) sulfate pentahydrate; sodium L-ascorbate In water; N,N-dimethyl-formamide at 80℃; for 0.666667h; Microwave irradiation; | 100% |
5-azido-2-hydroxy-N-(3-(trifluoromethyl)phenyl)benzamide
3-hydroxy phenylacetylene
2-hydroxy-5-[4-(3-hydroxyphenyl)-1H-1,2,3-triazol-1-yl]-N-(3-trifluoromethylphenyl)benzamide
Conditions | Yield |
---|---|
With copper(II) sulfate; sodium L-ascorbate In water; dimethyl sulfoxide; tert-butyl alcohol at 20℃; for 96h; Inert atmosphere; | 99% |
diethyl 2,2-di(prop-2-yn-1-yl)malonate
3-hydroxy phenylacetylene
diethyl 5-(3-hydroxyphenyl)-1H-indene-2,2(3H)-dicarboxylate
Conditions | Yield |
---|---|
With cobalt(II) chloride hexahydrate; 2-(2,6-diisopropylphenyliminomethyl)pyridine; zinc In tetrahydrofuran at 40℃; Inert atmosphere; | 99% |
3-hydroxy phenylacetylene
3-hydroxystyrene
Conditions | Yield |
---|---|
With formic acid; iron(II) tetrafluoroborate hexahydrate; tris(2-diphenylphosphinoethyl)phosphine In tetrahydrofuran at 40℃; for 5h; Inert atmosphere; | 99% |
Stage #1: 3-hydroxy phenylacetylene With tetrakis(triphenylphosphine) palladium(0) In 1,4-dioxane at 20℃; for 0.25h; Inert atmosphere; Stage #2: With formic acid In 1,4-dioxane at 80℃; for 3h; Inert atmosphere; | 91% |
With hydrogen In ethanol at 40℃; under 760.051 Torr; for 1.5h; Schlenk technique; Sealed tube; chemoselective reaction; | 95 %Chromat. |
With Dimethylphenylsilane; water In dimethyl sulfoxide at 70℃; for 0.333333h; Inert atmosphere; stereoselective reaction; |
3-hydroxy phenylacetylene
(Z)-C-6-azido-2,3-O,O-dibenzyl-4,5-didehydro-5,6-dideoxy-L-ascorbic acid
Conditions | Yield |
---|---|
With copper diacetate In methanol at 50℃; Temperature; Flow reactor; Sonication; | 99% |
With copper diacetate In methanol |
3-hydroxy phenylacetylene
tert-butyldimethylsilyl chloride
3-tert-butyldimethylsilyloxyphenylacetylene
Conditions | Yield |
---|---|
With 1H-imidazole In N,N-dimethyl-formamide at 20℃; for 14h; | 98% |
With 1H-imidazole In N,N-dimethyl-formamide at 20℃; | 86% |
Conditions | Yield |
---|---|
With copper(l) iodide; N-ethyl-N,N-diisopropylamine; bis-triphenylphosphine-palladium(II) chloride In N,N-dimethyl-formamide for 6h; | 98% |
3-hydroxy phenylacetylene
isopropenylbenzene
3-(3-methyl-3-phenylcyclobut-1-enyl)phenol
Conditions | Yield |
---|---|
With (acetonitrile)[(2',4',6'-triisopropyl-1,1'-biphenyl-2-yl)di-tert-butylphosphine]gold(I) tetrakis[3,5-bis(trifluoromethyl)phenyl]borate In dichloromethane at 23℃; Inert atmosphere; regioselective reaction; | 98% |
With (acetonitrile)[2-di-tert-butyl(2′,4′,6′-triiso-propylbiphenyl)phosphine]gold(I) hexafluoroantimonate In dichloromethane at 20℃; for 26h; Inert atmosphere; regioselective reaction; | 74% |
carbon dioxide
3-hydroxy phenylacetylene
3-(3-hydroxyphenyl)-2-propynoic acid
Conditions | Yield |
---|---|
With caesium carbonate In dimethyl sulfoxide at 50℃; under 760.051 Torr; for 16h; Sealed tube; | 98% |
With caesium carbonate In N,N-dimethyl-formamide at 24℃; for 20h; | 92% |
With caesium carbonate; silver(I) iodide In N,N-dimethyl-formamide at 25℃; under 760.051 Torr; for 16.25h; Inert atmosphere; Schlenk technique; | 90% |
p-nitrobenzene iodide
3-hydroxy phenylacetylene
Conditions | Yield |
---|---|
With sodium azide; trans-N,N'-dimethylcyclohexane-1,2-diamine; sodium L-ascorbate; copper(l) iodide In dimethyl sulfoxide at 20℃; for 1h; | 97% |
3-hydroxy phenylacetylene
o-iodo-methyl-benzoic acid
Conditions | Yield |
---|---|
Stage #1: 3-hydroxy phenylacetylene; o-iodo-methyl-benzoic acid With trans-bis(triphenylphosphine)palladium dichloride; triethylamine at 20℃; for 0.25h; Sonogashira Cross-Coupling; Inert atmosphere; Stage #2: With copper(l) iodide at 50℃; for 1h; Sonogashira Cross-Coupling; Inert atmosphere; | 97% |
3-hydroxy phenylacetylene
indole-2,3-dione
Conditions | Yield |
---|---|
With C36H29N2O2P; cobalt(II) diacetate tetrahydrate In ethanol at 30℃; for 20h; Schlenk technique; Glovebox; Inert atmosphere; enantioselective reaction; | 97% |
Conditions | Yield |
---|---|
With 1,3‐bis[2,6‐bis(propan‐2‐yl)phenyl]‐2‐[(phenylformonitrile)aurio]‐2,3‐dihydro‐1H‐imidazol‐2‐yl hexafluorostibane In dichloromethane at 23℃; Inert atmosphere; | 96% |
3-hydroxy phenylacetylene
3-(4-(3-hydroxyphenyl)buta-1,3-diynyl)phenol
Conditions | Yield |
---|---|
With oxygen; potassium carbonate In dimethyl sulfoxide at 50℃; for 8h; | 95% |
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