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Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product s

1,3,2-Dioxathiolane,2,2-dioxide

Cas:1072-53-3

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Jinan Finer Chemical Co., Ltd

Product description: Product name Ethylene sulfate CAS number 1072-53-3 Assay ≥99.5% Appearance White powder Capacity 500mt/year Application Lithium ion batteries electrolyte

Ethylene sulfate

Cas:1072-53-3

Min.Order:100 Gram

FOB Price: $12.0

Type:Lab/Research institutions

inquiry

Henan Allgreen Chemical Co.,Ltd

high purity Appearance:white crystal or crystalline powder Storage:Sealed, dry, microtherm , avoid light and smell. Package:meet customer's demand Application:organic synthesis Transportation:by sea or by air Port:shanghai

ETHYLENESULFATE

Cas:1072-53-3

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

inquiry

Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 1,3,2-dioxathiolane 2,2-dioxide

Cas:1072-53-3

Min.Order:1

Negotiable

Type:Other

inquiry

Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

High Quality Oled CAS 1072-53-3 1,3,2-Dioxathiolane,2,2-dioxide

Cas:1072-53-3

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

inquiry

Henan Tianfu Chemical Co., Ltd.

High purity CAS 1072-53-3 ETHYLENESULFATE in stock Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED intermediates (Fluorene,C

High purity CAS 1072-53-3 ETHYLENESULFATE in stock

Cas:1072-53-3

Min.Order:1 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

Our advantages: 1, High quality with competitive price: 1) Standard:BP/USP/EP/Enterprise standard 2) All Purity≥99% 3) We are manufacturer and can provide high quality products with factory price. 2, Fast and safe delivery 1) Parcel can be

ETHYLENESULFATE cas 1072-53-3

Cas:1072-53-3

Min.Order:1 Kilogram

FOB Price: $48.0 / 58.0

Type:Trading Company

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

99% Pure CAS 1072-53-3 with fast shipping

Cas:1072-53-3

Min.Order:10 Gram

FOB Price: $146.0 / 176.0

Type:Trading Company

inquiry

Hebei yanxi chemical co.,LTD.

hebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developmen

1,3,2-Dioxathiolane 2,2-dioxide CAS NO.1072-53-3

Cas:1072-53-3

Min.Order:20 Kilogram

FOB Price: $10.0 / 100.0

Type:Trading Company

inquiry

Hangzhou Sartort Biopharma Co., Ltd

Appearance:White to off-white powder Storage:2-8°C Package:25kg/drum Application:it is an alkylating agent with carcinogenic activty. Transportation:Express/Sea/Air Port:any port in china

ETHYLENESULFATE factory price

Cas:1072-53-3

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Lab/Research institutions

inquiry

Hefei TNJ chemical industry co.,ltd

Properties It is a kind of White crystal, with melting point 99 ℃, flash point 93.5±18.2 ℃.can be used as the additives of electrolyte in lithium ion battery . Specification Index name Spec Appearance

Ethylene Sulfate

Cas:1072-53-3

Min.Order:1 Metric Ton

Negotiable

Type:Trading Company

inquiry

Xi'an Faithful Biotech Co., Ltd.

We are the manufacturers and suppliers of API in China, and warehouse in Germany and USA of California, which can quickly and safely deliver to your address 1.High quality and competitive price. 2.Free sample for your evaluation. 3.Promptly delivery

Shanghai Upbio Tech Co.,Ltd

1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ

1,3,2-Dioxathiolane,2,2-dioxide

Cas:1072-53-3

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

1,3,2-Dioxathiolane,2,2-dioxide

Cas:1072-53-3

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

inquiry

Baoji Guokang Healthchem co.,ltd

Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese

ETHYLENESULFATE 99%

Cas:1072-53-3

Min.Order:1 Kilogram

FOB Price: $68.0 / 75.0

Type:Trading Company

inquiry

Qingdao Beluga Import and Export Co., LTD

ETHYLENESULFATE CAS:1072-53-3 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermedia

ETHYLENESULFATE CAS:1072-53-3

Cas:1072-53-3

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

1,3,2-Dioxathiolane,2,2-dioxide

Cas:1072-53-3

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

1,3,2-Dioxathiolane,2,2-dioxide

Cas:1072-53-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

Ethylene Sulfate (DTD)

Cas:1072-53-3

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

SHANGHAI T&W PHARMACEUTICAL CO., LTD.

A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc

1,3,2-Dioxathiolane 2,2-dioxide

Cas:1072-53-3

Min.Order:4 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Ethylenesulfate

Cas:1072-53-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Massive Chemical Technology Co., Ltd.

Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and als

ETHYLENESULFATE

Cas:1072-53-3

Min.Order:1 Gram

FOB Price: $1.0

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

Glycol sulfite

Cas:1072-53-3

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

SHANGHAI SYSTEAM BIOCHEM CO., LTD

We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov

1,3,2-Dioxathiolane,2,2-dioxide

Cas:1072-53-3

Min.Order:100 Gram

FOB Price: $100.0 / 2000.0

Type:Lab/Research institutions

inquiry

Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

Ethylenesulfate ,98%

Cas:1072-53-3

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Siwei Development Group Ltd.

Product name: Ethylene Sulfate CAS No.:1072-53-3 Molecule Formula:C2H4O4S Molecule Weight:124.12 Purity: 99.0% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard TESTING ITEMS

Best Quality Ethylene Sulfate

Cas:1072-53-3

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

supply 1,3,2-dioxathiolane 2,2-dioxide CAS NO.1072-53-3

Cas:1072-53-3

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

inquiry

Hangzhou Huarong Pharm Co., Ltd.

We Huarong Pharm can provide Customized Synthesis & Process R&D & APIs and intermediates Production & Quality Research & Registration Application, especially our GMP validation service which complies with SFDA, FDA, WHO and EU EMPA. O

ETHYLENESULFATE

Cas:1072-53-3

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

supply 1,3,2-dioxathiolane 2,2-dioxide CAS NO.1072-53-3

Cas:1072-53-3

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Synthetic route

oxirane
75-21-8

oxirane

ethyleneglycol sulfate
1072-53-3

ethyleneglycol sulfate

Conditions
ConditionsYield
With cerium(IV) oxide; iron(III) chloride; sulfur dioxide; antimony(III) chloride at 140℃; under 45004.5 Torr; for 2h; Pressure; Temperature; Inert atmosphere; Autoclave;97.8%
With aminosulfonic acid; acetic anhydride at -10 - 20℃; for 24h; Autoclave;73.22%
ethylene glycol
107-21-1

ethylene glycol

ethyleneglycol sulfate
1072-53-3

ethyleneglycol sulfate

Conditions
ConditionsYield
With fluorosulfonyl fluoride; N,N,N,N,-tetramethylethylenediamine In acetonitrile at 60℃; for 36h; Reagent/catalyst; Solvent; Temperature;96.5%
Stage #1: ethylene glycol With fluorosulfonyl fluoride; sodium sulfate; tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide In tert-butyl methyl ether at 5 - 10℃; for 1h; Autoclave;
Stage #2: With 15-crown-5; 18-crown-6 ether In dichloromethane Solvent; Reagent/catalyst; Temperature;
81.8%
With potassium hydroxide; sulfuryl dichloride; silica gel 1.) reflux; 2.) rt., 3 h; Yield given. Multistep reaction;
Stage #1: ethylene glycol With potassium hydroxide In 5,5-dimethyl-1,3-cyclohexadiene at 130 - 140℃; for 20h;
Stage #2: With fluorosulfonyl fluoride In acetonitrile at -15 - -5℃; for 1h; Temperature; Reagent/catalyst; Solvent; Sealed tube; Inert atmosphere;
106.3 g
With sulfuryl dichloride In chloroform at 5 - 60℃; for 3h;375 g
ethylene sulfite
3741-38-6

ethylene sulfite

ethyleneglycol sulfate
1072-53-3

ethyleneglycol sulfate

Conditions
ConditionsYield
With manganese(IV) oxide In water at 5℃; for 0.75h; Reagent/catalyst; Temperature;95.84%
With sodium hydrogencarbonate; iron(II) sulfate In dichloromethane pH=7 - 8; Concentration;90.66%
With ruthenium trichloride; calcium hypochlorite at 15℃;83%
ethene
74-85-1

ethene

ethyleneglycol sulfate
1072-53-3

ethyleneglycol sulfate

Conditions
ConditionsYield
With PhI(1+)OSO2O(1-) In dichloromethane at 15℃; for 0.3h;85%
With μ-oxodiphenyldiiodine(III) sulfate; phenyliodine(III) sulfate Yield given;
[1,3]-dioxolan-2-one
96-49-1

[1,3]-dioxolan-2-one

ethyleneglycol sulfate
1072-53-3

ethyleneglycol sulfate

Conditions
ConditionsYield
With carbon dioxide; sulfur trioxide at 25 - 65℃; for 8h; Inert atmosphere;76%
thionyl chloride
7719-09-7

thionyl chloride

ethylene glycol
107-21-1

ethylene glycol

ethyleneglycol sulfate
1072-53-3

ethyleneglycol sulfate

Conditions
ConditionsYield
Stage #1: thionyl chloride; ethylene glycol at 25 - 30℃; for 3h; Inert atmosphere;
Stage #2: With sodium hypochlorite; ruthenium(III) chloride trihydrate at 0 - 10℃; for 3h; pH=7-8; Concentration; Temperature;
74%
C2H5ClO3S

C2H5ClO3S

ethyleneglycol sulfate
1072-53-3

ethyleneglycol sulfate

Conditions
ConditionsYield
With sodium periodate; ruthenium(III) chloride trihydrate In water; acetonitrile for 0.25h; Cooling with ice; Inert atmosphere;70%
ethylene dibromide
106-93-4

ethylene dibromide

ethyleneglycol sulfate
1072-53-3

ethyleneglycol sulfate

Conditions
ConditionsYield
With silver sulfate; xylene
With silver sulfate In xylene
ethylene sulfite
3741-38-6

ethylene sulfite

ruthenium (IV) oxide dihydrate

ruthenium (IV) oxide dihydrate

ethyleneglycol sulfate
1072-53-3

ethyleneglycol sulfate

Conditions
ConditionsYield
With sodium hypochlorite In dichloromethane; isopropyl alcohol
ethyleneglycol sulfate
1072-53-3

ethyleneglycol sulfate

Conditions
ConditionsYield
Stage #1: potassium ethyleneglycolate With sulfuryl dichloride In dichloromethane at -10 - 10℃; for 2h; Inert atmosphere;
Stage #2: With 18-crown-6 ether In toluene at 20℃; for 1h; Reagent/catalyst; Solvent;
37.9 g
ethane
74-84-0

ethane

A

ethyleneglycol sulfate
1072-53-3

ethyleneglycol sulfate

B

ethane-1,2-diyl bis(hydrogen sulfate)
6914-91-6

ethane-1,2-diyl bis(hydrogen sulfate)

Conditions
ConditionsYield
With fuming sulphuric acid; iodine at 90℃; under 22502.3 Torr; for 2h; Catalytic behavior; Reagent/catalyst; Temperature; Autoclave;
ethyleneglycol sulfate
1072-53-3

ethyleneglycol sulfate

tert-butyl cinnamate
14990-09-1

tert-butyl cinnamate

C12H20NSi(1-)*Li(1+)

C12H20NSi(1-)*Li(1+)

(-)-tert-butyl (2S,3R)-1-benzyl-2-phenylpyrrolidine-3-carboxylate
1394979-11-3

(-)-tert-butyl (2S,3R)-1-benzyl-2-phenylpyrrolidine-3-carboxylate

Conditions
ConditionsYield
Stage #1: C12H20NSi(1-)*Li(1+) With (1S,2S)-1,2-dimethoxy-1,2-diphenylethane In toluene at -78℃; for 0.583333h;
Stage #2: tert-butyl cinnamate In toluene at -78℃; for 1.63h;
Stage #3: ethyleneglycol sulfate enantioselective reaction; Further stages;
97%
ethyleneglycol sulfate
1072-53-3

ethyleneglycol sulfate

2-methyl-acrylic acid 3-dimethylamino-propyl amide
5205-93-6

2-methyl-acrylic acid 3-dimethylamino-propyl amide

2-((3-methacrylamidopropyl)dimethylammonio)ethyl sulfate

2-((3-methacrylamidopropyl)dimethylammonio)ethyl sulfate

Conditions
ConditionsYield
With nitrobenzene In acetonitrile at 50℃; for 24h; Schlenk technique; Inert atmosphere;95.6%
ethyleneglycol sulfate
1072-53-3

ethyleneglycol sulfate

difluoromethyl phenyl sulfone
1535-65-5

difluoromethyl phenyl sulfone

3,3-difluoro-3-(phenylsulfonyl)propan-1-ol

3,3-difluoro-3-(phenylsulfonyl)propan-1-ol

Conditions
ConditionsYield
With N,N,N,N,N,N-hexamethylphosphoric triamide; sulfuric acid; lithium hexamethyldisilazane In tetrahydrofuran; water at 20℃; for 2h;94%
Stage #1: ethyleneglycol sulfate; difluoromethyl phenyl sulfone With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium hexamethyldisilazane In tetrahydrofuran at -78 - 20℃; for 3.5h; Inert atmosphere;
Stage #2: With sulfuric acid In tetrahydrofuran at 60℃;
90%
6-methylbenzo[b]thiophene
16587-47-6

6-methylbenzo[b]thiophene

ethyleneglycol sulfate
1072-53-3

ethyleneglycol sulfate

2-(6-methyl-benzo[b]thiophen-2-yl)-ethanol
873692-99-0

2-(6-methyl-benzo[b]thiophen-2-yl)-ethanol

Conditions
ConditionsYield
Stage #1: 6-methylbenzo[b]thiophene With n-butyllithium In tetrahydrofuran; hexanes at -60℃; for 0.75h;
Stage #2: ethyleneglycol sulfate In tetrahydrofuran; hexanes at -60 - 20℃;
Stage #3: With acetyl chloride In methanol at 0 - 20℃; for 4.25h;
89%
1-methyl-1H-imidazole
616-47-7

1-methyl-1H-imidazole

ethyleneglycol sulfate
1072-53-3

ethyleneglycol sulfate

lithium diphenylphosphide
65567-06-8, 4541-02-0

lithium diphenylphosphide

2-(2-(diphenylphosphino)ethyl)-1-methyl-1H-imidazol

2-(2-(diphenylphosphino)ethyl)-1-methyl-1H-imidazol

Conditions
ConditionsYield
Stage #1: 1-methyl-1H-imidazole With n-butyllithium In tetrahydrofuran; hexane at -78 - 60℃; Inert atmosphere;
Stage #2: ethyleneglycol sulfate In tetrahydrofuran; hexane at -78 - 0℃; Inert atmosphere;
Stage #3: lithium diphenylphosphide In tetrahydrofuran; hexane at 0℃; Inert atmosphere; Reflux;
89%
ethyleneglycol sulfate
1072-53-3

ethyleneglycol sulfate

2-fluoro-3-iodopyridine
113975-22-7

2-fluoro-3-iodopyridine

2-(2-fluoro-4-iodopyridin-3-yl)ethane-1-ol
1620011-25-7

2-(2-fluoro-4-iodopyridin-3-yl)ethane-1-ol

Conditions
ConditionsYield
Stage #1: 2-fluoro-3-iodopyridine With lithium diisopropyl amide In tetrahydrofuran; n-heptane at -78℃; for 1.5h;
Stage #2: ethyleneglycol sulfate In tetrahydrofuran; n-heptane at -78 - 20℃; for 2.33333h;
Stage #3: With hydrogenchloride In tetrahydrofuran; n-heptane; water at 0 - 20℃; for 3h;
87%
Stage #1: 2-fluoro-3-iodopyridine With lithium diisopropyl amide In tetrahydrofuran; n-heptane; ethylbenzene at -78℃; for 1.5h;
Stage #2: ethyleneglycol sulfate In tetrahydrofuran; n-heptane; ethylbenzene at -78 - 30℃; for 2.67h;
Stage #3: With hydrogenchloride; water In tetrahydrofuran; n-heptane; ethylbenzene at 0 - 30℃; for 3h;
87%
ethyleneglycol sulfate
1072-53-3

ethyleneglycol sulfate

2-fluoro-4-iodopyridine
22282-70-8

2-fluoro-4-iodopyridine

2-(2-fluoro-4-iodopyridin-3-yl)ethane-1-ol
1620011-25-7

2-(2-fluoro-4-iodopyridin-3-yl)ethane-1-ol

Conditions
ConditionsYield
Stage #1: 2-fluoro-4-iodopyridine With lithium diisopropyl amide In tetrahydrofuran; n-heptane; ethylbenzene at -78℃; for 1.5h;
Stage #2: ethyleneglycol sulfate In tetrahydrofuran; n-heptane; ethylbenzene at -78 - 20℃; for 2.66667h;
Stage #3: With hydrogenchloride In tetrahydrofuran; n-heptane; ethylbenzene; water at 0 - 20℃; for 3h;
87%
Stage #1: 2-fluoro-4-iodopyridine With lithium diisopropyl amide In tetrahydrofuran at -65℃; for 1.5h; Inert atmosphere;
Stage #2: ethyleneglycol sulfate In tetrahydrofuran at -65 - 20℃; Inert atmosphere;
86.2%
Stage #1: 2-fluoro-4-iodopyridine With lithium diisopropyl amide In tetrahydrofuran; n-heptane; ethylbenzene at -78℃; for 1.5h;
Stage #2: ethyleneglycol sulfate In tetrahydrofuran; n-heptane; ethylbenzene at -78 - 20℃; for 2.67h;
1950 mg
ethyleneglycol sulfate
1072-53-3

ethyleneglycol sulfate

2,2-bis((decyloxy)methyl)propane-1,3-diol
1191028-34-8

2,2-bis((decyloxy)methyl)propane-1,3-diol

disodium 5,5-bis(decyloxymethyl)-3,7-dioxa-1,9-nonadiyl disulfate

disodium 5,5-bis(decyloxymethyl)-3,7-dioxa-1,9-nonadiyl disulfate

Conditions
ConditionsYield
Stage #1: 2,2-bis((decyloxy)methyl)propane-1,3-diol With sodium hydride In tetrahydrofuran; mineral oil for 0.5h; Cooling with ice;
Stage #2: ethyleneglycol sulfate In tetrahydrofuran; mineral oil at 20℃; for 26h;
86%
Stage #1: 2,2-bis((decyloxy)methyl)propane-1,3-diol With sodium hydride In tetrahydrofuran; mineral oil for 0.5h; Cooling with ice;
Stage #2: ethyleneglycol sulfate In tetrahydrofuran; mineral oil for 24.33h;
ethyleneglycol sulfate
1072-53-3

ethyleneglycol sulfate

1-bromo-4-(2-bromo-1,1,2,2-tetrafluoroethoxy)benzene
113939-45-0

1-bromo-4-(2-bromo-1,1,2,2-tetrafluoroethoxy)benzene

4-(4-bromophenoxy)-3,3,4,4-tetrafluorobutan-1-ol

4-(4-bromophenoxy)-3,3,4,4-tetrafluorobutan-1-ol

Conditions
ConditionsYield
Stage #1: 1-bromo-4-(2-bromo-1,1,2,2-tetrafluoroethoxy)benzene With TurboGrignard In tetrahydrofuran at -78℃; Inert atmosphere; Schlenk technique;
Stage #2: ethyleneglycol sulfate In tetrahydrofuran at -78 - 20℃; for 3h; Inert atmosphere; Schlenk technique;
Stage #3: With sulfuric acid In water Inert atmosphere; Schlenk technique; Reflux;
86%
ethyleneglycol sulfate
1072-53-3

ethyleneglycol sulfate

8-cyclosporin

8-cyclosporin

C64H114N11O17S(1-)*Na(1+)

C64H114N11O17S(1-)*Na(1+)

Conditions
ConditionsYield
With sodium hydride In tetrahydrofuran at 30℃; for 2h;85%
ethyleneglycol sulfate
1072-53-3

ethyleneglycol sulfate

1-methyl-2-((trimethylsilyl)methyl)-1H-imidazole
91631-71-9

1-methyl-2-((trimethylsilyl)methyl)-1H-imidazole

lithium diphenylphosphide
65567-06-8, 4541-02-0

lithium diphenylphosphide

2-(2-(diphenylphosphino)ethyl)-1-methyl-1H-imidazol

2-(2-(diphenylphosphino)ethyl)-1-methyl-1H-imidazol

Conditions
ConditionsYield
Stage #1: ethyleneglycol sulfate; 1-methyl-2-[(trimethylsilyl)methyl]-1H-imidazole In tetrahydrofuran at -78 - 100℃; for 6h;
Stage #2: lithium diphenylphosphide at -78℃; Reflux;
85%
ethyleneglycol sulfate
1072-53-3

ethyleneglycol sulfate

(3S)-4-(4,6-dichloropyrimidin-2-yl)-3-methylmorpholine
1333108-98-7

(3S)-4-(4,6-dichloropyrimidin-2-yl)-3-methylmorpholine

2-{4,6-dichloro-2-[(3S)-3-methylmorpholin-4-yl]pyrimidin-5-yl}ethanol

2-{4,6-dichloro-2-[(3S)-3-methylmorpholin-4-yl]pyrimidin-5-yl}ethanol

Conditions
ConditionsYield
Stage #1: (3S)-4-(4,6-dichloropyrimidin-2-yl)-3-methylmorpholine With n-butyllithium In tetrahydrofuran at -78℃; for 0.5h;
Stage #2: ethyleneglycol sulfate In tetrahydrofuran for 0.5h;
Stage #3: With hydrogenchloride In tetrahydrofuran; water at 40℃; for 22h;
85%
ethyleneglycol sulfate
1072-53-3

ethyleneglycol sulfate

benzyl N-[2-[2-(cyanomethyl)phenoxy]ethyl]-N-methylcarbamate

benzyl N-[2-[2-(cyanomethyl)phenoxy]ethyl]-N-methylcarbamate

benzyl N-[2-[2-(1-cyanocyclopropyl)phenoxy]ethyl]-N-methylcarbamate

benzyl N-[2-[2-(1-cyanocyclopropyl)phenoxy]ethyl]-N-methylcarbamate

Conditions
ConditionsYield
Stage #1: benzyl N-[2-[2-(cyanomethyl)phenoxy]ethyl]-N-methylcarbamate With sodium hydroxide In dimethyl sulfoxide at 20 - 25℃; for 0.166667h;
Stage #2: ethyleneglycol sulfate In tetrahydrofuran; dimethyl sulfoxide at 20 - 25℃; for 16h;
84.6%
4,6-dichloro-2-(morpholine-4-yl)pyrimidine
10397-13-4

4,6-dichloro-2-(morpholine-4-yl)pyrimidine

ethyleneglycol sulfate
1072-53-3

ethyleneglycol sulfate

2-[4,6-dichloro-2-(morpholin-4-yl)pyrimidin-5-yl]ethanol

2-[4,6-dichloro-2-(morpholin-4-yl)pyrimidin-5-yl]ethanol

Conditions
ConditionsYield
Stage #1: 4,6-dichloro-2-(morpholine-4-yl)pyrimidine With n-butyllithium In tetrahydrofuran; hexane at -65℃; for 0.5h; Inert atmosphere;
Stage #2: ethyleneglycol sulfate In tetrahydrofuran; hexane at -65℃; for 1.5h;
Stage #3: With hydrogenchloride In tetrahydrofuran; hexane; water at 20℃; for 18h;
84%
Stage #1: 4,6-dichloro-2-(morpholine-4-yl)pyrimidine With n-butyllithium In tetrahydrofuran at -78℃; for 0.5h;
Stage #2: ethyleneglycol sulfate In tetrahydrofuran for 0.666667h;
Stage #3: With hydrogenchloride In tetrahydrofuran; water at 20 - 40℃; for 22h;
42%
2,2-bis((dodecyloxy)methyl)propane-1,3-diol

2,2-bis((dodecyloxy)methyl)propane-1,3-diol

ethyleneglycol sulfate
1072-53-3

ethyleneglycol sulfate

disodium 5,5-bis(dodecyloxymethyl)-3,7-dioxa-1,9-nonadiyl disulfate

disodium 5,5-bis(dodecyloxymethyl)-3,7-dioxa-1,9-nonadiyl disulfate

Conditions
ConditionsYield
Stage #1: 2,2-bis((dodecyloxy)methyl)propane-1,3-diol With sodium hydride In tetrahydrofuran; mineral oil for 0.5h; Cooling with ice;
Stage #2: ethyleneglycol sulfate In tetrahydrofuran; mineral oil at 20℃;
83.3%
Stage #1: 2,2-bis((dodecyloxy)methyl)propane-1,3-diol With sodium hydride In tetrahydrofuran; mineral oil for 0.5h; Cooling with ice;
Stage #2: ethyleneglycol sulfate In tetrahydrofuran; mineral oil at 20℃; for 21h;
83%
ethyleneglycol sulfate
1072-53-3

ethyleneglycol sulfate

tert-butyl cinnamate
14990-09-1

tert-butyl cinnamate

Lithium N-benzyl-N-(trimethylsilyl)amide
113709-50-5

Lithium N-benzyl-N-(trimethylsilyl)amide

(-)-tert-butyl (2S,3R)-1-benzyl-2-phenylazetidine-3-carboxylate
1394979-19-1

(-)-tert-butyl (2S,3R)-1-benzyl-2-phenylazetidine-3-carboxylate

Conditions
ConditionsYield
Stage #1: Lithium N-benzyl-N-(trimethylsilyl)amide With (1S,2S)-1,2-dimethoxy-1,2-diphenylethane In toluene at -78℃; for 0.583333h;
Stage #2: tert-butyl cinnamate In toluene at -78℃; for 1.63h;
Stage #3: ethyleneglycol sulfate enantioselective reaction; Further stages;
82%
ethyleneglycol sulfate
1072-53-3

ethyleneglycol sulfate

(μ-1,3-propanedithiolate)Fe2(CO)4[μ-3-(Ph2P)2NC5H4N]

(μ-1,3-propanedithiolate)Fe2(CO)4[μ-3-(Ph2P)2NC5H4N]

(μ-1,3-propanedithiolate)Fe2(CO)4[μ-3-(Ph2P)2NC5H4N((CH2)2OSO3)]

(μ-1,3-propanedithiolate)Fe2(CO)4[μ-3-(Ph2P)2NC5H4N((CH2)2OSO3)]

Conditions
ConditionsYield
In acetonitrile for 8h; Inert atmosphere; Schlenk technique; Reflux;81%
ethyleneglycol sulfate
1072-53-3

ethyleneglycol sulfate

N,N-dibenzylamino-acetonitrile
51643-96-0

N,N-dibenzylamino-acetonitrile

1-<(dibenzyl)amino>cyclopropanecarbonitrile
137360-51-1

1-<(dibenzyl)amino>cyclopropanecarbonitrile

Conditions
ConditionsYield
With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium diisopropyl amide In tetrahydrofuran at -70℃;80%
With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium diisopropyl amide In tetrahydrofuran at -70℃; for 1.5h; Product distribution; further dielectophiles; access to cyclopropane aminonitriles;
With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium diisopropyl amide In tetrahydrofuran at -70℃; for 1.5h; Yield given;
ethyleneglycol sulfate
1072-53-3

ethyleneglycol sulfate

(2S)-2-(6-methoxy(2-naphthyl))propanoic acid
22204-53-1

(2S)-2-(6-methoxy(2-naphthyl))propanoic acid

(S)-naproxen ethyl sulfate potassium salt

(S)-naproxen ethyl sulfate potassium salt

Conditions
ConditionsYield
With potassium tert-butylate In isopropyl alcohol at 45℃; for 0.166667h;80%
ethyleneglycol sulfate
1072-53-3

ethyleneglycol sulfate

bis(2-phenylpyridinato-N,C2)-mono(4-[hydroxymethyl]-2-pyridine carboxylato-N,O)iridium(III)

bis(2-phenylpyridinato-N,C2)-mono(4-[hydroxymethyl]-2-pyridine carboxylato-N,O)iridium(III)

tetrabutyl-ammonium chloride
1112-67-0

tetrabutyl-ammonium chloride

tetra-n-butylammonium bis(2-phenylpyridinato-N,C2)-mono(4-[sulfatoethyloxymethyl]-2-pyridinecarboxylato-N,O)iridium(III)
1119493-11-6

tetra-n-butylammonium bis(2-phenylpyridinato-N,C2)-mono(4-[sulfatoethyloxymethyl]-2-pyridinecarboxylato-N,O)iridium(III)

Conditions
ConditionsYield
With NaH In N,N-dimethyl-formamide (N2, in the absence of light); a soln. of Ir complex stirred at 0°C for 30 min, NaH added, stirred at room temp. for 16 h, (CH2O)2SO2 added, stirred for 12 h; concd., pptd. in Et2O, dissolved in CH2Cl2, added to an aq. soln. of N(C4H9)4Cl, stirred for 16 h, the org. layer sepd., washed (H2O), dried (MgSO4), concd., pptd. in Et2O; elem. anal.;80%
ethyleneglycol sulfate
1072-53-3

ethyleneglycol sulfate

methyl 2-(pyrimidin-5-yl)acetate

methyl 2-(pyrimidin-5-yl)acetate

methyl 1-(pyrimidin-5- yl)cyclopropane-1-carboxylate

methyl 1-(pyrimidin-5- yl)cyclopropane-1-carboxylate

Conditions
ConditionsYield
Stage #1: methyl 2-(pyrimidin-5-yl)acetate With lithium hexamethyldisilazane In tetrahydrofuran at -70℃; for 1h;
Stage #2: ethyleneglycol sulfate In tetrahydrofuran at -70 - -20℃; for 1.5h;
Stage #3: With lithium hexamethyldisilazane In tetrahydrofuran at -72 - 20℃; for 15h;
80%
thiophene
188290-36-0

thiophene

ethyleneglycol sulfate
1072-53-3

ethyleneglycol sulfate

2-thiophenethanol
5402-55-1

2-thiophenethanol

Conditions
ConditionsYield
Stage #1: thiophene With n-butyllithium In tetrahydrofuran; hexane at -78℃;
Stage #2: ethyleneglycol sulfate In tetrahydrofuran; hexane at -78 - 20℃;
Stage #3: With sulfuric acid In tetrahydrofuran; hexane for 3h; Heating; Further stages.;
79%
ethyleneglycol sulfate
1072-53-3

ethyleneglycol sulfate

Benzo[b]thiophene
95-15-8

Benzo[b]thiophene

2-(β-Hydroxyethyl)-benzothiophene
30962-69-7

2-(β-Hydroxyethyl)-benzothiophene

Conditions
ConditionsYield
Stage #1: Benzo[b]thiophene In tetrahydrofuran; hexanes at -50 - -40℃; for 0.75h;
Stage #2: ethyleneglycol sulfate In tetrahydrofuran; hexanes at -40 - 20℃;
Stage #3: With acetyl chloride In methanol at 20℃; for 4.25h;
79%
ethyleneglycol sulfate
1072-53-3

ethyleneglycol sulfate

cyclopentylacetic acid methyl ester
2723-38-8

cyclopentylacetic acid methyl ester

3-cyclopentyldihydrofuran-2(3H)-one

3-cyclopentyldihydrofuran-2(3H)-one

Conditions
ConditionsYield
Stage #1: cyclopentylacetic acid methyl ester With lithium diisopropyl amide In tetrahydrofuran at -78℃;
Stage #2: ethyleneglycol sulfate In tetrahydrofuran at -78 - 20℃; for 5h;
Stage #3: With sulfuric acid In toluene Reflux;
79%
ethyleneglycol sulfate
1072-53-3

ethyleneglycol sulfate

di-isopropylphosphine
20491-53-6

di-isopropylphosphine

diphenylphosphane
829-85-6

diphenylphosphane

(CH(CH3)2)2PCH2CH2P(C6H5)2
262359-83-1

(CH(CH3)2)2PCH2CH2P(C6H5)2

Conditions
ConditionsYield
Multistep reaction;76%
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