CAS No.7719-09-7,Thionyl chloride Suppliers,MSDS download

Lonwin Chemical Group Limited

Thionyl chloride CAS：7719-09-7 Specification Welcome to contact us to get complete COA. Shanghai Lonwin Chemical Co.,Ltd is a leading manufacturer and supplier of chemicals in China.We develop,produce and distribute high quality pharmaceutic

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Cas:7719-09-7

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Hunan Russell Chemicals Technology Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China

thionyl dichloride 7719-09-7

Cas:7719-09-7

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Shang Hai Grade Biochemical Co,. Limited

low price and good quality Application:It is an important raw material and intermediate used in Organic Synthesis, Pharmaceuticals, Agrochemicals and D

Thionyl chloride

Cas:7719-09-7

Min.Order:0

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ZHENFEI INDUSTRY CO.,LTD

Thionyl chloride

Cas:7719-09-7

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Synthetic route

: 10545-99-0
sulfur dichloride

: 7446-11-9
sulfur trioxide

A: 7719-09-7
thionyl chloride

B: 7446-09-5
sulfur dioxide

Conditions

Conditions	Yield
In neat (no solvent) below -10°C or under pressure;;	A 100% B n/a

...Expand

: 7647-01-0
hydrogenchloride

: 222851-56-1
N-phenylsulfinylamine

A: 7719-09-7
thionyl chloride

B: 142-04-1
aniline hydrochloride

Conditions

Conditions	Yield
In Petroleum ether decompn. of thioaniline dissolved in dild. petroleum (b.p. 200-250°C) on introduction of dry HCl (shaking) at -10°C;; filtration (anilinium chloride); fractionation;;	A 94% B n/a

...Expand

: 10545-99-0
sulfur dichloride

: 7446-11-9
sulfur trioxide

A: 7719-09-7
thionyl chloride

B: 7791-27-7
pyrosulfuryl chloride

C: 7446-09-5
sulfur dioxide

Conditions

Conditions	Yield
In neat (no solvent) SO3 is distilled (from 65 % oleum) into cooled (ice/water) vessel containing SCl2; evolution of SO2;; multiple fractionation (at last in presence of sulfur);;	A 80% B n/a C n/a

...Expand

: 56-23-5
tetrachloromethane

A: 75-44-5
phosgene

B: 7719-09-7
thionyl chloride

Conditions

Conditions	Yield
With sulfur dioxide In neat (no solvent) reaction of CCl4 with SO2 on heating to 200°C;;	A n/a B 72%

: 594-44-5
Ethanesulfonyl chloride

A: 7719-09-7
thionyl chloride

B: 75-00-3
chloroethane

C: 10026-13-8, 874483-75-7
phosphorus pentachloride

D: 10025-87-3, 12599-09-6, 63736-95-8
trichlorophosphate

...Expand

: 10026-13-8, 874483-75-7
phosphorus pentachloride

: 98-09-9
benzenesulfonyl chloride

A: 7719-09-7
thionyl chloride

B: 108-90-7
chlorobenzene

C: 10025-87-3, 12599-09-6, 63736-95-8
trichlorophosphate

Conditions

Conditions	Yield
at 200 - 210℃;

...Expand

: 56-23-5
tetrachloromethane

: 7446-70-0
aluminium trichloride

SO2: SO2

: 7719-09-7
thionyl chloride

Conditions

Conditions	Yield
at 200℃; unter Druck;

...Expand

: 75-15-0
carbon disulfide

hypochlorous acid anhydride: hypochlorous acid anhydride

A: 75-44-5
phosgene

B: 7719-09-7
thionyl chloride

...Expand

: 75-44-5
phosgene

SO2: SO2

A: 7719-09-7
thionyl chloride

B: 124-38-9
carbon dioxide

C sulfur chloride: sulfur chloride

Conditions

Conditions	Yield
at 200 - 400℃;

...Expand

: 2547-61-7
Trichloromethanesulfonyl chloride

A: 56-23-5
tetrachloromethane

B: 75-44-5
phosgene

C: 7719-09-7
thionyl chloride

D sulfur dioxide: sulfur dioxide

Conditions

Conditions	Yield
at 200℃;

...Expand

: 7446-70-0
aluminium trichloride

: 67-66-3
chloroform

SO2: SO2

: 7719-09-7
thionyl chloride

Conditions

Conditions	Yield
at 150℃;

...Expand

: 623-81-4
diethyl sulphite

: 10026-13-8, 874483-75-7
phosphorus pentachloride

A: 7719-09-7
thionyl chloride

B: 6378-11-6
ethyl chlorosulfite

C: 75-00-3
chloroethane

Conditions

Conditions	Yield
bei niedrigerer Temperatur;

...Expand

: 623-98-3
dipropyl sulfite

: 10026-13-8, 874483-75-7
phosphorus pentachloride

A: 7719-09-7
thionyl chloride

B: 540-54-5
1-Chloropropane

Conditions

Conditions	Yield
beim Erwaermen;

...Expand

: 626-85-7
sulfurous acid dibutyl ester

: 10026-13-8, 874483-75-7
phosphorus pentachloride

A: 7719-09-7
thionyl chloride

B: 109-69-3
n-Butyl chloride

Conditions

Conditions	Yield
bei schwachem Erwaermen;

...Expand

: 7446-70-0
aluminium trichloride

: 7791-25-5
sulfuryl dichloride

: 95-94-3
1,2,4,5-tetrachlorobenzene

disulfur dichloride: disulfur dichloride

A: 56-23-5
tetrachloromethane

B: 7719-09-7
thionyl chloride

C: 608-93-5
pentachlorobenzene

D: 118-74-1
hexachlorobenzene

...Expand

: 6378-11-6
ethyl chlorosulfite

: 10026-13-8, 874483-75-7
phosphorus pentachloride

A: 7719-09-7
thionyl chloride

B: 75-00-3
chloroethane

C: 10025-87-3, 12599-09-6, 63736-95-8
trichlorophosphate

Conditions

Conditions	Yield
at 25℃;

...Expand

: 98-67-9
p-hydoroxybenzenesulfonic acid

: 10026-13-8, 874483-75-7
phosphorus pentachloride

A: 7719-09-7
thionyl chloride

B: 106-46-7
para-dichlorobenzene

C: 772-79-2
4-chlorophenylphosphorodichloridate

D: 10025-87-3, 12599-09-6, 63736-95-8
trichlorophosphate

Conditions

Conditions	Yield
Reaktion des Kaliumsalzes;

...Expand

: 623-81-4
diethyl sulphite

: 10026-13-8, 874483-75-7
phosphorus pentachloride

A: 7719-09-7
thionyl chloride

B: 75-00-3
chloroethane

C SO2: SO2

...Expand

: 10026-13-8, 874483-75-7
phosphorus pentachloride

: 32337-45-4
4,4'-sulfonyl-bis-benzenesulfonyl chloride

A: 7719-09-7
thionyl chloride

B: 106-46-7
para-dichlorobenzene

C: 10025-87-3, 12599-09-6, 63736-95-8
trichlorophosphate

D: 7719-12-2, 52843-90-0
phosphorus trichloride

...Expand

: 10026-13-8, 874483-75-7
phosphorus pentachloride

: 85-46-1
1-Naphthalenesulfonyl chloride

A: 7719-09-7
thionyl chloride

B: 10025-87-3, 12599-09-6, 63736-95-8
trichlorophosphate

C: 90-13-1
1-Chloronaphthalene

Conditions

Conditions	Yield
at 150 - 160℃;

...Expand

: 4895-65-2
phenyltetrachlorophosphorane

sulfur dioxide: sulfur dioxide

A: 824-72-6
P,P-dichlorophenylphosphine oxide

B: 7719-09-7
thionyl chloride

...Expand

: 13165-73-6
phenyl chlorosulphinate

A: 7719-09-7
thionyl chloride

B: 4773-12-0
diphenyl sulfite

Conditions

Conditions	Yield
at 70℃; Einleiten von HCl;

: 13165-73-6
phenyl chlorosulphinate

: 10025-87-3, 12599-09-6, 63736-95-8
trichlorophosphate

A: 7719-09-7
thionyl chloride

B: 115-86-6
phosphoric acid triphenyl ester

...Expand

: 861087-97-0
2-benzoylamino-[1]naphthoic acid

A: 7719-09-7
thionyl chloride

B: 2-benzoyl-2H-naphth[2,1-b]azet-1-one

: 10026-13-8, 874483-75-7
phosphorus pentachloride

: 2,2'-sulfonyl-bis-benzenesulfonyl chloride

A: 7719-09-7
thionyl chloride

B: 95-50-1
1,2-dichloro-benzene

Conditions

Conditions	Yield
at 200 - 210℃;

...Expand

: tetrachloro-dipropylamino-phosphorane; compound with phosphorus pentachloride

SO2: SO2

A: 7719-09-7
thionyl chloride

B: 40881-98-9
N,N-dipropylphosphoramidic dichloride

C: 10025-87-3, 12599-09-6, 63736-95-8
trichlorophosphate

...Expand

: 10026-13-8, 874483-75-7
phosphorus pentachloride

: phenyl-methanesulfonic acid ; potassium salt

A: 7719-09-7
thionyl chloride

B: 100-44-7
benzyl chloride

C: 10025-87-3, 12599-09-6, 63736-95-8
trichlorophosphate

...Expand

: 2',2',2'-Trichloroethyl 3-methyl-2-[2-chlorosulfinyl-4-oxo-3-(2-tert-butoxycarbonylamino-2-phenylacetamido)-1-azetidinyl]-3-butenoate

A: 7719-09-7
thionyl chloride

B: 2',2',2'-Trichloroethyl 3-methyl-2-[2-sulfino-4-oxo-3-(2-tert-butoxycarbonylamino-2-phenylacetamido)-1-azetidinyl]-3-butenoate

Conditions

Conditions	Yield
In acetone

: 75-15-0
carbon disulfide

: 7791-21-1
hypochlorous anhydride

A: 75-44-5
phosgene

B: 7719-09-7
thionyl chloride

Conditions

Conditions	Yield
In tetrachloromethane CS2 dild. in CCl4 (to diminuish vehemence of reaction);;
In tetrachloromethane

...Expand

: 7719-09-7
thionyl chloride

: (S)-4,5,6,7-tetrahydro-3H-imidazo[4,5-c]pyridine-6-carboxylic acid dihydrochloric acid salt

: 114786-39-9
methyl (S)-4,5,6,7-tetrahydro-3H-imidazo[4,5-c]pyridine-6-carboxylate hydrochloric acid salt

Conditions

Conditions	Yield
In methanol for 3.5h; Heating / reflux;	100%

: 7719-09-7
thionyl chloride

: bis(tetrabutylammonium) hexatungstate

: N(C4H9)4(1+)*WOCl5(1-) = [N(C4H9)4][WOCl5]

Conditions

Conditions	Yield
In thionyl chloride (argon); stirring (ca. 16 h); pptn. with Et2O, washing (Et2O), drying (vac.);	100%

: 7719-09-7
thionyl chloride

: tetrabutylammonium decatungstate ammonium salt

: N(C4H9)4(1+)*WOCl5(1-) = [N(C4H9)4][WOCl5]

Conditions

Conditions	Yield
In thionyl chloride (argon); stirring (ca. 16 h); pptn. with Et2O, washing (Et2O), drying (vac.);	100%

: 7719-09-7
thionyl chloride

: (5,7,12,14-tetramethyldibenzo[b,i][1,4,8,11]tetraazacyclotetradecinate(2-))V=O

: 173105-66-3
(5,7,12,14-tetramethyldibenzo[b,i][1,4,8,11]tetraazacyclotetradecinate(2-))VCl2

Conditions

Conditions	Yield
In dichloromethane (Ar); react. (0°C), warming (room temp.), stirring (6 h), solventevapn.; washing (diethyl ether, pentane), drying (high vacuum, 50°C, 8 h);	100%

: 7719-09-7
thionyl chloride

: Se4(1+)*[MoOCl4](1-)=Se4[MoOCl4]

: [SeCl3][MoOCl4], β

Conditions

Conditions	Yield
In thionyl chloride vac., 150°C, 3 d;	100%

: 7719-09-7
thionyl chloride

: 6575-24-2
2-(2,6-dichlorophenyl)acetic acid

: 880089-70-3
1-bromo-3-(2,6-dichlorophenyl)propan-2-one

Conditions

Conditions	Yield
Stage #1: thionyl chloride; 2-(2,6-dichlorophenyl)acetic acid With diazomethyl-trimethyl-silane Stage #2: With hydrogen bromide In water	100%

: 7719-09-7
thionyl chloride

: 1218941-06-0
C14H12Cl2N2O3S

: 1218941-07-1
C14H11Cl3N2O2S

Conditions

Conditions	Yield
	100%

: 7719-09-7
thionyl chloride

: 1376437-09-0
4-[1-(trifluoroacetyl)piperidin-4-yl]benzoic acid

: 1331747-36-4
4-(1-(2,2,2-trifluoroacetyl)piperidin-4-yl)benzoyl chloride

Conditions

Conditions	Yield
In N,N-dimethyl-formamide at 70℃; for 5h; Sealed tube;	100%

: 7719-09-7
thionyl chloride

: 47818-40-6
dimer acid

: C36H62Cl2O2

Conditions

Conditions	Yield
With triethylamine In ethyl acetate at 35℃; for 4h; Inert atmosphere;	100%

: 7719-09-7
thionyl chloride

: cobalt(II) 2,9,16,23-phthalocyanine tetrasulfonic acid

: cobalt[2,9,16,23-tetrakis(chlorosulfonyl)]phthalocyanine

Conditions

Conditions	Yield
at 80℃; for 12h;	100%

: 67-56-1
methanol

: 7719-09-7
thionyl chloride

: 5334-40-7
4-nitro-1H-pyrazole-3-carboxylic acid

: 138786-86-4
methyl 4-nitro-1H-pyrazole-3-carboxylate

Conditions

Conditions	Yield
at 0 - 25℃; for 16 - 48h; Product distribution / selectivity;	99.5%

...Expand

: 7783-99-5
silver(I) nitrite

: 7719-09-7
thionyl chloride

A: 2696-92-6
nitrosylchloride

B: silver(I) chloride

Conditions

Conditions	Yield
In diethyl ether byproducts: SO2; to finely ground dry Ag salt in anhyd. Et2O cooled to 0°C added dropwise with vigorous stirring equimolar amt. of thionyl chloride; suspn. stirred for 15 min; soln. was decanted from AgCl; AgCl dried; soln. washed (Et2O); all extracts combined; cooled to 0°C;	A n/a B 99%

...Expand

: 7719-09-7
thionyl chloride

: silver nitrate

A: Nitryl chloride

B: 2696-92-6
nitrosylchloride

C: silver(I) chloride

Conditions

Conditions	Yield
In diethyl ether byproducts: SO2, SO3; to finely ground dry Ag salt in anhyd. Et2O cooled to 0°C added dropwise with vigorous stirring equimolar amt. of thionyl chloride; suspn. stirred for 15 min; soln. was decanted from AgCl; AgCl dried; soln. washed (Et2O); all extracts combined; cooled to 0°C;	A n/a B n/a C 99%

...Expand

: 7719-09-7
thionyl chloride

: (4,4'-dicarboxy-2,2'-bipyridine)bis(2,2'-bipyridine)ruthenium-(II) dichloride dihydrate

: (4,4'-bis(chlorocarbonyl)-2,2'-bipyridine)bis(2,2'-bipyridine)ruthenium-(II) dichloride*SOCl2*HCl

Conditions

Conditions	Yield
In dichloromethane (N2); stirring (4 h, reflux); solvent removal (reduced pressure), drying (vac., 60-70 degree.C, 1 h); elem. anal.;	99%

: 7719-09-7
thionyl chloride

: tributylammonium dodecaborododecahydride

: 2(C4H9)3NH(1+)*B12H9(SO)3(2-)=((C4H9)3NH)2(B12H9(SO)3)

Conditions

Conditions	Yield
In dichloromethane SOCl2 added to CH2Cl2 soln. of B compd. (molar ratio 1:3, 1:4); concd. slowly; ppt. purified by column chromy. (silica gel, CH2Cl2);	99%
In neat (no solvent) excess of SOCl2 added to B compd.; purified by column chromy. (silica gel, CH2Cl2);	99%
In dichloromethane SOCl2 added to CH2Cl2 soln. of B compd. (molar ratio 2:1, 1:1, 1:2); concd. slowly; mixt. of the starting B compd. and title compd. pptd.; purified by column chromy. (silica gel, CH2Cl2);	15%

: 7719-09-7
thionyl chloride

: 864767-27-1
[(C5(CH3)5)TiCl(C5H4C(CH3)2CH2CO2)]

: 864767-39-5
[(C5(CH3)5)TiCl2(C5H4C(CH3)2CH2COCl)]

Conditions

Conditions	Yield
In not given	99%

: 7719-09-7
thionyl chloride

: 864766-99-4
chloro(cyclopentadienyl)(cyclopentadienyl-3-methyl-3-butanoate)titanium(IV)

: 864767-00-0
Cp(CpCMe2CH2COCl)titanium(IV)dichloride

Conditions

Conditions	Yield
In not given	99%
In neat (no solvent) at 20℃; for 1h; Inert atmosphere; Schlenk technique; Glovebox;

: 7719-09-7
thionyl chloride

: 864767-24-8
[(C5H5)TiCl(C5H4C(CH2)5CH2CO2)]

: 864767-36-2
[(C5H5)TiCl2(C5H4C(CH2)5CH2COCl)]

Conditions

Conditions	Yield
In not given	99%

: 7719-09-7
thionyl chloride

: 864766-99-4
chloro(cyclopentadienyl)(cyclopentadienyl-3-methyl-3-butanoate)titanium(IV)

: 57-88-5
cholesterol

: [(C5H5)TiCl2(C5H4C(CH3)2CH2CO2C27H45)]

Conditions

Conditions	Yield
With sodium hydride In dichloromethane mixt. of Ti complex and SOCl2 was stirred for 3 h; evapd. (vac., 80°C); dissolved in CH2Cl2; added to mixt. of NaH and cholesterol; stirred for 16 h; filtered; solvent removed (vac.); crystd. (CH2Cl2);	99%

...Expand

: 7719-09-7
thionyl chloride

: 1122084-99-4
[(C5H5)TiCl(C5H4C(CH3)2CH2CH2CO2)]

: 57-88-5
cholesterol

: [(C5H5)TiCl2(C5H4C(CH3)2(CH2)2CO2C27H45)]

Conditions

Conditions	Yield
With sodium hydride In dichloromethane mixt. of Ti complex and SOCl2 was stirred for 3 h; evapd. (vac., 80°C); dissolved in CH2Cl2; added to mixt. of NaH and cholesterol; stirred for 16 h; filtered; solvent removed (vac.); crystd. (CH2Cl2);	99%

...Expand

: 7719-09-7
thionyl chloride

: 1202357-35-4
(4R,5S)-5-phenylthio-4-octanol

: 1202357-36-5
((4S,5R)-5-chlorooctan-4-yl)(phenyl)sulfane

Conditions

Conditions	Yield
With N,N-dimethyl-formamide In dichloromethane at 0℃; for 0.5h; Inert atmosphere; optical yield given as %ee;	99%

: 7719-09-7
thionyl chloride

: 50571-15-8
1,7-dihydroxycarbonyl-1,7-dicarba-closo-dodecaborane

: 23810-52-8
m-carborane-1,7-dicarboxylic acid dichloride

Conditions

Conditions	Yield
In thionyl chloride B compd. and SOCl2 placed into a flask under N2, refluxed for 24 h; evapd. (vac.); obtained as an oil;	99%

: 7719-09-7
thionyl chloride

: 372515-55-4
tris(8-carboxyl-2,2,6,6-tetramethylbenzo[1,2-d;4,5-d′]bis[1,3]dithiol-4-yl)methyl radical sodium salt

: 1079975-19-1
C40H36Cl3O3S12

Conditions

Conditions	Yield
Stage #1: tris(8-carboxyl-2,2,6,6-tetramethylbenzo[1,2-d;4,5-d′]bis[1,3]dithiol-4-yl)methyl radical sodium salt With triethylamine In chloroform at 20℃; for 0.5h; Stage #2: thionyl chloride In chloroform at 20 - 50℃;	99%

: 7719-09-7
thionyl chloride

: thallium chloride

: 7782-50-5
chlorine

: 13453-32-2
thallium (III) chloride

Conditions

Conditions	Yield
In acetonitrile TlCl suspd. in CH3CN; Cl2 added under vigorous stirring; stirred for 30 min; soln. filtered; solvent evapd. in vacuum; SOCl2 added; evapd. after 10 min;	98.5%

...Expand

: 7719-09-7
thionyl chloride

: 10113-29-8
tetrabenzyltin

A: 41719-05-5
phenylmethanesulfinyl chloride

B: 3002-01-5
dibenzyltin(IV) dichloride

Conditions

Conditions	Yield
In not given dropwise addn. of thionyl chloride to tetraalkyltin(IV) compd. under dry N2 atmosphere under ice cooling, warming to room temp., refluxing for 30 min; distn. (removal of excess of SOCl2), cooling resulting liquids, sepn., elem. anal.;	A n/a B 98%

...Expand

: 7719-09-7
thionyl chloride

: 69934-86-7
(29H,31H-2,9,16,23-tetracarboxyphthalocyaninato-N(29),N(30),N(31),N(32))cobalt(II)

: 73533-44-5
cobalt tetra-4-(chlorocarbonyl)phthalocyanine

Conditions

Conditions	Yield
In benzene a mixt. in dry benzene was refluxed for 7 h; filtered, washed with dry benzene, dried in a vac. at room temp.;	98%
With pyridine In benzene at 80℃;	96%

: 7719-09-7
thionyl chloride

: 72850-61-4
2-chloro-4-(trifluoromethyl)-5-thiazolecarboxylic acid

: 72850-62-5
2-chloro-4-(trifluoromethyl)-5-thiazolecarbonyl chloride

Conditions

Conditions	Yield
6 h refluxing with excess SOCl2;	98%

: 7719-09-7
thionyl chloride

: 683816-30-0
(m-carborane-9,10-diyl)diacetic acids

: 683816-32-2
(m-carboranyl-9,10-diyl)di(acetyl chlorides)

Conditions

Conditions	Yield
In benzene byproducts: SO2, HCl; addn. of SOCl2 to soln. of (CH2COOH)2C2B10H10 in dry benzene at 20°C; heating for 2 h; cooling, removal of solvent and excess SOCl2 in vac.;	98%