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inquirySynonyms: Benzenoform;Benzinoform;Benzinofrm;Carbon chloride;Carbon chloride (CCl4);Carbon tet;carbon(IV)chloride;Carbona CAS: 56-23-5 MF: CCl4 MW: 153.82 EINECS: 203-453-4 Product Categories: CFC;refrigerants;Organics;Analytical Chemistry;Sta
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Carbon tetrachloride Basic information Product Name: Carbon tetrachloride Synonyms: Benzenoform;Benzinoform;Benzinofrm;Carbon chloride;Carbon chloride (CCl4);Carbon tet;carbon(IV)chloride;Carbona
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inquirybis(trichloromethyl) carbonate
A
tetrachloromethane
B
phosgene
C
carbon dioxide
Conditions | Yield |
---|---|
With copper phthalocyanine at 90℃; for 0.583333h; Mechanism; Reagent/catalyst; Temperature; Time; | A n/a B 100% C n/a |
Conditions | Yield |
---|---|
With chlorine; aluminum oxide; molybdenum(VI) oxide at 380 - 400℃; for 0.00277778h; other metal oxide catalysts; | A 98.2% B 96.3% |
Conditions | Yield |
---|---|
With 2,2'-azobis(isobutyronitrile); chlorine; aluminum oxide; molybdenum(VI) oxide at 380 - 400℃; for 0.00277778h; | A 95.15% B 98.06% |
Conditions | Yield |
---|---|
iron(III) chloride Kinetics; heating in a sealed tube, 350°C 26 atm 20 h; | A 86% B n/a |
iron(III) chloride Kinetics; heating in a sealed tube, 400°C 28 atm 17 h; | A 84% B n/a |
aluminium trichloride Kinetics; heating in a sealed tube, 400°C 144 atm 2 h; | A 81% B n/a |
toluene
A
tetrachloromethane
B
hexachlorobenzene
C
α,α,2,3,4,5,6-pentachlorotoluene
Conditions | Yield |
---|---|
With chlorine; KSK silica gel; magnesium chloride at 295 - 320℃; for 0.005h; other methal oxide and chloride catalysts; | A n/a B n/a C 84% |
arsenic pentafluoride
trans-CF3SF4Cl
A
tetrachloromethane
B
chlorodifluorosulfur(IV) hexafluoroarsenate
Conditions | Yield |
---|---|
In neat (no solvent) The react. mixt. is warmed slowly from -78°C to +25°C over a period of 12-16 h.; Elem.anal.; | A n/a B 70% |
In dichloromethane The react. mixt. is warmed slowly from -78°C to +25°C over a period of 12-16 h.; Elem.anal.; | A n/a B 70% |
In neat (no solvent) Rapid warmup of the react. mixt.; Elem.anal.; | A n/a B 50% |
In dichloromethane Rapid warmup of the react. mixt.; Elem.anal.; | A n/a B 50% |
methane
A
tetrachloromethane
B
methylene chloride
C
dichloromethane
D
chloroform
E
methanesulfonyl chloride
Conditions | Yield |
---|---|
With hydrogenchloride; sulfur dioxide; chlorine at 63 - 67℃; under 6750.68 Torr; Photolysis; | A n/a B n/a C n/a D n/a E 55% |
phosgene
hydrogen fluoride
chlorine
A
tetrachloromethane
B
chlorotrifluoromethane
C
Dichlorodifluoromethane
D
trichlorofluoromethane
Conditions | Yield |
---|---|
With catalyst : charcoal heating in autoclave, 350°C, 6 h, charcoal impregnated with FeCl3; | A 7% B 13% C 47% D 7% |
perfluoro(N,N-diethylcarbamoyl fluoride)
A
tetrachloromethane
B
phosgene
Conditions | Yield |
---|---|
With aluminium trichloride at 100℃; for 100h; | A 0.03 g B 0.02 g C 38.7% |
Conditions | Yield |
---|---|
In neat (no solvent) equilibrium over catalyst; equilibrium constant at 290-540°C;; | A n/a B 22% |
Conditions | Yield |
---|---|
With mercury dichloride In ethanol reaction in abs. alcohol at 100°C for 6 h;; | 17% |
With chlorine im Licht; | |
With chlorine at 100℃; |
methane
A
tetrachloromethane
B
methylene chloride
C
dichloromethane
D
chloroform
Conditions | Yield |
---|---|
With chlorine for 4h; Product distribution; Ambient temperature; var. catalysts and times; | A 4.8% B 6.5% C 15% D 14% |
With molybdenum(V) chloride at 699.9℃; Product distribution; Mechanism; var. time, temp., and transition-metal chlorides; var. methane and argon flow rates; | |
With copper dichloride In melt at 449.9℃; Kinetics; Product distribution; further temperatures and concentrations; |
Conditions | Yield |
---|---|
at 168℃; |
Conditions | Yield |
---|---|
With chlorine | |
With iodine; chlorine |
Conditions | Yield |
---|---|
With chlorine |
phosgene
Carbonyl fluoride
A
tetrachloromethane
B
chlorotrifluoromethane
C
Dichlorodifluoromethane
D
trichlorofluoromethane
Conditions | Yield |
---|---|
at 420 - 450℃; Produkt 5-8:Carbonylchloridfluorid,Carbonylchlorid,Kohlendioxid,Tetrafluormethan; | |
at 450℃; Produkt 5-8:Carbonylchloridfluorid,Carbonylchlorid,Kohlendioxid,Tetrafluormethan; |
Conditions | Yield |
---|---|
With phosphorus pentachloride at 370℃; |
2-benzothiazolylsulfenyl chloride
A
tetrachloromethane
B
S-benzothiazol-2-yl-N-phenyl-thiohydroxylamine
Conditions | Yield |
---|---|
With aniline | |
With aniline |
Conditions | Yield |
---|---|
at 700 - 800℃; Chlorierung; |
Conditions | Yield |
---|---|
With ammonium chloride at 200℃; | |
With aluminium trichloride at 100℃; | |
With iron at 37℃; | |
at 200℃; |
Conditions | Yield |
---|---|
With iron at 37℃; |
Conditions | Yield |
---|---|
With chlorine at 400℃; under 51485.6 Torr; |
methane
tetrachloromethane
Conditions | Yield |
---|---|
With pumice stone; chlorine at 380 - 400℃; | |
With chlorine at 305℃; beim Belichtung und Leiten des Reaktionsgemisches ueber Aktivkohle bei 453grad; | |
With air; pumice stone; chlorine; copper dichloride at 430℃; |
Conditions | Yield |
---|---|
With nitrosylchloride at 350℃; | |
With chlorine at 550℃; under 4897.34 Torr; Temperature; Flow reactor; |
1,1,2,3,4,5,5,5-octachloro-penta-1,3-diene
A
tetrachloromethane
B
1,1,2,2-tetrachloroethylene
C
Hexachlorobutadiene
D
hexachlorocyclopentadiene
Conditions | Yield |
---|---|
at 450 - 500℃; Reaktion mit:Produkt5:Hexachlorbenzol;bei der Pyrolyse des Dampfes Hexachloraethan;bei der Pyrolyse in fluessiger Phase Octachlorcyclopenten und ein Octachlor-1-methylen-cyclopenten.; | |
at 270℃; Reaktion mit:Produkt5:Hexachlorbenzol;bei der Pyrolyse des Dampfes Hexachloraethan,bei der Pyrolyse in fluessiger Phase Octachlorcyclopenten und ein Octachlor-1-methylen-cyclopenten.; |
Conditions | Yield |
---|---|
With chlorine bei hoeherer Temperatur oder im Licht auch mit Chlorderivate des Edukts 1.; | |
With chlorine bei hoeherer Temperatur oder im Licht auch mit Chlorderivate des Edukts 1.; |
Conditions | Yield |
---|---|
With chlorine bei hoeherer Temperatur oder im Licht auch mit Chlorderivate des Edukts 1.; | |
With chlorine bei hoeherer Temperatur oder im Licht auch mit Chlorderivate des Edukts 1.; |
propane
A
tetrachloromethane
B
1,1,2,2-tetrachloroethylene
C
hexachloroethane
D
hexachlorobenzene
Conditions | Yield |
---|---|
Chlorierung und Spaltung der Reaktionsprodukten im Licht bei 460-480grad; | |
Chlorierung und Spaltung der Reaktionsprodukten an Aktivkohle bei 600-650grad; | |
Chlorierung und Spaltung der Reaktionsprodukten im Licht bei 460-480grad; | |
Chlorierung und Spaltung der Reaktionsprodukten in CCl4 bei 200grad und 40-50 at; | |
Chlorierung und Spaltung der Reaktionsprodukten in CCl4 oder CCl4 + Tetrachloraethylen als Verduennungsmittel bei 610-625grad; |
Conditions | Yield |
---|---|
at 400 - 700℃; Chlorierung in Gegenwart von Katalysatoren; |
dichloromethane
A
tetrachloromethane
B
1,1,2,2-tetrachloroethylene
C
hexachloroethane
D
hexachlorobenzene
Conditions | Yield |
---|---|
at 400 - 700℃; Chlorierung; |
tetrachloromethane
ethyl vinyl ether
Ethyl-(1,3,3,3-tetrachlor-propyl)-ether
Conditions | Yield |
---|---|
With dibenzoyl peroxide | 100% |
With dibenzoyl peroxide for 2h; Heating; | 90.3% |
With pyridine; dibenzoyl peroxide |
tetrachloromethane
N-formyl-N-(4-methylpent-4-enyl)-4-methylbenzenesulfonamide
N-(2,2-dichlorovinyl)-N-(4-methylpent-4-enyl)-4-methylbenzenesulfonamide
Conditions | Yield |
---|---|
With triphenylphosphine In tetrahydrofuran at 60℃; for 6h; | 100% |
Conditions | Yield |
---|---|
In tetrahydrofuran with cooling; pptn.;; | 100% |
In tetrahydrofuran addn. of CCl4 to Cr complex soln. with cooling in H2O bath;; | 100% |
In tetrahydrofuran addn. of CCl4 to Cr complex soln. with cooling in H2O bath;; | 100% |
Conditions | Yield |
---|---|
With CO In dichloromethane-d2 Irradiation (UV/VIS); 355-385 nm; 20 atm CO;; | A 100% B n/a C n/a D n/a |
tetrachloromethane
(2,4,6-tris{bis(trimethylsilyl)methyl}phenyl)(phenyl)dihydrostannane
Conditions | Yield |
---|---|
In tetrachloromethane dissoln. stannane in CCl4; stirring soln. at room temp., 10h;; removal of solvent; recrystn. from ethanol; elem. anal.;; | 100% |
tetrachloromethane
(mesityl)(2,4,6-tris{bis(trimethylsilyl)methyl}phenyl)dihydrostannane
Conditions | Yield |
---|---|
In tetrachloromethane dissoln. stannane in CCl4; stirring soln. at room temp., 10h;; removal of solvent; recrystn. from ethanol; elem. anal.;; | 100% |
Conditions | Yield |
---|---|
In benzene-d6 Ar-atmosphere; stirring (room temp., 1.5 h); detd. by (1)H and (31)P NMR spectroscopy; | 100% |
Conditions | Yield |
---|---|
In tetrachloromethane Irradiation (UV/VIS); irradn. (>300 nm); | 100% |
tetrachloromethane
Conditions | Yield |
---|---|
In benzene-d6 N2-atmosphere, NMR tube, 2 h; detd. by NMR spectroscopy; | 100% |
tetrachloromethane
[(CO)3Mo(C5H4C2H4NHC(O)C14H7O2)]2
(C14H7O2C(O)NHC2H4C5H4)Mo(CO)3(Cl)
Conditions | Yield |
---|---|
In tetrahydrofuran Irradiation (UV/VIS); N2-atmosphere; irradn. (λ > 525 nm, 1 min); detd. by IR spectroscopy; | 100% |
tetrachloromethane
Conditions | Yield |
---|---|
With triphenylphosphine In dichloromethane at 20℃; for 22h; Cooling with ice; | 100% |
With triphenylphosphine In dichloromethane at 20℃; for 22h; Cooling with ice; | 100% |
tetrachloromethane
Conditions | Yield |
---|---|
With triethylamine; triphenylphosphine In dichloromethane at 20℃; for 9h; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
With 2,2'-azobis(isobutyronitrile); tris[2-(methylamino)ethyl]amine; copper(l) chloride at 80℃; for 1h; Reagent/catalyst; Temperature; Autoclave; Inert atmosphere; | 99.6% |
With 1-ethyl-3-methylimidazol-3-ium ethyl sulfate; copper(l) iodide at 130℃; Product distribution / selectivity; | 95.7% |
With 1-ethyl-3-methylimidazol-3-ium ethyl sulfate; ferric(III) bromide at 130℃; Product distribution / selectivity; | 93.5% |
Conditions | Yield |
---|---|
With dodecane; [RuH(η5-[9-SMe2-7,8-C2B9H10])(PPh3)2] In toluene at 40℃; for 16h; Kharash addition; | 99% |
With N2[(RuCl2)2(1,3,5-iPr3C6H3)(tricyclohexylphosphine]2 In toluene at 40℃; for 2h; | 98% |
With NbCl3(N,N′-bis-(2,6-diisopropylphenyl)-1,4-diaza-2,3-dimethyl-1,3-butadiene) In benzene-d6 at 100℃; for 3h; Catalytic behavior; Kinetics; Mechanism; Reagent/catalyst; Solvent; Temperature; Inert atmosphere; Schlenk technique; Glovebox; | 97% |
tetrachloromethane
methacrylic acid methyl ester
methyl 2,4,4,4-tetrachloro-2-methylbutanoate
Conditions | Yield |
---|---|
With dodecane; [RuH(η5-[9-SEtPh-7,8-C2B9H10])(PPh3)2] In toluene at 40℃; for 16h; Kharash addition; | 99% |
With homobimetallic; ruthenium(II) In toluene at 85℃; for 8h; | 94% |
With dodecane; dichloro(3-phenyl-1H-indene-1-ylidene)(bistriphenylphosphine)ruthenium(II) In toluene at 80℃; for 17h; Product distribution; Further Variations:; Catalysts; atom transfer radical addition; | 94% |
tetrachloromethane
N-butyl-N-formyl-4-methyl-benzenesulfonamide
N-butyl-N-(2,2-dichlorovinyl)-4-methyl-benzenesulfonamide
Conditions | Yield |
---|---|
With triphenylphosphine In tetrahydrofuran at 60℃; for 1h; Condensation; Dichloromethylenation; | 99% |
With triphenylphosphine In tetrahydrofuran at 60℃; for 7h; Corey-Fuchs reaction; | 99% |
tetrachloromethane
dicarbonyl(η(5)-cyclopentadienyl)[2,4,6-tri(tert-butyl)-phenyl-λ(4)-phosphanediyl]molybdenum(II)
dicarbonyl(η(5)-cyclopentadienyl)([2,4,6-tri(tert-butyl)-phenyl](chloro)-λ(4)-phosphanediyl)molybdenum(II)
Conditions | Yield |
---|---|
In pentane byproducts: CHCl3; N2-atmosphere; stirring equimolar amts. (room temp., 3 d); solvent removal (vac.), washing (pentane), drying (vac.); elem. anal.; | 99% |
tetrachloromethane
(η(5);η(5)-fulvalene)W2(CO)4(P(C6H5)2CH3)2H2
cis,cis-(η(5):η(5)-fulvalene)W2(CO)4(P(C6H5)2CH3)2Cl2
Conditions | Yield |
---|---|
In dichloromethane inert atmosphere; excess of CCl4, stirring (room temp., 1 d; pptn.); vol. reduction (vac.), hexane addn., collection (filtration), washing (hexane), drying (reduced pressure); | 99% |
tetrachloromethane
(CO)RuC20N4H8[C6H3(CH3)2]4
RuCl2(5,10,15,20-tetrakis(2,6-dimethylphenyl)porphyrinato)
Conditions | Yield |
---|---|
In tetrachloromethane heating 2 h; | 99% |
tetrachloromethane
Conditions | Yield |
---|---|
In tetrachloromethane reaction of cyclic Si2GeSn-compd. with CCl4; | 99% |
Conditions | Yield |
---|---|
at 250℃; under 52505.3 Torr; for 7h; Inert atmosphere; | 99% |
1-benzofurane
methanol
tetrachloromethane
methyl benzofuran-2-carboxylate
Conditions | Yield |
---|---|
With iron(II) bromide at 160℃; for 4h; Inert atmosphere; sealed ampule; regioselective reaction; | 99% |
tetrachloromethane
[IrCl(PPh2(o-C6H4CO))2(NH2C6H11)]
Conditions | Yield |
---|---|
In tetrachloromethane (N2) suspn. Ir complex in CCl4 was refluxed for 1 h; solvent was evapd., residue was washed with Et2O and vac.-drieed; elem. anal.; | 99% |
Conditions | Yield |
---|---|
With triethylsilane at 70℃; for 72h; Catalytic behavior; | 99% |
tetrachloromethane
1,1,1-trifluoropropylene
1,1,1,3-tetrachloro-4,4,4-trifluorobutane
Conditions | Yield |
---|---|
With phosphoric acid tributyl ester; iron at 110℃; for 3h; | 98.5% |
With 2,2'-azobis(isobutyronitrile); 4-fluoroaniline; copper(I) bromide at 60℃; for 4h; Reagent/catalyst; Temperature; Autoclave; Inert atmosphere; | 94.2% |
iron(III) chloride; phosphoric acid tributyl ester; iron at 80 - 100℃; under 2311.54 Torr; | 90% |
Conditions | Yield |
---|---|
With iron; trimethyl orthoformate at 100℃; under 1500.15 Torr; for 1h; | 98.1% |
With iron(III) chloride; phosphoric acid tributyl ester; iron at 110℃; under 5931.67 Torr; Reagent/catalyst; Pressure; Flow reactor; Large scale; | 96% |
iron(III) chloride; triethyl phosphate; iron at 110 - 134℃; under 1875.19 - 6000.6 Torr; Autoclave; Inert atmosphere; | 91% |
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