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Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe

Phenylphosphonic dichloride

Cas:824-72-6

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality Dichlorophenylphosphine oxide supplier in China

Cas:824-72-6

Min.Order:1 Metric Ton

Negotiable

Type:Manufacturers

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Henan Allgreen Chemical Co.,Ltd

high quality Located in Zhengdong New District, Zhengzhou of Henan province, Henan Allgreen Chemical Co.,Ltd is comprehensive high-tech modern enterprises integrating professional R&D, production and sales. Strong technical force, with a long

Phenylphosphonic dichloride

Cas:824-72-6

Min.Order:1 Gram

Negotiable

Type:Manufacturers

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply Dichlorophenylphosphine oxide

Cas:824-72-6

Min.Order:1

Negotiable

Type:Other

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Chemwill Asia Co., Ltd.

Phenylphosphonic dichloride -- CHemwill

Cas:824-72-6

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Manufacturers

inquiry

Henan Sinotech Import&Export Corporation

Product Name: Phenylphosphonic dichloride Appearance: Colorless transparent liquid M.F.: C6H5Cl2OP M.W.: 194.98 CAS NO.: 824-72-6 EINECS NO.: 212-534-3 Appearance:Colorless liquid Storage: RT. Package: 25KG/drum,50KG/drum Application: Pharma

Phenylphosphonic dichloride CAS: 824-72-6

Cas:824-72-6

Min.Order:5 Metric Ton

FOB Price: $1.0 / 2.0

Type:Other

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

CAS NO.:824-72-6

Cas:824-72-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

Dichlorophenylphosphine oxide

Cas:824-72-6

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Phenylphosphonic dichloride

Cas:824-72-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Massive Chemical Technology Co., Ltd.

Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and

Phenylphosphonic dichloride/High quality/Best price

Cas:824-72-6

Min.Order:1 Gram

FOB Price: $1.0

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High quality Dichlorophenylphosphine oxide

Cas:824-72-6

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

Hunan chemfish Pharmaceutical co.,Ltd

Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea

Phenylphosphonic dichloride

Cas:824-72-6

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Hangzhou Dingyan Chem Co., Ltd

C-3955 Phenylphosphonic dichloride M.F:C6H5Cl2OPAppearance:Colorless clear liquid Package:250kg net/plastic drum

Phenylphosphonic dichloride

Cas:824-72-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

GIHI CHEMICALS CO.,LIMITED

high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,or Intermediates,fine chemicals Transportation:air,sea,courier

Phenylphosphonic dichloride

Cas:824-72-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Aecochem Corp.

Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS

Dichlorophenylphosphine oxide

Cas:824-72-6

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Enke Pharma-tech Co.,Ltd. (Cangzhou, China )

Cangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city?in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api,?intermediat

Phenylphosphonic dichloride

Cas:824-72-6

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Henan Tianfu Chemical Co., Ltd.

Appearance:powder Package:Aluminium foil bag

Phenylphosphonic dichloride

Cas:824-72-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard

factory supply CAS 824-72-6 with competitive price

Cas:824-72-6

Min.Order:1 Kilogram

FOB Price: $112.0

Type:Trading Company

inquiry

Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

Phenylphosphonic dichloride

Cas:824-72-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Xiamen AmoyChem Co.,Ltd

Amoychem is committed to providing the top-quality chemical products and services Internationally. We offer our customers with friendly, professional service and reliable, high performance products that have been manufactured according to the accredi

Phenylphosphonic?dichloride

Cas:824-72-6

Min.Order:0

Negotiable

Type:Other

inquiry

Hangzhou ZeErRui Chemical Co., Ltd.

Known for its best quality and competitve price, this chemicals we offered is widely appreciated by our customers. Prompt reaction, good quality and best service make us reliable and outstanding in this industry.Appearance:Clear yellow to brown liqui

Dichlorophenylphosphine oxide manufacture

Cas:824-72-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

SAGECHEM LIMITED

824-72-6 Application:intermediate

Phenylphosphonic dichloride

Cas:824-72-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hunan Russell Chemicals Technology Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China

Phenylphosphonic dichloride 824-72-6

Cas:824-72-6

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Chemsigma International Co.,Ltd.

bulk?production Application:Pharmaceutical intermediates

Phenylphosphonic dichloride

Cas:824-72-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Beantown Chemical

in stock Application:824-72-6

Phenylphosphonic dichloride, technical, 90%

Cas:824-72-6

Min.Order:0

Negotiable

Type:Trading Company

inquiry

HWRK Chem

in storeAppearance:Colorless liquid Package:100g Application:Organic Chemicals

Phenylphosphonic dichloride

Cas:824-72-6

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Amadis Chemical Co., Ltd.

1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G

Phenylphosphonic dichloride

Cas:824-72-6

Min.Order:10 Milligram

Negotiable

Type:Lab/Research institutions

inquiry

HENAN SUNLAKE ENTERPRISE CORPORATION

Phenylphosphonic dichloride Basic information Product Name: Phenylphosphonic dichloride Synonyms: Benzenephosphonicaciddichloride;Benzenephosphonyl chloride;phenyl-phosphonicdichlorid;Phenylphosphonodichl

Phenylphosphonic dichloride

Cas:824-72-6

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Chemtn Biological Technology Limited

Our company is a professional chemical raw materials manufacturer and exporter for many years in chemical market. There are more than 200 excellent staffs and four factories working for us . Company advantage: 1.Place of Origin in China with Su

Phenylphosphonic dichloride

Cas:824-72-6

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Watson International Ltd

Watson International Ltd' has a very strong R&D and technical capacity supported by FCAD's platform. The subsidiaries under FCAD Group have accumulated much know-how of different fine chemical branches. For example, Apnoke Scientific L

Phenylphosphonicdichloride

Cas:824-72-6

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Synthetic route

phenyltetrachlorophosphorane
4895-65-2

phenyltetrachlorophosphorane

P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

Conditions
ConditionsYield
With sodium dithionite In tetrachloromethane at 20℃; Substitution;96%
With water
With sulfur dioxide
Multi-step reaction with 2 steps
1: NEt3 / CH2Cl2 / 13 h / 40 °C
2: 38 percent Spectr. / NEt3 / toluene; CH2Cl2 / 4 h / 0 °C
View Scheme
With amino acid at 20 - 25℃;
phosphoric acid monophenyl ester
701-64-4

phosphoric acid monophenyl ester

P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

Conditions
ConditionsYield
With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane at 20 - 45℃; for 5h;96%
phenylphosphonate
1571-33-1

phenylphosphonate

P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

Conditions
ConditionsYield
With oxalyl dichloride In dichloromethane; N,N-dimethyl-formamide Heating;93%
With phosphorus pentachloride for 2h; Heating;91%
With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane at 20 - 40℃; for 1h;
diethyl phenylphosphonate
1754-49-0

diethyl phenylphosphonate

P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

Conditions
ConditionsYield
With thionyl chloride; N-Formylpiperidine for 20h; Heating;91.3%
Multi-step reaction with 2 steps
1: hydrogenchloride / 12 h / 100 °C
2: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 5 h / 20 - 45 °C
View Scheme
dimethyl phenylphosphonate
2240-41-7

dimethyl phenylphosphonate

P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

Conditions
ConditionsYield
With thionyl chloride In N,N-dimethyl-formamide at 120℃; for 4h;88.2%
oxalyl dichloride
79-37-8

oxalyl dichloride

dimethyl phenylphosphonate
2240-41-7

dimethyl phenylphosphonate

P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

Conditions
ConditionsYield
84%
Dichlorophenylphosphine
644-97-3

Dichlorophenylphosphine

P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

Conditions
ConditionsYield
With chlorine; iodine; iron(III) chloride In tetrachloromethane at 60 - 70℃; for 5h;82.5%
With air
With oxygen
phosgene
75-44-5

phosgene

phenylphosphonate
1571-33-1

phenylphosphonate

P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

Conditions
ConditionsYield
In chlorobenzene75%
With pyridine In chlorobenzene
phosgene
75-44-5

phosgene

diethyl phenylphosphonate
1754-49-0

diethyl phenylphosphonate

P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

Conditions
ConditionsYield
71%
phenyl-phosphonothioic acid
25331-57-1

phenyl-phosphonothioic acid

P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

Conditions
ConditionsYield
With pyridine; thionyl chloride for 4h; Heating;70%
diethyl phenylphosphonothioate
6231-03-4

diethyl phenylphosphonothioate

P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

Conditions
ConditionsYield
With pyridine; thionyl chloride for 4h; Heating;50%
triphenylphosphine
603-35-0

triphenylphosphine

P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

Conditions
ConditionsYield
With trichlorophosphate at 325℃; for 2h;31%
N,N'-Dimethylurea
96-31-1

N,N'-Dimethylurea

2,2-Dichlor-1,3-dimethyl-2-phenyl-2λ5-phosphetidin-4-on
131561-32-5

2,2-Dichlor-1,3-dimethyl-2-phenyl-2λ5-phosphetidin-4-on

A

P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

B

1,3 Dimethyl-2-phenyl-1,3,2-diazaphosphetidin-4-on-2-oxid
126695-50-9

1,3 Dimethyl-2-phenyl-1,3,2-diazaphosphetidin-4-on-2-oxid

C

1,3,5,7-Tetramethyl-4-phenyl-1,3,5,7-tetraaza-4λ5-phosphaspiro<3.3>heptan-2,6-dion
74411-89-5

1,3,5,7-Tetramethyl-4-phenyl-1,3,5,7-tetraaza-4λ5-phosphaspiro<3.3>heptan-2,6-dion

Conditions
ConditionsYield
With triethylamine In dichloromethane; toluene at 0℃; for 4h;A 38 % Spectr.
B 26 % Spectr.
C 6%
phenylphosphonate
1571-33-1

phenylphosphonate

phenyltetrachlorophosphorane
4895-65-2

phenyltetrachlorophosphorane

P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

phenylphosphinic acid
1779-48-2

phenylphosphinic acid

P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

Conditions
ConditionsYield
With phosphorus pentachloride unter Kuehlung;
phenyltetrachlorophosphorane
4895-65-2

phenyltetrachlorophosphorane

acetic acid
64-19-7

acetic acid

A

P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

B

acetyl chloride
75-36-5

acetyl chloride

benzene
71-43-2

benzene

P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

Conditions
ConditionsYield
With phosphorus pentoxide at 275℃; beim Erwaermen des Reaktionsprodukts mit PCl5 und POCl3;
N,N'-Dimethylurea
96-31-1

N,N'-Dimethylurea

phenyltetrachlorophosphorane
4895-65-2

phenyltetrachlorophosphorane

A

P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

B

2,2-Dichlor-1,3-dimethyl-2-phenyl-2λ5-phosphetidin-4-on
131561-32-5

2,2-Dichlor-1,3-dimethyl-2-phenyl-2λ5-phosphetidin-4-on

Conditions
ConditionsYield
With triethylamine In dichloromethane at 40℃; for 13h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
trichloro(2-ethoxyvinyl)phenylphosphorane
90876-60-1

trichloro(2-ethoxyvinyl)phenylphosphorane

A

P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

B

phenyl-β-ethoxyvinylphosphinic chloride
90876-11-2

phenyl-β-ethoxyvinylphosphinic chloride

C

(1-chloro-2-ethoxyvinyl)phenylphosphinic chloride

(1-chloro-2-ethoxyvinyl)phenylphosphinic chloride

D

(1,1,2-trichloro-2-ethoxyethyl)phenylphosphinic chloride

(1,1,2-trichloro-2-ethoxyethyl)phenylphosphinic chloride

Conditions
ConditionsYield
With sulfuryl dichloride In benzene at -3 - 0℃;
phenyltetrachlorophosphorane
4895-65-2

phenyltetrachlorophosphorane

A

P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

B

Dichlorophenylphosphine
644-97-3

Dichlorophenylphosphine

Conditions
ConditionsYield
With Diethyl phosphate In benzene for 1h; Product distribution; (C2H5O)2PONa;
C8H8Cl4NOP
135289-86-0

C8H8Cl4NOP

P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

Conditions
ConditionsYield
With sulfur dioxide In toluene at 0 - 5℃;14.2 g
C10H12Cl4NOP
135289-88-2

C10H12Cl4NOP

P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

Conditions
ConditionsYield
With sulfur dioxide In toluene at 0 - 5℃;15.9 g
C10H12Cl4NOP
135289-87-1

C10H12Cl4NOP

P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

Conditions
ConditionsYield
With sulfur dioxide In toluene at 0 - 5℃;9.9 g
Dichlorophenylphosphine
644-97-3

Dichlorophenylphosphine

oxygen

oxygen

P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

phenyltetrachlorophosphorane
4895-65-2

phenyltetrachlorophosphorane

sulfur dioxide

sulfur dioxide

A

P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

B

thionyl chloride
7719-09-7

thionyl chloride

P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

(S,S)-1,2-diphenyl-1,2-diaminoethane
29841-69-8

(S,S)-1,2-diphenyl-1,2-diaminoethane

(S3,S4)-1-phenyl-(3,4-diphenyl)diazaphospholidine 1-oxide

(S3,S4)-1-phenyl-(3,4-diphenyl)diazaphospholidine 1-oxide

P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

meso-1,2-bis(1-hydroxyethyl)benzene
53354-75-9

meso-1,2-bis(1-hydroxyethyl)benzene

meso-1,5-dimethyl-3-phenyl-1,5-dihydro-benzo[e][1,3,2]dioxa-phosphepine-3-oxide
679430-35-4

meso-1,5-dimethyl-3-phenyl-1,5-dihydro-benzo[e][1,3,2]dioxa-phosphepine-3-oxide

Conditions
ConditionsYield
With pyridine In dichloromethane at 0℃; for 1h;100%
P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

(-)-menthol
2216-51-5

(-)-menthol

A

(1R,2S,5R)-5-methyl-2-(propan-2-yl)cyclohexyl phenylphosphinate
31352-60-0, 31352-61-1, 54353-18-3

(1R,2S,5R)-5-methyl-2-(propan-2-yl)cyclohexyl phenylphosphinate

B

(-)-menthyl chloride

(-)-menthyl chloride

Conditions
ConditionsYield
In dichloromethane at 20℃; for 12h;A 99.6%
B n/a
P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

ethanol
64-17-5

ethanol

diethyl phenylphosphonate
1754-49-0

diethyl phenylphosphonate

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃; for 1h; Substitution;99%
With triethylamine In diethyl ether at 0 - 20℃; Inert atmosphere; Schlenk technique;97%
With pyridine In diethyl ether for 6h; Ambient temperature;92%
With pyridine
P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

allyl alcohol
107-18-6

allyl alcohol

phenylphosphonic acid diallyl ester
2948-89-2

phenylphosphonic acid diallyl ester

Conditions
ConditionsYield
With dmap; triethylamine In dichloromethane at 0 - 20℃; Substitution;98%
With pyridine at 2 - 5℃; for 6h;97.7%
With pyridine In benzene Ambient temperature;65%
With pyridine
P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

tert-butylamine
75-64-9

tert-butylamine

N,N'-Di-tert-butyl-P-phenylphosphonyldiamid
15916-99-1

N,N'-Di-tert-butyl-P-phenylphosphonyldiamid

Conditions
ConditionsYield
In neat (no solvent) at 20℃; for 0.166667h; Sonication; Green chemistry;98%
In acetonitrile for 3h; Heating;64%
In acetonitrile Cooling with ice;64%
P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

propylamine
107-10-8

propylamine

bis(propylamino)phenylphosphine oxide
14360-80-6

bis(propylamino)phenylphosphine oxide

Conditions
ConditionsYield
In neat (no solvent) at 20℃; for 0.0833333h; Sonication; Green chemistry;98%
P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

trimethyl ammonium 8,8'-dihydroxy-bis(1,2-dicarbollido)-3-cobalt(1-)ate

trimethyl ammonium 8,8'-dihydroxy-bis(1,2-dicarbollido)-3-cobalt(1-)ate

potassium hydroxide

potassium hydroxide

[8,8'-μ-PhP(O)(O)2<(1,2-C2B9H10)2-3,3'-Co]K

[8,8'-μ-PhP(O)(O)2<(1,2-C2B9H10)2-3,3'-Co]K

Conditions
ConditionsYield
With triethylamine In chloroform to soln. Et3N in CHCl3 PhPOCl2 was added followed by suspn. cobaltcarborane in CHCl3 and stirred for 1 h at 80°C., soln. was cooled , water was added and stirred for 4 h at room temp., chloroform layer was separated and evapd.,; residue was dissolved in soln. KOH in aq. EtOH, organics were evapd., EtOH was added and heated to 80°C followed by cooling;97.5%
P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

N-butylamine
109-73-9

N-butylamine

P-phenyl-N,N'-di-n-butylphosphonic diamide
14360-81-7

P-phenyl-N,N'-di-n-butylphosphonic diamide

Conditions
ConditionsYield
In neat (no solvent) at 20℃; for 0.0833333h; Sonication; Green chemistry;97%
In diethyl ether for 0.5h; Ambient temperature;41%
P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

cyclohexylamine
108-91-8

cyclohexylamine

Bis(cyclohexylamino)phenylphosphine oxide
14612-96-5

Bis(cyclohexylamino)phenylphosphine oxide

Conditions
ConditionsYield
In neat (no solvent) at 20℃; for 0.0833333h; Sonication; Green chemistry;97%
In acetonitrile at 0℃; for 24h;60%
P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

1-(3-bromophenyl)-pyrrolidine
219928-13-9

1-(3-bromophenyl)-pyrrolidine

phenylbis(3-(pyrrolidin-1-yl)phenyl)phosphine oxide

phenylbis(3-(pyrrolidin-1-yl)phenyl)phosphine oxide

Conditions
ConditionsYield
Stage #1: 1-(3-bromophenyl)-pyrrolidine With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 1h; Inert atmosphere;
Stage #2: P,P-dichlorophenylphosphine oxide In tetrahydrofuran; hexane at -78℃; for 1h; Inert atmosphere;
97%
P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

diphenylamine
122-39-4

diphenylamine

bis(diphenylamino)phenylphosphine oxide
107822-55-9

bis(diphenylamino)phenylphosphine oxide

Conditions
ConditionsYield
In neat (no solvent) at 20℃; for 0.25h; Sonication; Green chemistry;97%
P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

1,2-diamino-benzene
95-54-5

1,2-diamino-benzene

1,3-dihydro-2-phenyl-1,3,2-benzodiazaphosphole-2-oxide
7597-43-5

1,3-dihydro-2-phenyl-1,3,2-benzodiazaphosphole-2-oxide

Conditions
ConditionsYield
In various solvent(s) at 135℃;96.8%
In various solvent(s) at 135℃; other diamines, other phophonates;96.8%
With bromobenzene Heating;
piperazine
110-85-0

piperazine

P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

phenylbis(1-piperazinyl)phosphine oxide

phenylbis(1-piperazinyl)phosphine oxide

Conditions
ConditionsYield
With triethylamine In chloroform at -5 - 25℃; for 2.5h; Inert atmosphere;96.5%
P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

1-methyl-1-sila-2,6,7-trioxa-4-hydroxymethylbicyclo[2,2,2]octyl

1-methyl-1-sila-2,6,7-trioxa-4-hydroxymethylbicyclo[2,2,2]octyl

C18H27O9PSi2

C18H27O9PSi2

Conditions
ConditionsYield
In 1,1,2,2-tetrachloroethane at 35 - 120℃; for 7h; Temperature; Inert atmosphere;96.1%
P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

2,2-dimethyl-3-(methylamino)propan-1-ol
16047-86-2

2,2-dimethyl-3-(methylamino)propan-1-ol

3,5,5-Trimethyl-2-phenyl-[1,3,2]oxazaphosphinane 2-oxide

3,5,5-Trimethyl-2-phenyl-[1,3,2]oxazaphosphinane 2-oxide

Conditions
ConditionsYield
With triethylamine In benzene for 20h; Ambient temperature;96%
P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

butan-1-ol
71-36-3

butan-1-ol

Phenylphosphonsaeure-n-butylesterfluorid
2062-48-8

Phenylphosphonsaeure-n-butylesterfluorid

Conditions
ConditionsYield
With sodium fluoride In acetonitrile for 1h; Heating;96%
P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

para-tert-butylphenol
98-54-4

para-tert-butylphenol

bis(4-tert-butylphenyl) phenylphosphonate
89410-43-5

bis(4-tert-butylphenyl) phenylphosphonate

Conditions
ConditionsYield
With pyridine at 140℃; for 20h;96%
P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

Mesitol
527-60-6

Mesitol

bis(2,4,6-trimethylphenyl) phenylphosphonate
1160309-46-5

bis(2,4,6-trimethylphenyl) phenylphosphonate

Conditions
ConditionsYield
With pyridine at 140℃; for 20h;96%
P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

1,1-dimethyl-1-sila-2,6-dioxa-4-oxy-4-phospha-4-hydroxymethylcyclohexane

1,1-dimethyl-1-sila-2,6-dioxa-4-oxy-4-phospha-4-hydroxymethylcyclohexane

C16H29O9P3Si2

C16H29O9P3Si2

Conditions
ConditionsYield
With pyridine In diethylene glycol dimethyl ether at 30 - 140℃; for 11h; Temperature; Solvent; Reagent/catalyst;95.6%
P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

2,4,6-tribromophenol
118-79-6

2,4,6-tribromophenol

C18H9Br6O3P

C18H9Br6O3P

Conditions
ConditionsYield
With ammonia In chloroform at 55℃; for 2h; Temperature; Concentration; Solvent; Reagent/catalyst; Inert atmosphere; Sealed tube;95.3%
P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

tri(hydroxymethyl)phosphine oxide
1067-12-5

tri(hydroxymethyl)phosphine oxide

C9H12O5P2

C9H12O5P2

Conditions
ConditionsYield
In 5,5-dimethyl-1,3-cyclohexadiene at 20 - 140℃; for 6h; Solvent; Temperature;95.3%
P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

di-sec-butyl phenylphosphonate
2783-48-4

di-sec-butyl phenylphosphonate

Conditions
ConditionsYield
With pyridine In benzene Ambient temperature;95%
With pyridine
P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

rac-octan-2-ol
4128-31-8

rac-octan-2-ol

di-2-octyl phenylphosphonate
107465-90-7

di-2-octyl phenylphosphonate

Conditions
ConditionsYield
With pyridine In benzene Ambient temperature;95%
P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

benzylamine
100-46-9

benzylamine

bis(benzylamino)phenylphosphine oxide
53721-41-8

bis(benzylamino)phenylphosphine oxide

Conditions
ConditionsYield
In neat (no solvent) at 20℃; for 0.0833333h; Sonication; Green chemistry;95%
In tetrahydrofuran for 4h; Ambient temperature;83%
With pyridine at 70℃; for 4.5h;82%
In diethyl ether at 0 - 20℃; for 2h;59%
P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

(R,R)-N,N'-dimethyl-1,2-diaminocyclohexane
68737-65-5

(R,R)-N,N'-dimethyl-1,2-diaminocyclohexane

(R3a,R7a)-(1,3-dimethyl)-2-phenyl-2,3,3a,4,5,6,7,7a-octahydro-1H-1,3,2-benzodiazaphosphole 2-oxide
184535-50-0

(R3a,R7a)-(1,3-dimethyl)-2-phenyl-2,3,3a,4,5,6,7,7a-octahydro-1H-1,3,2-benzodiazaphosphole 2-oxide

Conditions
ConditionsYield
With triethylamine In benzene for 1.5h; Ambient temperature;95%
P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

(tert-butyldimethylsilyl)acetylene
86318-61-8

(tert-butyldimethylsilyl)acetylene

bis(2-(tert-butyldimethylsilyl)-1-ethynyl)(phenyl)phosphine oxide

bis(2-(tert-butyldimethylsilyl)-1-ethynyl)(phenyl)phosphine oxide

Conditions
ConditionsYield
Stage #1: (tert-butyldimethylsilyl)acetylene With n-butyllithium In tetrahydrofuran; hexane at -75 - -55℃; for 0.416667h; Inert atmosphere;
Stage #2: P,P-dichlorophenylphosphine oxide In tetrahydrofuran; hexane at -70 - 20℃; for 1.95h; Inert atmosphere;
95%
2-bromo-N-(furan-2-ylmethyl)prop-2-en-1-amine
448905-30-4

2-bromo-N-(furan-2-ylmethyl)prop-2-en-1-amine

P,P-dichlorophenylphosphine oxide
824-72-6

P,P-dichlorophenylphosphine oxide

N-(2-bromoallyl)-N-(furan-2-ylmethyl)-P-phenyl phosphonamidic chloride

N-(2-bromoallyl)-N-(furan-2-ylmethyl)-P-phenyl phosphonamidic chloride

Conditions
ConditionsYield
With dmap In dichloromethane at 0 - 20℃; for 2h;95%

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