As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for the fine c
Cas:122-39-4
Min.Order:1 Kilogram
FOB Price: $14.0 / 15.0
Type:Lab/Research institutions
inquiryItems Standard Test Result Appearance White flake White flake Diphenylamine 152.0~156.0℃
Cas:122-39-4
Min.Order:1 Gram
FOB Price: $100.0 / 500.0
Type:Manufacturers
inquiryProduct description: Product name Diphenylamine CAS number 122-39-4 Assay ≥99.6% Appearance White flake Capacity 2000mt/year Application Rubber antioxidant, dye, pharmaceutic
Cas:122-39-4
Min.Order:100 Gram
FOB Price: $12.0
Type:Lab/Research institutions
inquiryhebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm
ISO 9001 certificate Good quality Competitive price On time delivery 1.high purity 99.7% 2.use for synthesize rubber antiager, dye, medicine intermediate, lubricating oil antioxidant 3.SGS,MSDS Diphenylamine(DPA) CAS NO.
Cas:122-39-4
Min.Order:1 Metric Ton
Negotiable
Type:Trading Company
inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Good quantity Diphenylamine Basic information Product Name: Diphenylamine Synonyms: (phenylamino)-benzen;Aniline, N-phenyl-;anilino-benzen;Benzenamine, N-phenyl-;Benzenamine,N-phenyl-;
Cas:122-39-4
Min.Order:1 Metric Ton
Negotiable
Type:Lab/Research institutions
inquirySynonyms: (phenylamino)-benzen;Aniline, N-phenyl-;anilino-benzen;Benzenamine, N-phenyl-;Benzenamine,N-phenyl-;Benzene, (phenylamino)-;Benzene, anilino-;Big Dipper CAS: 122-39-4 MF: C12H11N MW: 169.22 EINECS: 204-539-4 Product Categories: Inter
Cas:122-39-4
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present
Cas:122-39-4
Min.Order:1 Kilogram
FOB Price: $35.0 / 50.0
Type:Trading Company
inquiryMinimum Order Qty. 10 Gram Supply Ability 500 Kilograms/Month Storage store in cool, dry, ventilated place 20℃ Delivery Time 3 business days after payment Payment Term TT,western union,Paypal,MoneyGram Package 10g,20g,50g,100g,500g,1KGS,
Cas:122-39-4
Min.Order:10 Gram
Negotiable
Type:Trading Company
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
N-phenylaniline C12H11N 122-39-4 99.5% Appearance:White powder Application:Analytical reagent, REDOX indicator and liquid desiccant, synthesis of organic dyes
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Superior quality, moderate price & quick delivery. Appearance:white crystal powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum, or as per your request. Application:Used as Pharmaceutical Intermed
Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:122-39-4
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryWe are leading fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...)
Cas:122-39-4
Min.Order:1 Kilogram
FOB Price: $5.0
Type:Lab/Research institutions
inquiryLocated in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service an
SAGECHEM is a chemical R&D, manufacturing and distribution company in China since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and etc. We also offer a full range of services in custom synthe
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,or Intermediates,fine chemicals Transportation:air,sea,courier
1.High quality : the purity is 99% min . through multiple producing procedures. 2.Competitive price : low price because of our skilled production technolpgy ,save the production cost at most , and give big profit room to our customers233.Safe and fa
high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
Hunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as
Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
Cas:122-39-4
Min.Order:1 Kilogram
FOB Price: $112.0
Type:Trading Company
inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
Amoychem is committed to providing the top-quality chemical products and services Internationally. We offer our customers with friendly, professional service and reliable, high performance products that have been manufactured according to the accredi
Diphenylamine 99.5% 122-39-4 Application:Diphenylamine 99.5% 122-39-4
Xiamen Luyunjia Trading Co.,Ltd Package:1kg/bag; 2644kg/drum, or as customer's request. Application:Xiamen Luyunjia Trading Co.,Ltd Transportation:DHL, EMS, FedEx, TNT, AIR, SEA Port:Beijing,Shanghai,Guangzhou ,China main port
Conditions | Yield |
---|---|
With sodium t-butanolate; tri tert-butylphosphoniumtetrafluoroborate; Pd{dba(OMe)}2 In toluene at 25℃; for 0.166667h; Buchwald-Hartwig cross coupling reaction; | 100% |
With potassium ethoxide In 1,4-dioxane at 200℃; Catalytic behavior; Buchwald-Hartwig Coupling; | 100% |
With C31H26N4PPdS(1+)*Cl(1-); sodium t-butanolate In toluene at 95℃; for 14h; Catalytic behavior; | 100% |
Conditions | Yield |
---|---|
palladium-carbon In diethylene glycol dimethyl ether; water; nitrobenzene; benzene | 100% |
palladium-carbon In water; nitrobenzene; benzene | 100% |
palladium-carbon In diethylene glycol dimethyl ether; water; nitrobenzene; benzene | 100% |
Conditions | Yield |
---|---|
With tetra(n-butyl)ammonium hydroxide In tetrahydrofuran; water for 0.166667h; Ambient temperature; | 100% |
With potassium phosphate; C29H55FeNOP2; hydrogen In tetrahydrofuran at 110℃; under 15001.5 Torr; for 3h; Catalytic behavior; | 99% |
With C18H37ClMoNO2P2; hydrogen; sodium triethylborohydride In tetrahydrofuran; toluene at 100℃; under 37503.8 Torr; for 24h; Autoclave; Glovebox; | 86% |
With [bis({2‐[bis(propan‐2‐yl)phosphanyl]ethyl})amide](carbonyl)(hydride)iron(II); hydrogen In tetrahydrofuran at 100℃; under 22801.5 Torr; for 4h; Catalytic behavior; |
Conditions | Yield |
---|---|
[1,3-{bis-N-(N-methylimidazolylidene)methyl}-5-methylbenzenecopper dibromide]; caesium carbonate at 170℃; for 12h; Conversion of starting material; | 100% |
[(N,N-dipyridyl-imidazolylidene)copper dibromide]; caesium carbonate at 170℃; for 12h; Conversion of starting material; | 100% |
With C31H26N4PPdS(1+)*Cl(1-); sodium t-butanolate In toluene at 95℃; for 10h; Catalytic behavior; | 100% |
Conditions | Yield |
---|---|
With 2,6-dimethylpyridine; fac-tris(2-phenylpyridinato-N,C2')iridium(III); copper diacetate; n-tetradecanoic acid In toluene; acetonitrile at 35℃; for 20h; Chan-Lam Coupling; Irradiation; | 100% |
With copper diacetate; potassium carbonate; benzoic acid In ethyl acetate at 80℃; for 4h; air; | 98% |
With potassium carbonate In water at 20℃; Reagent/catalyst; Solvent; | 95% |
diphenylamine
Conditions | Yield |
---|---|
With aminomethyl resin-supported N-propylbarbituric acid; tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran at 20℃; for 1h; | 100% |
Conditions | Yield |
---|---|
palladium-carbon In diethylene glycol dimethyl ether; water; nitrobenzene; benzene | 100% |
palladium-carbon In diethylene glycol dimethyl ether; water; nitrobenzene; benzene | 100% |
palladium-carbon In water; nitrobenzene; benzene | 99.4% |
palladium-carbon In water; nitrobenzene; benzene | 99.4% |
1-tert-butyl-1,1-dimethyl-N,N-diphenylsilanamine
diphenylamine
Conditions | Yield |
---|---|
With silica gel In ethanol; water at 20℃; for 2h; | 100% |
Conditions | Yield |
---|---|
Stage #1: aniline With n-butyllithium; dichloro(N,N,N’,N‘-tetramethylethylenediamine)zinc In tetrahydrofuran; hexane at 0 - 20℃; for 0.5h; Inert atmosphere; Schlenk technique; Stage #2: phenylmagnesium bromide With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; bis(acetylacetonate)nickel(II); 1,2-dichloro-2-methylpropane In tetrahydrofuran; hexane at 0 - 20℃; for 3h; Inert atmosphere; Schlenk technique; | A n/a B 100% |
Conditions | Yield |
---|---|
With sodium t-butanolate; 1,3-bis[2,6-diisopropylphenyl]imidazolium chloride; Ni(PPh3)2(1-(p-acetylnaphthyl))Cl In 1,4-dioxane at 100℃; | 99% |
With bis(η3-allyl-μ-chloropalladium(II)); potassium tert-butylate; 1,3-bis[(2,6-diisopropyl)phenyl]imidazolinium chloride In 1,4-dioxane at 100℃; for 1.5h; Inert atmosphere; | 99% |
With sodium t-butanolate In toluene at 110℃; Inert atmosphere; Glovebox; chemoselective reaction; | 99% |
Conditions | Yield |
---|---|
copper In dichloromethane for 0.5h; Ambient temperature; | 99% |
Conditions | Yield |
---|---|
With (1,3-bis(2,6-diisopropylphenyl)imidazolidene)Ni(styrene)2; lithium tert-butoxide In 1,4-dioxane for 10h; Inert atmosphere; Heating; Schlenk technique; | 99% |
With potassium hydroxide; [(N,N-dimethylbenzylamine)(trifluoroacetato)palladium(II)]2; XPhos In water at 80℃; for 16h; | 91% |
With di-tert-butyl{2′-isopropoxy-[1,1′-binaphthalen]-2-yl}phosphane; potassium phosphate; palladium diacetate; phenylboronic acid In butan-1-ol at 110℃; for 2h; Inert atmosphere; | 99 %Chromat. |
Conditions | Yield |
---|---|
With potassium phosphate; C29H55FeNOP2; hydrogen In tetrahydrofuran at 130℃; under 37503.8 Torr; for 3h; Catalytic behavior; | 99% |
With triethyl borane; sodium hydroxide In tert-butyl methyl ether at 80℃; for 6h; Inert atmosphere; Sealed tube; | 78% |
Stage #1: N,N-diphenylbenzamide With Triethoxysilane; sodium triethylborohydride In tert-butyl methyl ether at 80℃; for 6h; Stage #2: With hydrogenchloride In tert-butyl methyl ether; water at 20℃; for 1h; chemoselective reaction; | 73% |
Multi-step reaction with 2 steps 1: potassium hydroxide; triethyl borane / tetrahydrofuran / 24 h / 100 °C / Inert atmosphere; Schlenk technique; Sealed tube 2: sodium hydroxide; water / tetrahydrofuran / 1 h / 25 °C / Inert atmosphere; Schlenk technique; Sealed tube View Scheme |
Conditions | Yield |
---|---|
With 3-Hydroxy-1-methylpiperidine; nickel diacetate; sodium hydride In tetrahydrofuran at 65℃; for 4h; | 98% |
With sodium tetrahydroborate; nickel dichloride In tetrahydrofuran; methanol for 1h; Mechanism; Ambient temperature; kinetic isotope effect; desulfurization of other benzo- and dibenzothiophenes; | 68% |
bei der Zinkstaub-Destillation; |
diphenylamine
Conditions | Yield |
---|---|
With Triethylgermyl-natrium In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide at 60℃; for 68h; | 98% |
Conditions | Yield |
---|---|
With C46H27F24FeNiP2(1+)*CF3O3S(1-); triethylamine In 2-methyltetrahydrofuran at 100℃; for 16h; Solvent; Reagent/catalyst; Inert atmosphere; Schlenk technique; Glovebox; Sealed tube; | 98% |
With [(2,6-bis(2,4,6-triisopropylphenyl)phenyl)dicyclohexylphosphine](allyl-η3)palladium(II) chloride; potassium hydrogencarbonate In dodecane; tert-butyl alcohol at 100℃; for 12h; Inert atmosphere; Sealed tube; | 92% |
With caesium carbonate; palladium diacetate In toluene at 100℃; for 10h; | |
With palladium diacetate; caesium carbonate; XPhos In toluene at 100℃; for 1.5h; | |
With XPhos; palladium diacetate; caesium carbonate In toluene at 20 - 100℃; Inert atmosphere; |
Conditions | Yield |
---|---|
With aniline; sodium t-butanolate; Pd(dba)2 In chlorobenzene; toluene | 98% |
Conditions | Yield |
---|---|
With palladium on activated carbon; ammonium formate; lithium hydroxide In m-xylene at 160℃; for 24h; Catalytic behavior; Reagent/catalyst; Solvent; Temperature; Schlenk technique; Inert atmosphere; | 98% |
Multi-step reaction with 2 steps 1: Inert atmosphere 2: bis(1,5-cyclooctadiene)nickel(0); sodium t-butanolate; 1,3-bis[2,6-diisopropylphenyl]imidazolium chloride / 1,4-dioxane / 3 h / 80 °C / Inert atmosphere View Scheme | |
With ammonium formate In 1,3,5-trimethyl-benzene at 140℃; under 760.051 Torr; Reagent/catalyst; Solvent; Temperature; Inert atmosphere; | 73 %Chromat. |
Conditions | Yield |
---|---|
With L-arginine; potassium hydroxide In water at 80℃; under 760.051 Torr; for 2h; Reagent/catalyst; Solvent; Temperature; Green chemistry; | 98% |
With potassium phosphate; copper(l) iodide; lithium amide In N,N-dimethyl-formamide at 130℃; for 24h; Inert atmosphere; chemoselective reaction; | 90% |
Multi-step reaction with 2 steps 1: ammonia / water / 16 h / 75 °C / Ionic liquid 2: Cu2O nanoparticles (Cu2O-NPs) synthesized in n-Bu4POAc from CuCO3 / 16 h / 75 °C / Ionic liquid View Scheme |
N-carbobenzyloxydiphenylamine
diphenylamine
Conditions | Yield |
---|---|
With N1,N1,N12,N12-tetramethyl-7,8-dihydro-6H-dipyrido[1,2-a:2,1'-c][1,4]diazepine-2,12-diamine In N,N-dimethyl-formamide for 72h; Inert atmosphere; Glovebox; UV-irradiation; | 98% |
Conditions | Yield |
---|---|
With potassium phosphate; bis[chloro(1,2,3-trihapto-allylbenzene)palladium(II)]; N-[2-(di(1-adamantyl)phosphino)phenyl]morpholine In 1,4-dioxane; tert-butyl alcohol at 110℃; Buchwald-Hartwig Coupling; Inert atmosphere; Glovebox; chemoselective reaction; | 98% |
Conditions | Yield |
---|---|
With sodium t-butanolate In ethylene glycol at 100℃; for 12h; | 97% |
With 1,1'-bis-(diphenylphosphino)ferrocene; bis(1,5-cyclooctadiene)nickel(0); sodium t-butanolate In toluene at 20 - 105℃; Inert atmosphere; | 94% |
With bis(1,5-cyclooctadiene)nickel(0); sodium t-butanolate; 1,3-bis[2,6-diisopropylphenyl]imidazolium chloride In 1,4-dioxane at 80℃; for 3h; Inert atmosphere; | 77% |
With sodium t-butanolate; bis(1,5-cyclooctadiene)nickel (0); 1,3-bis[(2,6-diisopropyl)phenyl]imidazolinium chloride In 1,4-dioxane at 80℃; for 3h; Inert atmosphere; | 77% |
With (1,2-dimethoxyethane)dichloronickel(II); 2-phenyl-4,4,5,5-tetramethyl-1,3,2-dioxoborole; sodium t-butanolate; 1,3-bis[(2,6-diisopropyl)phenyl]imidazolinium chloride In 1,4-dioxane at 23 - 80℃; for 4h; Inert atmosphere; | 63% |
Conditions | Yield |
---|---|
With triethylamine at 95℃; Catalytic behavior; Reagent/catalyst; Temperature; | 97% |
With triethylamine at 90℃; for 12h; Reagent/catalyst; Temperature; Stille Cross Coupling; | 96% |
With triethylamine at 20℃; for 15h; Catalytic behavior; Temperature; | 95% |
With copper diacetate; triethylamine at 20℃; for 24h; | 94% |
Conditions | Yield |
---|---|
With potassium phosphate; C29H55FeNOP2; hydrogen In tetrahydrofuran at 110℃; under 22502.3 Torr; for 3h; Catalytic behavior; | 96% |
With triethyl borane; sodium hydroxide In tert-butyl methyl ether at 80℃; for 6h; Inert atmosphere; Sealed tube; | 89% |
Stage #1: N,N-diphenylacetamide With Triethoxysilane; sodium triethylborohydride In tert-butyl methyl ether at 80℃; for 6h; Stage #2: With hydrogenchloride In tert-butyl methyl ether; water at 20℃; for 1h; chemoselective reaction; | 83% |
Conditions | Yield |
---|---|
copper In dichloromethane for 2h; Ambient temperature; | 96% |
With copper(II) dipivaloate In dichloromethane for 0.0833333h; Ambient temperature; | 100 % Chromat. |
N,N-diphenylpyridine-2-sulfonamide
diphenylamine
Conditions | Yield |
---|---|
With magnesium In methanol at 0℃; for 1h; | 96% |
Conditions | Yield |
---|---|
With [2,2]bipyridinyl; potassium tert-butylate; copper(l) iodide In toluene at 115℃; for 3.5h; Product distribution; Further Variations:; Reagents; | A 95% B 2% |
With copper at 180℃; for 12h; | A 46% B 31% |
With copper(l) iodide; cesium fluoride In dimethyl sulfoxide at 130℃; for 24h; Ullmann Condensation; Inert atmosphere; Glovebox; | A 12% B 39 %Chromat. |
With potassium tert-butylate; copper(l) iodide; tributylphosphine In toluene at 110℃; for 3.5h; Product distribution; Further Variations:; Catalysts; high pressure; |
Conditions | Yield |
---|---|
With hydrogen In toluene at 160℃; under 45004.5 Torr; for 15h; Catalytic behavior; Autoclave; | A 89 %Chromat. B 95% |
With cis-[Ru(CH3CN)2(η3-C3H5)(CO1,5-cyclooctadiene)]BF4; hydrogen; potassium hexamethylsilazane; (2-aminoethyl)diphenylphosphane In tetrahydrofuran at 100℃; under 38002.6 Torr; for 24h; Autoclave; | |
With {Ru(H)(BH4)(CO)(3-(di-tert-butylphosphino)-N-((1-methyl-1H-imidazol-2-yl)methyl)propylamine)}; hydrogen In isopropyl alcohol at 120℃; under 22502.3 Torr; for 18h; Autoclave; | A 96 %Chromat. B 96 %Chromat. |
With C16H25MnN3O3P(1+)*Br(1-); potassium tert-butylate; hydrogen In cyclohexane at 100℃; under 22502.3 Torr; for 16h; Inert atmosphere; Autoclave; | A 80 %Chromat. B 82 %Chromat. |
Conditions | Yield |
---|---|
With hydrogen; sodium methylate; [carbonylchlorohydrido{bis[2-(diphenylphosphinomethyl)ethyl]amino}ethylamino] ruthenium(II) In methanol at 100℃; under 37503.8 Torr; for 16h; Autoclave; | A 77% B 95% |
Conditions | Yield |
---|---|
With trimethylamine Ambient temperature; | 100% |
With magnesium carbonate In water; acetonitrile for 288h; Heating; | 54% |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 20℃; for 0.333333h; | 100% |
In toluene at 90℃; for 4h; Inert atmosphere; | 99% |
In N,N-dimethyl-formamide at 80℃; for 2h; | 97% |
diphenylamine
bis(4-bromophenyl)amine
Conditions | Yield |
---|---|
With N-Bromosuccinimide Bromination; | 100% |
With N-Bromosuccinimide In N,N-dimethyl-formamide at 0℃; for 6h; Inert atmosphere; | 100% |
With tetra-N-butylammonium tribromide In chloroform for 0.0333333h; Ambient temperature; | 99% |
diphenylamine
N-nitrosodiphenylamine
Conditions | Yield |
---|---|
With oxalic acid; sodium nitrite In dichloromethane for 5h; Ambient temperature; | 100% |
With [NO(1+)*18-crown-6*H(NO3)2(1-)] In dichloromethane at 20℃; for 0.0833333h; | 100% |
With sodium azide In water; acetonitrile at 20℃; | 100% |
Conditions | Yield |
---|---|
With lithium derivative In water; toluene; benzene for 2h; | 100% |
Stage #1: diphenylamine With Lithium dimsyl In tetrahydrofuran at 0℃; for 0.5h; Stage #2: carbon disulfide In tetrahydrofuran at 0 - 20℃; for 12h; Reagent/catalyst; | 98% |
With n-butyllithium 1) hexane, -78 deg C to RT, 2) -78 deg C to RT; Multistep reaction; | |
Stage #1: diphenylamine With n-butyllithium In tetrahydrofuran at 0 - 20℃; for 0.5h; Stage #2: carbon disulfide In tetrahydrofuran at 0 - 12℃; for 12h; | |
Stage #1: diphenylamine With n-butyllithium In tetrahydrofuran at 0℃; for 0.5h; Stage #2: carbon disulfide In tetrahydrofuran at 0 - 20℃; for 12h; |
pentafluorosulfanyl isocyanate
diphenylamine
N'-(Pentafluorosulfanyl)-N,N-diphenylurea
Conditions | Yield |
---|---|
In chloroform | 100% |
diphenylamine
diphenylamine; deprotonated form
Conditions | Yield |
---|---|
With NaH-cryptand<2.2.1> In tetrahydrofuran for 0.166667h; | 100% |
1-bromo-4-tert-butylbenzene
diphenylamine
N,N-diphenyl-N-(4-tert-butylphenyl)amine
Conditions | Yield |
---|---|
With bis(tri-t-butylphosphine)palladium(0); potassium tert-butylate In toluene at 20℃; for 4h; | 100% |
With palladium diacetate; P(i-BuNCH2CH2)3N; sodium t-butanolate In toluene at 80℃; | 96% |
for 3h; | 96% |
diphenylamine
diphenyl acetylene
((E)-1,2-Diphenyl-vinyl)-diphenyl-amine
Conditions | Yield |
---|---|
phosphazene base-P4-tert-butyl In hexane; dimethyl sulfoxide at 120℃; for 24h; | 100% |
Conditions | Yield |
---|---|
With sodium t-butanolate; tris(dibenzylideneacetone)dipalladium (0); P(i-BuNCH2CH2)3N In toluene at 100℃; for 20h; Buchwald-Hartwig amination; | 100% |
With palladium diacetate; sodium t-butanolate; ruphos In neat (no solvent) at 110℃; for 12h; Buchwald-Hartwig Coupling; Green chemistry; | 99% |
With (1,3-bis(2,6-diisopropylphenyl)-3,4,5,6-tetrahydropyrimidin-2-ylidene)Pd(cinnamyl, 3-phenylallyl)Cl; sodium t-butanolate In neat (no solvent) at 110℃; for 12h; Buchwald-Hartwig Coupling; Inert atmosphere; Green chemistry; | 99% |
Conditions | Yield |
---|---|
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; palladium 10% on activated carbon; sodium t-butanolate In 1,3,5-trimethyl-benzene for 24h; Inert atmosphere; Reflux; | 100% |
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In toluene at 80℃; | 90.7% |
With tris-(dibenzylideneacetone)dipalladium(0); johnphos; sodium t-butanolate In toluene at 100℃; for 24h; Buchwald-Hartwig Coupling; Sealed tube; Inert atmosphere; | 79% |
Conditions | Yield |
---|---|
With tetra-(n-butyl)ammonium iodide; potassium carbonate In acetonitrile Reflux; | 100% |
With tetra-(n-butyl)ammonium iodide; potassium carbonate In acetonitrile Reflux; | 100% |
With tetra-(n-butyl)ammonium iodide; potassium carbonate In acetonitrile at 110℃; Inert atmosphere; | 81% |
(chloromethyl)methoxydimethylsilane
diphenylamine
Conditions | Yield |
---|---|
In toluene at 80℃; for 2h; | 100% |
Conditions | Yield |
---|---|
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; palladium 10% on activated carbon; sodium t-butanolate In 1,3,5-trimethyl-benzene for 24h; Inert atmosphere; Reflux; | 100% |
Stage #1: diphenylamine; 4'-biphenyl chloride With palladium diacetate; sodium sulfate; sodium t-butanolate; XPhos for 1h; Buchwald-Hartwig Coupling; Milling; Stage #2: In water; ethyl acetate for 0.0333333h; Reagent/catalyst; Buchwald-Hartwig Coupling; Milling; | 51% |
diphenylamine
Conditions | Yield |
---|---|
With potassium hydride In tetrahydrofuran at 50℃; for 6h; Schlenk technique; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
In toluene for 3h; Reflux; Inert atmosphere; | 100% |
hydrogen tetrakis(3,5-bis(trifluoromethyl)phenyl)borate
diphenylamine
Conditions | Yield |
---|---|
In diethyl ether at 20℃; for 1h; Glovebox; Inert atmosphere; | 100% |
2,2,6-trimethyl-4H-1,3-dioxin-4-one
diphenylamine
N,N-diphenylacetoacetamide
Conditions | Yield |
---|---|
In toluene at 20℃; for 12.25h; Reflux; | 100% |
Conditions | Yield |
---|---|
In pentane at 20℃; for 0.5h; Inert atmosphere; Glovebox; Schlenk technique; | 100% |
(5R,6S,9R)-2-(2,6-diisopropylphenyl)-6-isopropyl-3,3,9-trimethyl-2-azaspiro[4.5]decan-1-ylidene
diphenylamine
Conditions | Yield |
---|---|
In pentane at 20℃; for 0.5h; Inert atmosphere; Glovebox; | 100% |
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