Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:603-34-9
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:603-34-9
Min.Order:1 Kilogram
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Type:Manufacturers
inquiryItems Standard Result Assay 98%min -----------------------------------------------------------------------------------------------
Cas:603-34-9
Min.Order:1 Gram
FOB Price: $100.0 / 500.0
Type:Manufacturers
inquiryhigh quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:OLED Intermediate Transportation:by air or by sea Port:shanghai
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:603-34-9
Min.Order:1 Gram
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Type:Manufacturers
inquiry1)Entity factory, can batch production 2)Sample service 3)the most competitive price with good quality: we do this products so many years with Skilled craft can control the cost. so we can provide the most competitive price for our cust
Cas:603-34-9
Min.Order:1 Kilogram
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Product Description Product website: http://www.finerchem.com/pro01en/id/1450.html Product Name Triphenylamine CAS No. 603-34-9
Cas:603-34-9
Min.Order:1 Gram
FOB Price: $11.0
Type:Lab/Research institutions
inquiryTriphenylamine Basic information Product Name: Triphenylamine Synonyms: amine,triphenyl;N,N,N-Triphenylamine;n,n-diphenyl-benzenamin;Triphenylamin;N,N-DIPHENYLANILINE;N,N-diphenylbenzena
Cas:603-34-9
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufactu
Cas:603-34-9
Min.Order:1 Kilogram
FOB Price: $1.0 / 10.0
Type:Trading Company
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:603-34-9
Min.Order:1 Kilogram
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Type:Trading Company
inquiryTriphenylamine CAS No: 603-34-9 Assay: >98% Appearance: light yellow to off-white powder Application: OLED material interm Product Name: Triphenylamine Synonyms: amine,triphenyl;N,N,N-Triphenylamine;n,n-diphenyl-benzenamin;Triphen
1)quick response within 12 hours; 2)quality guarantee: all products are strictly tested by our qc, confirmed by qa and approved by third party lab in china, usa, canada, germany, uk, italy, france etc. 3) oem/odm available; 4) rea
Cas:603-34-9
Min.Order:1 Gram
FOB Price: $1.0 / 2.0
Type:Lab/Research institutions
inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:603-34-9
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
Cas:603-34-9
Min.Order:1 Kilogram
FOB Price: $39.6 / 45.1
Type:Trading Company
inquiryTriphenylamine CAS:603-34-9 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediate
Cas:603-34-9
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
1.Product name: Triphenylamine 2.CAS No. 603-34-9 3.MF: C18H15N 4.Assay:99.0%min ISO9001 Storage:Store in dry and cool place with good seal Package: 25kg/drum, or as per your request. Application:Pharmaceutical Intermediates ect. Transportati
Appearance:White or off-white Solid Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for research and industrial manufacture. Transportation:Common products:Se
Cas:603-34-9
Min.Order:100 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:603-34-9
Min.Order:0 Metric Ton
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Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Packing: According to customer requirements Delivery time: In stock or depands Port of shipment: Ningbo/Shanghai/Qingdao OEM/ODM:Welcome Sample:We can offer our existing samples at once Transportation:Express/Sea/Air Port:Ningbo/Shanghai/Qingd
Chemlyte Solutions believe that customers and suppliers deserve much more than what traditional distributors can offer. To grow in today s fast-paced and increasingly competitive market it is essential to be able to quickly adapt to market forces eff
Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:603-34-9
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryOur advantages: 1, High quality with competitive price: 1) Standard:BP/USP/EP/Enterprise standard 2) All Purity≥99% 3) We are manufacturer and can provide high quality products with factory price. 2, Fast and safe delivery 1) Parcel can be
Cas:603-34-9
Min.Order:1 Gram
Negotiable
Type:Other
inquirySuperior quality Appearance:off-white solid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:Used as Pharmaceutical Intermediates Transportation:BY
Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
GMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,
Conditions | Yield |
---|---|
With monophosphine 1,2,3,4,5-pentaphenyl-1'-(di-tert-butylphosphino)ferrocene; bis(dibenzylideneacetone)-palladium(0); sodium t-butanolate In toluene at 20℃; for 1h; | 99% |
With palladium diacetate; sodium t-butanolate; ruphos In neat (no solvent) at 110℃; for 24h; Catalytic behavior; Reagent/catalyst; Time; Buchwald-Hartwig Coupling; Inert atmosphere; Green chemistry; | 99% |
With palladium diacetate; sodium t-butanolate; ruphos In neat (no solvent) at 110℃; for 12h; Reagent/catalyst; Buchwald-Hartwig Coupling; Inert atmosphere; Green chemistry; | 99% |
Conditions | Yield |
---|---|
With (1,3-bis(2,6-diisopropylphenyl)-3,4,5,6-tetrahydropyrimidin-2-ylidene)Pd(cinnamyl, 3-phenylallyl)Cl; sodium t-butanolate In neat (no solvent) at 110℃; for 12h; Reagent/catalyst; Buchwald-Hartwig Coupling; Inert atmosphere; Green chemistry; | 99% |
With potassium tert-butylate In toluene at 135℃; for 36h; | 78% |
With copper chromium oxide; potassium hydroxide In toluene for 18h; Ullmann Condensation; Inert atmosphere; Reflux; Green chemistry; | 43% |
With bis-triphenylphosphine-palladium(II) chloride; (E)-2-(((2,5-bis(trifluoromethyl)phenyl)imino)methyl)phenol; sodium t-butanolate In o-xylene at 145℃; for 12h; Schlenk technique; Inert atmosphere; |
Conditions | Yield |
---|---|
With palladium diacetate; sodium t-butanolate; ruphos In neat (no solvent) at 110℃; for 12h; Buchwald-Hartwig Coupling; Green chemistry; | 99% |
With C30H41ClPPd; sodium t-butanolate In toluene at 100℃; for 2h; Buchwald-Hartwig Coupling; Inert atmosphere; | 99% |
With monophosphine 1,2,3,4,5-pentaphenyl-1'-(di-tert-butylphosphino)ferrocene; bis(dibenzylideneacetone)-palladium(0); sodium t-butanolate In toluene at 100℃; for 21h; | 98% |
2-(trimethylsilyl)phenyl trifluoromethanesulfonate
aniline
N,N-diphenylaminobenzene
Conditions | Yield |
---|---|
With cesium fluoride In acetonitrile at 25℃; for 72h; | 98% |
With cesium fluoride In acetonitrile at 20℃; for 72h; | 98% |
Conditions | Yield |
---|---|
With potassium tert-butylate; 1,2-bis(2,6-diisopropylphenylimino)ethane; copper(l) iodide In toluene at 120℃; for 48h; | 97% |
With potassium tert-butylate In toluene at 120℃; for 12h; Ullmann coupling; Inert atmosphere; | 95% |
With copper chromium oxide; potassium hydroxide In toluene for 6h; Catalytic behavior; Reagent/catalyst; Solvent; Ullmann Condensation; Inert atmosphere; Reflux; Green chemistry; | 95% |
Conditions | Yield |
---|---|
With cesium fluoride; bis(dibenzylideneacetone)-palladium(0); XPhos at 100℃; for 1h; Inert atmosphere; | 97% |
With cesium fluoride; bis(dibenzylideneacetone)-palladium(0); XPhos at 100℃; for 1h; Time; Inert atmosphere; | 97% |
4-(diphenylamino)phenyl boronic acid
N,N-diphenylaminobenzene
Conditions | Yield |
---|---|
With silver nitrate; triethylamine In ethanol; water at 80℃; for 0.166667h; Solvent; Reagent/catalyst; | 97% |
With copper(ll) sulfate pentahydrate; oxygen; diisopropylamine In ethanol; water at 80℃; for 1.5h; Catalytic behavior; Reagent/catalyst; Green chemistry; | 96% |
Conditions | Yield |
---|---|
With bis(triphenylphosphine)nickel(II) chloride; ethylmagnesium bromide; triphenylphosphine In tetrahydrofuran at 80℃; for 3h; | 96% |
With [Pd{C6H4(CH2N(CH2Ph)2)}(μ-Br)]2; potassium hydroxide In dimethyl sulfoxide at 120℃; for 0.666667h; | 96% |
With potassium tert-butylate In toluene at 120℃; for 12h; | 95% |
2-((4-diphenylamino)phenyl)[1,3,2]dioxaborolane
N,N-diphenylaminobenzene
Conditions | Yield |
---|---|
With silver nitrate; triethylamine In ethanol; water at 80℃; for 0.233333h; | 96% |
Conditions | Yield |
---|---|
With N/O-doped porous carbon (on base of polypyrrole) supported nanopalladium In toluene at 160℃; for 36h; Reagent/catalyst; Inert atmosphere; Sealed tube; | 96% |
Conditions | Yield |
---|---|
With potassium tert-butylate; urea; tris(dibenzylideneacetone)dipalladium(0) chloroform complex; tri tert-butylphosphoniumtetrafluoroborate In 1,4-dioxane at 100℃; for 46h; | 95% |
With ammonia; sodium; Petroleum ether | |
Multi-step reaction with 2 steps 1: sodium t-butanolate; (1,3-bis(2,6-diisopropylphenyl)-3,4,5,6-tetrahydropyrimidin-2-ylidene)Pd(cinnamyl, 3-phenylallyl)Cl / neat (no solvent) / 12 h / 110 °C / Inert atmosphere; Green chemistry 2: sodium t-butanolate; (1,3-bis(2,6-diisopropylphenyl)-3,4,5,6-tetrahydropyrimidin-2-ylidene)Pd(cinnamyl, 3-phenylallyl)Cl / neat (no solvent) / 12 h / 110 °C / Inert atmosphere; Green chemistry View Scheme |
Conditions | Yield |
---|---|
With [2,2]bipyridinyl; potassium tert-butylate; copper(l) iodide In toluene at 115℃; for 3.5h; Product distribution; Further Variations:; Reagents; | A 95% B 2% |
With copper at 180℃; for 12h; | A 46% B 31% |
With copper(l) iodide; cesium fluoride In dimethyl sulfoxide at 130℃; for 24h; Ullmann Condensation; Inert atmosphere; Glovebox; | A 12% B 39 %Chromat. |
With potassium tert-butylate; copper(l) iodide; tributylphosphine In toluene at 110℃; for 3.5h; Product distribution; Further Variations:; Catalysts; high pressure; |
Conditions | Yield |
---|---|
With potassium tetrachloropalladate(II); L-arginine; potassium hydroxide In water at 80℃; for 2h; Reagent/catalyst; | 95% |
With potassium phosphate; copper(l) iodide; lithium amide In N,N-dimethyl-formamide at 130℃; for 24h; Inert atmosphere; chemoselective reaction; | 79% |
Multi-step reaction with 2 steps 1: 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; caesium carbonate / 1,4-dioxane / 24 h / Reflux 2: 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; caesium carbonate / 1,4-dioxane / 144 h / Reflux View Scheme | |
Multi-step reaction with 2 steps 1: Pd(tris[2-(diphenylphosphino)ethyl]phosphine tetrasulfide)(dibenzylideneacetone); caesium carbonate / isopropyl alcohol / 6 h / 80 °C 2: Pd(tris[2-(diphenylphosphino)ethyl]phosphine tetrasulfide)(dibenzylideneacetone); caesium carbonate / isopropyl alcohol / 24 h / 80 °C View Scheme | |
Multi-step reaction with 3 steps 1: ammonia; potassium carbonate / water; ethanol / 20 °C / UV-irradiation; Green chemistry 2: potassium carbonate / water; ethanol / 20 °C / UV-irradiation; Green chemistry 3: potassium carbonate / water; ethanol / 20 °C / UV-irradiation; Green chemistry View Scheme |
Conditions | Yield |
---|---|
With chloranil at -60℃; | 94% |
Conditions | Yield |
---|---|
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; palladium 10% on activated carbon; sodium t-butanolate In 1,3,5-trimethyl-benzene for 24h; Inert atmosphere; Reflux; | 92% |
With dichloro{1,10-[dicyclohexylbenzyl]-3,3'-o-xylyldibenzimidazolidin-2,2'-diylidene}palladium (II); potassium tert-butylate In 1,2-dimethoxyethane at 80℃; for 15h; Buchwald-Hartwig amination; Inert atmosphere; | 92% |
With potassium hydroxide In water for 24h; Buchwald-Hartwig reaction; Reflux; Inert atmosphere; | 88% |
4-(diphenylamino)phenylboronic pinacol ester
N,N-diphenylaminobenzene
Conditions | Yield |
---|---|
With silver nitrate; triethylamine In ethanol; water at 80℃; for 0.916667h; | 92% |
With copper(ll) sulfate pentahydrate; oxygen; diisopropylamine In ethanol; water at 80℃; for 24h; Green chemistry; | 61% |
4-N,N-diphenylamino-1-bromobenzene
N,N-diphenylaminobenzene
Conditions | Yield |
---|---|
With 1,4-dioxane; 1,10-Phenanthroline; sodium hydride In mineral oil at 140℃; for 22h; Schlenk technique; Inert atmosphere; | 90% |
With tributyl-amine; tetrabutylammonium tetrafluoroborate In acetonitrile at 20℃; for 1.8h; Inert atmosphere; Electrolysis; | 80% |
With formic acid; C59H60N6O2Pt; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide for 4h; Inert atmosphere; Sealed tube; UV-irradiation; | 74 %Spectr. |
Conditions | Yield |
---|---|
toluene-4-sulfonic acid | 88.2% |
toluene-4-sulfonic acid In toluene for 12h; Heating; | 88% |
Conditions | Yield |
---|---|
potassium hydroxide; copper In various solvent(s) at 160℃; for 8h; | 88% |
diphenylamine
chlorobenzene
A
N,N-diphenylaminobenzene
B
N-(2-biphenyl)aniline
Conditions | Yield |
---|---|
With 2,2,6,6-tetramethylpiperidinyl-lithium In diethyl ether; cyclohexane at 25℃; for 24h; Inert atmosphere; | A n/a B 87% |
Conditions | Yield |
---|---|
With CoCuFe2O4; potassium hydroxide In ethanol at 60℃; for 5h; Green chemistry; | 85% |
With potassium carbonate In ethanol; water at 70℃; for 8h; Chan-Lam Coupling; | 40 %Chromat. |
Conditions | Yield |
---|---|
With C46H58Br2N4O4Pd; potassium tert-butylate In 1,2-dimethoxyethane at 80℃; for 15h; Inert atmosphere; Buchwald-Hartwig amination; | A 84% B 16% |
With water; sodium t-butanolate In N,N-dimethyl-formamide at 120℃; for 3h; Schlenk technique; | A 40% B 60% |
With potassium tert-butylate; copper(l) iodide; tributylphosphine In toluene at 135℃; for 10.5h; Product distribution; Further Variations:; Catalysts; high pressure; |
Conditions | Yield |
---|---|
With potassium tert-butylate; urea; tri tert-butylphosphoniumtetrafluoroborate; tris(dibenzylideneacetone)dipalladium(0) chloroform complex In 1,4-dioxane at 100℃; for 19h; | 83% |
With potassium tert-butylate; urea; tris(dibenzylideneacetone)dipalladium(0) chloroform complex; tri tert-butylphosphoniumtetrafluoroborate In 1,4-dioxane at 100℃; for 19h; | 83% |
Multi-step reaction with 2 steps 1: 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; caesium carbonate / 1,4-dioxane / 96 h / Reflux 2: 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; caesium carbonate / 1,4-dioxane / 144 h / Reflux View Scheme |
Conditions | Yield |
---|---|
With potassium phosphate; bis(acetylacetonato)palladium(II); dicyclohexyl-(2′,4′,6′-triisopropyl-3,6-dimethoxy-[1,1′-biphenyl]-2-yl)phosphine In n-heptane at 130℃; for 24h; Buchwald-Hartwig Coupling; Sealed tube; Inert atmosphere; | 83% |
With potassium phosphate; bis(acetylacetonato)palladium(II); BrettPhos In n-heptane at 130℃; for 24h; | 83% |
iodobenzene
copper
N,N-diphenylaminobenzene
Conditions | Yield |
---|---|
With potassium hydroxide; diphenylamine | 82% |
Conditions | Yield |
---|---|
With methanol; gold; hydrogen; caesium carbonate at 100℃; under 3800.26 Torr; for 132h; | 82% |
Conditions | Yield |
---|---|
With potassium hydroxide at 60℃; for 0.5h; Catalytic behavior; Green chemistry; | 81% |
2-(trimethylsilyl)phenyl trifluoromethanesulfonate
A
N,N-diphenylaminobenzene
B
(E)-2-[(4-nitrophenyl)methylene]cyclohexanone
Conditions | Yield |
---|---|
Stage #1: 2-[10-(N-phenylamino)-1'-(4-nitrophenyl)]methylcyclohexanone; 2-(trimethylsilyl)phenyl trifluoromethanesulfonate With potassium fluoride; 18-crown-6 ether In acetonitrile at 20℃; Inert atmosphere; Stage #2: With hydrogenchloride In water; acetonitrile for 1h; Inert atmosphere; Reflux; | A 15% B 15% C 80% |
Conditions | Yield |
---|---|
With N-Bromosuccinimide; triethylamine In N,N-dimethyl-formamide at 20℃; | 100% |
With bromine In chloroform at 0 - 20℃; for 1h; | 97% |
With N-Bromosuccinimide In N,N-dimethyl-formamide at 20℃; for 12h; Cooling with ice; | 94% |
Conditions | Yield |
---|---|
With sodium nitrate; acetic acid In chloroform at 85℃; Inert atmosphere; | 100% |
With 3-(ethoxycarbonyl)-1-(5-methyl-5-(nitrosooxy)hexyl)pyridin-1-ium bis(trifluoromethanesulfonyl)imide at 20℃; for 3h; Ionic liquid; | 89% |
With dinitrogen trioxide In dichloromethane at 0℃; | 42% |
N,N-diphenylaminobenzene
N,N,N',N'-tetraphenyl-4,4'-diaminobiphenyl
Conditions | Yield |
---|---|
Stage #1: N,N-diphenylaminobenzene With methanesulfonic acid In dichloromethane at 0℃; Stage #2: With chloranil In dichloromethane at 0 - 20℃; for 0.0166667h; Reagent/catalyst; Solvent; Time; | 99% |
With 5% rhodium-on-charcoal; trifluoroacetic acid at 50℃; for 1h; Reagent/catalyst; Green chemistry; regioselective reaction; | 99% |
Stage #1: N,N-diphenylaminobenzene With copper(II) perchlorate In acetonitrile at 25℃; for 12h; Stage #2: With potassium carbonate In water; acetonitrile at 25℃; for 0.5h; Further stages.; | 81% |
Conditions | Yield |
---|---|
Stage #1: N,N-diphenylaminobenzene With trifluorormethanesulfonic acid; [bis(pyridine)iodine]+ tetrafluoroborate In dichloromethane at 0 - 20℃; for 21h; Stage #2: With water; sodium thiosulfate In dichloromethane | 99% |
Stage #1: N,N-diphenylaminobenzene With trifluorormethanesulfonic acid; [bis(pyridine)iodine]+ tetrafluoroborate In dichloromethane at 0 - 20℃; for 21h; Stage #2: With sodium thiosulfate In dichloromethane; water | 99% |
With iodine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In dimethyl sulfoxide at 20℃; | 97% |
N,N-diphenylaminobenzene
N,N-bis(4-bromophenyl)aniline
Conditions | Yield |
---|---|
With N-Bromosuccinimide In ethyl acetate at 20℃; for 24h; | 99% |
With N-Bromosuccinimide In ethyl acetate at 20℃; for 24h; | 99% |
With N-Bromosuccinimide In N,N-dimethyl-formamide at 0℃; for 4h; | 90% |
N,N-diphenylaminobenzene
Conditions | Yield |
---|---|
With C21H17F3OP(1+)*C32H12BF24(1-) In 1,2-dichloro-ethane at 20℃; for 0.0833333h; Friedel-Crafts Alkylation; | 99% |
Conditions | Yield |
---|---|
Stage #1: 1H-imidazole; N,N-diphenylaminobenzene In acetonitrile for 0.5h; Stage #2: trifluoroacetic anhydride In acetonitrile for 1.5h; | 98.32% |
N,N-diphenylaminobenzene
5-hexylbicyclo[2.2.1]hept-2-ene
Conditions | Yield |
---|---|
{(η6-toluene)Ni(C6F5)2} In toluene at 20℃; for 24h; | 98% |
N,N-diphenylaminobenzene
tris(phenyl-2,4,6-d3)amine
Conditions | Yield |
---|---|
With tris(pentafluorophenyl)borate; water-d2 In chloroform-d1 at 80℃; for 24h; Sealed tube; regioselective reaction; | 98% |
N,N-diphenylaminobenzene
N,N-dimethyl-formamide
4-(diphenylamino)benzaldehyde
Conditions | Yield |
---|---|
Stage #1: N,N-dimethyl-formamide With trichlorophosphate In 1,2-dichloro-ethane at 20℃; for 0.0833333h; Inert atmosphere; Stage #2: N,N-diphenylaminobenzene In 1,2-dichloro-ethane at 60℃; for 16h; Inert atmosphere; | 97.6% |
With trichlorophosphate at 35 - 40℃; Inert atmosphere; | 96% |
Stage #1: N,N-diphenylaminobenzene; N,N-dimethyl-formamide With trichlorophosphate In 1,2-dichloro-ethane at 0 - 45℃; Vilsmeier-Haack reaction; Stage #2: With water In 1,2-dichloro-ethane Vilsmeier-Haack reaction; Cooling with ice; | 96% |
Conditions | Yield |
---|---|
In water at 50℃; for 3h; | 97% |
N,N-diphenylaminobenzene
chloranil
A
2,3,5,6-tetrachlorobenzene-1,4-diol
B
N,N,N',N'-tetraphenyl-4,4'-diaminobiphenyl
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 0.0166667h; Molecular sieve; | A 96% B 83% |
Conditions | Yield |
---|---|
With trichlorophosphate In dichloromethane; N,N-dimethyl-formamide at 0 - 20℃; for 0.5h; Reflux; | 95% |
Stage #1: N,N-diphenylaminobenzene With trichlorophosphate In N,N-dimethyl-formamide for 1h; Stage #2: With sodium hydroxide | 85% |
With N,N-dimethyl-formamide; trichlorophosphate at 100℃; for 6h; | 52.74% |
N,N-diphenylaminobenzene
acetyl chloride
(1,1',1''-[nitrilotri(4,1-phenylene)]tri(ethan-1-one))
Conditions | Yield |
---|---|
With aluminum (III) chloride In dichloromethane at 0 - 20℃; Friedel-Crafts Acylation; Inert atmosphere; | 95% |
With aluminum (III) chloride In dichloromethane at 0℃; for 12h; | 95% |
With aluminum (III) chloride In dichloromethane Reflux; | 92% |
N,N-diphenylaminobenzene
2,7-dibromo-(9-phenyl-9H-fluoren-9-ol)
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate In dichloromethane at 20℃; for 2h; Inert atmosphere; Schlenk technique; | 95% |
N,N-diphenylaminobenzene
4-N,N-diphenylamino-1-bromobenzene
Conditions | Yield |
---|---|
With N-Bromosuccinimide In tetrachloromethane for 4h; Reflux; | 94% |
With N-Bromosuccinimide In tetrachloromethane for 4h; Heating; | 93% |
With N-Bromosuccinimide In tetrachloromethane for 4h; Inert atmosphere; Reflux; | 93% |
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