Dayangchem’s R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantiti
Cas:603-35-0
Min.Order:100 Gram
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Type:Lab/Research institutions
inquiryHangzhou ZeErRui Chemical Co., Ltd. located in Lingang industrial areas, our plant covers an area of 6000 square meters.ZeErRui dedicated to the development, production and marketing of chemicals. We have earned ourselves a good reputation at home
Cas:603-35-0
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryTest Items Standards Results Appearance White or almost white crystalline flake white crystalline flake solub
Cas:603-35-0
Min.Order:1 Kilogram
FOB Price: $6.5 / 10.0
Type:Manufacturers
inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:603-35-0
Min.Order:0 Metric Ton
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inquiryProduct Description Product name Triphenylphosphine CAS 603-35-0 Assay 99% Appearance White crystalline powder Capacity 2000mt/year Min.package 100gram Standard
Cas:603-35-0
Min.Order:1 Kilogram
FOB Price: $1.0
Type:Lab/Research institutions
inquiryHebei yanxi chemical co., LTD is a professional research, development and production 2-phenylacetamide enterprise backbone members by local well-known entrepreneurs and professional senior engineers in the party's "low carbon environ
Cas:603-35-0
Min.Order:100 Gram
FOB Price: $2.0
Type:Manufacturers
inquiry1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appearance:White or almost white crystalline powder Storage:Store at RT. Pack
Cas:603-35-0
Min.Order:25 Kilogram
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Type:Trading Company
inquiryJinlan Pharm-Drugs Technology Co.,Limited (with its export company Hangzhou Royall Import & Export Co.,Ltd.)is located in Hangzhou, Zhejiang Province. Neighboring Ningbo port, Shanghai port, Hangzhou Xiaoshan Int’l Airport and Shanghai Pu
Cas:603-35-0
Min.Order:1 Gram
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Type:Manufacturers
inquiryBest Service: 1.Sticking to such policy of "quality first, customer first". 2.Honest business as number one priority, and work for meeting your demands. 3.With the newest quality, and best service. 5.The most strict management sy
high quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
Cas:603-35-0
Min.Order:1 Kilogram
Negotiable
Type:Manufacturers
inquiryTriphenylphosphine Product Name: Triphenylphosphine Molecular Weight: 262.29 CAS NO: 603-35-0 EC NO: 210-036-0 Molecular Formula: C18H15
Cas:603-35-0
Min.Order:1 Kilogram
FOB Price: $2.0 / 3.0
Type:Manufacturers
inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Cas:603-35-0
Min.Order:1 Metric Ton
FOB Price: $1.0
Type:Manufacturers
inquiryLIDE PHARMACEUTICALS LIMITED is a professional chemicals and APIs leading manufacturer in China. Our core business line covers APIs, Intermediates, Herb extract, etc.
Cas:603-35-0
Min.Order:1 Kilogram
FOB Price: $0.9 / 1.0
Type:Lab/Research institutions
inquiryTriphenylphosphine Basic information Product Name: Triphenylphosphine Synonyms: phosphine,triphenyl;Phosphine,triphenyl-;Phosphoris triphenyl;Trifenylfosfin;Triphenylphosphane;triphenyl-
Cas:603-35-0
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryProName: Triphenylphosphine (TPP) CasNo: 603-35-0 Molecular Formula: C18H15P Appearance: White Crystalline Powder Application: 1、In vitamin synthesis and production ... DeliveryTime: 3-5Days PackAge: 25kg/Drum Port: Q
Cas:603-35-0
Min.Order:1 Metric Ton
FOB Price: $2.0
Type:Lab/Research institutions
inquiryProduct Name Triphenylphosphine Synonyms Triphenylphosphine;Triphenyl phosphine CAS: 603-35-0 MF: - MW: - EINECS: -
Cas:603-35-0
Min.Order:5 Metric Ton
FOB Price: $1.0 / 2.0
Type:Other
inquiry1)quick response within 12 hours; 2)quality guarantee: all products are strictly tested by our qc, confirmed by qa and approved by third party lab in china, usa, canada, germany, uk, italy, france etc. 3) oem/odm available; 4) rea
Cas:603-35-0
Min.Order:1 Gram
FOB Price: $1.0 / 2.0
Type:Lab/Research institutions
inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present
Cas:603-35-0
Min.Order:1 Kilogram
FOB Price: $16.0 / 20.0
Type:Trading Company
inquiryProduct Detail Minimum Order Qty. 10 Gram
Cas:603-35-0
Min.Order:10 Gram
Negotiable
Type:Trading Company
inquiryTriumph has the complete production of G- KG - MT service chain,we can make the new technology into productivity quickly in the research and development of new products. Main Service 1.Own made fine chemical products 2.Out sourcing and quality c
Cas:603-35-0
Min.Order:100 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryOur Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter
Cas:603-35-0
Min.Order:1 Kilogram
FOB Price: $1.0 / 100000.0
Type:Lab/Research institutions
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:603-35-0
Min.Order:0 Metric Ton
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Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:603-35-0
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryGMP factoryFull experience of large numbers containers loading in main Chinese seaports Packing with pallet as buyer's special request Best service after shipment with e-mail Cargos together with container sales seervice available Rich experience for
Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:603-35-0
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryHangzhou Fandachem Co.,Ltd, a China-based chemical company, specialize in exporting Triphenylphosphine (TPP;Triphenyl phosphine pellets)99.5%,cas603-35-0, Please contact us by email freely. We are leading exporter in China. If you real
Cas:603-35-0
Min.Order:0 Metric Ton
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Type:Other
inquiryLocated in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service and h
Superior quality, moderate price & quick delivery. Appearance:white crystalline powder Storage:stored in a cool, dry and ventilated place to provent sun and rain Package:25kg/drum, or as per your request. Application:Used as Pharmaceutical
Conditions | Yield |
---|---|
With 1,1,3,3-Tetramethyldisiloxane; titanium(IV) isopropylate In various solvent(s) at 100℃; for 5h; | 100% |
With aluminium hydride*tetrahydrofuran | 100% |
With titanium(IV) isopropylate; 1,1,3,3-Tetramethyldisiloxane In methyl cyclohexane at 80℃; for 14h; | 100% |
methanol
A
bromure de methoxyvinyltriphenylphosphonium
B
triphenylphosphine
Conditions | Yield |
---|---|
With potassium cyanide In dimethyl sulfoxide for 22h; Ambient temperature; | A 86% B 100% |
A
bromure de methoxyvinyltriphenylphosphonium
B
triphenylphosphine
Conditions | Yield |
---|---|
With potassium cyanide In dimethyl sulfoxide for 22h; Ambient temperature; | A 86% B 100% |
triphenylphosphinediiodogermylene
phenyllithium
A
iodobenzene
B
biphenyl
C
triphenylgermane
D
tetraphenylgermane
E
triphenylphosphine
Conditions | Yield |
---|---|
In diethyl ether under N2, to suspn. of Ph3PGeI2 in ether PhLi added dropwise (1:4 molarratio), stirred for 5 d under reflux, hydrolyzed; dried, analyzed by gas chromy.; | A 10% B 13% C 39% D 36% E 100% |
In diethyl ether under N2, to suspn. of Ph3PGeI2 in ether PhLi added dropwise (1:1 molarratio), stirred for 5 d under reflux, hydrolyzed; dried, analyzed by gas chromy.; | A 2.9% B 2.9% C 1.9% D 14% E 82% |
In diethyl ether under N2, to suspn. of Ph3PGeI2 in ether PhLi added dropwise (1:2 molarratio), stirred for 5 d under reflux, hydrolyzed; dried, analyzed by gas chromy.; | A 7.7% B 9.6% C 1.3% D 19% E 79% |
methanol
triphenylphosphine borane
A
Trimethyl borate
B
triphenylphosphine
Conditions | Yield |
---|---|
at 120℃; Inert atmosphere; Microwave irradiation; | A n/a B 99% |
Conditions | Yield |
---|---|
With cis-[NiCl2(PPh3)2]; potassium tert-butylate In 1,4-dioxane at 90℃; for 10h; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With 15-crown-5 In tetrahydrofuran at 25℃; for 16h; Reagent/catalyst; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With tributylphosphine | 98% |
With sodium | |
With bis(2-methylphenyl)disulfide; triethylamine In chloroform for 7h; Heating; |
2-[2-Oxo-1-(triphenyl-λ5-phosphanylidene)-propyl]-1,2-dihydro-indazol-3-one
A
2-acetyl-4-oxo-dihydroquinazoline
B
triphenylphosphine
Conditions | Yield |
---|---|
In toluene at 95℃; for 2h; | A 98% B n/a |
Conditions | Yield |
---|---|
With potassium acetate; 5percent Pd on charcoal In N,N-dimethyl-formamide at 190℃; for 0.05h; microwave irradiation; | 98% |
With caesium carbonate In toluene at 115℃; for 24h; Inert atmosphere; | 90% |
With potassium acetate In N,N-dimethyl acetamide at 130℃; for 3h; Reagent/catalyst; Solvent; Temperature; Schlenk technique; Inert atmosphere; | 86% |
With rongalite; potassium hydroxide In dimethyl sulfoxide at 80℃; for 24h; Inert atmosphere; Schlenk technique; Sealed tube; | 65% |
chlorobenzene
potassium diphenylphosphine
triphenylphosphine
Conditions | Yield |
---|---|
With N,N,N,N,N,N-hexamethylphosphoric triamide In tetrahydrofuran at 25 - 67℃; for 74.4h; | 98% |
Conditions | Yield |
---|---|
With phosphorus tribromide | 97.3% |
With anhydrous phosphorus trichloride In toluene |
cis-dichlorobis(triphenylphosphine)platinum(II)
cyclenphosphorane
cis-((H2cyclen)P)PtCl2PPh3}Cl
{(eta.2-cyclenphosphorane)PtClPPh3}
C
triphenylphosphine
Conditions | Yield |
---|---|
In tetrahydrofuran under N2, mixt. of phosphorane and Pt complex in THF was stirred for 12h, pptn.; volatiles removed in vac., residue washed (10 times hexane, 10 times THF (to dissolve the η2-complex), residue (cis complex) and washing (η2.-complex) pumped dry separately, each heated to 90°C under vac., elem. anal.; | A 96% B 97% C 97% |
Conditions | Yield |
---|---|
With 15-crown-5 In tetrahydrofuran; N,N-dimethyl-formamide at 100℃; for 3h; Reagent/catalyst; Inert atmosphere; | 97% |
Diphenylphosphonigsaeure-trimethylsilylester
phenyllithium
triphenylphosphine
Conditions | Yield |
---|---|
In tetrahydrofuran at 0 - 25℃; for 2h; | 97% |
Conditions | Yield |
---|---|
96.6% |
Conditions | Yield |
---|---|
With 2,2'-azobis(isobutyronitrile); tris-(trimethylsilyl)silane In toluene at 80℃; for 1h; Product distribution; Further Variations:; Reaction partners; reaction times; | 96% |
With n In tetrahydrofuran at 60℃; for 3h; | 95% |
Stage #1: triphenylphosphine sulfide With oxalyl dichloride In toluene at 20℃; for 0.166667h; Inert atmosphere; Stage #2: With lithium aluminium tetrahydride In tetrahydrofuran; toluene at 20℃; for 0.5h; Inert atmosphere; | 88% |
2-methyl-2-(triphenylphosphonio)dithiopropionate betaine
dimethyl acetylenedicarboxylate
A
2-isopropylidene-4,5-dimethoxycarbonyl-1,3-dithiole
B
triphenylphosphine
Conditions | Yield |
---|---|
In acetonitrile for 24h; Ambient temperature; | A 96% B 67% |
Conditions | Yield |
---|---|
With 2,2'-azobis(isobutyronitrile); tris-(trimethylsilyl)silane In toluene at 80℃; for 2h; | 96% |
Conditions | Yield |
---|---|
In chloroform soln. of educt in CHCl3 heated to 60°C and stirred for 0.5 h under N2, cooled; concd. in vac., chromd. (SiO2, C6H6), 1st colorless fraction contained PPh3, red 2nd fraction collected, concd.; | A 96% B n/a |
Conditions | Yield |
---|---|
In methanol for 0.75h; Ambient temperature; | A 95% B 89% |
ethanol
triphenylphosphine borane
A
triethyl borate
B
triphenylphosphine
Conditions | Yield |
---|---|
Inert atmosphere; Reflux; | A n/a B 95% |
Conditions | Yield |
---|---|
In tetrahydrofuran; methanol for 96h; Inert atmosphere; Molecular sieve; Reflux; | 95% |
With diisopropylamine In toluene at 30℃; Kinetics; Equilibrium constant; Reagent/catalyst; Solvent; |
triphenylphosphine
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In tetrahydrofuran for 4.5h; Inert atmosphere; Cooling with ice; | 95% |
3,3,4,4-tetramethyl-1,2-dioxetane
2,2-Dihydro-4,4,5,5-tetramethyl-2,2,2-triphenyl-1,3,2-dioxaphospholane
A
3,3-dimethyl-butan-2-one
B
triphenylphosphine
Conditions | Yield |
---|---|
In benzene-d6 at 23.9℃; Kinetics; Rate constant; Thermodynamic data; other temperatures, Ea, ΔS(excit); | A 6% B 94% |
Conditions | Yield |
---|---|
With tetrabutylammomium bromide; sodium hydroxide; palladium dichloride at 120℃; for 0.5h; Inert atmosphere; | 93% |
With nickel tetrafluoroborate; lithium chloride In acetonitrile electrolysis; var. supporting electrolytes, other aryl and alkyl halides; | 80% |
With pyridine; tris-(trimethylsilyl)silane; 1,1'-azobis(1-cyanocyclohexanenitrile) In benzene for 20h; Heating; |
2-{[(Toluene-4-sulfonyl)-(triphenyl-λ5-phosphanylidene)-methyl]-azo}-benzaldehyde
A
2-p.tosyl-4-oxo-dihydroquinazoline
B
triphenylphosphine
Conditions | Yield |
---|---|
In toluene at 70℃; for 5h; | A 93% B n/a |
Conditions | Yield |
---|---|
With bis(triphenylphosphine)nickel(II) chloride; potassium tert-butylate In 1,4-dioxane at 90℃; for 12h; Reagent/catalyst; Solvent; Inert atmosphere; | 93% |
Conditions | Yield |
---|---|
With 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); sodium carbonate In 1,4-dioxane at 160℃; for 48h; Reagent/catalyst; Inert atmosphere; Schlenk technique; | 93% |
1,3-propanesultone
triphenylphosphine
3-(triphenylphosphonio)propane-1-sulfonate
Conditions | Yield |
---|---|
In toluene for 12h; Reflux; | 100% |
In tetrahydrofuran at 25℃; | 95% |
In toluene for 24h; Reflux; | 43% |
Conditions | Yield |
---|---|
In xylene for 0.00833333h; Heating; microwave irradiation; | 100% |
In toluene for 12h; Reflux; | 100% |
at 100℃; for 0.0333333h; Irradiation; | 99% |
chloromethyl methyl ether
triphenylphosphine
(methoxymethyl)triphenylphosphonium chloride
Conditions | Yield |
---|---|
In dichloromethane Reflux; | 100% |
In toluene at 95℃; for 16h; | 97.3% |
In neat (no solvent) at 80℃; for 4h; Solvent; Temperature; Time; Inert atmosphere; Schlenk technique; | 93% |
1-dodecylbromide
triphenylphosphine
dodecyltriphenylphosphonium bromide
Conditions | Yield |
---|---|
In toluene Reflux; | 100% |
In 5,5-dimethyl-1,3-cyclohexadiene at 120℃; for 48h; | 96.1% |
In tetrahydrofuran for 12h; sealed tube, bath temperature 250 deg C; | 88% |
bromoacetic acid methyl ester
triphenylphosphine
(methyloxycarbonylmethyl)triphenylphosphonium bromide
Conditions | Yield |
---|---|
In ethyl acetate at 20℃; for 17h; | 100% |
In ethyl acetate | 97% |
In benzene at 20℃; for 4h; | 97% |
α-bromoacetophenone
triphenylphosphine
triphenylphenacylphosphonium bromide
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 24h; | 100% |
at 20℃; for 24h; | 100% |
In toluene for 4h; Reflux; | 99% |
p-methoxy-phenylazide
triphenylphosphine
4-methoxy-N-(triphenylphosphoran-ylidene)-aniline
Conditions | Yield |
---|---|
In toluene at 60℃; for 16h; Schlenk technique; Inert atmosphere; | 100% |
In diethyl ether at 20℃; for 2h; | 88% |
triphenylphosphine
1,3-dibromo-propane
3-bromopropyltriphenylphosphonium bromide
Conditions | Yield |
---|---|
In toluene at 110℃; for 16h; | 100% |
In toluene for 24h; Reflux; | 99% |
In toluene Inert atmosphere; Reflux; | 98% |
Conditions | Yield |
---|---|
In toluene at 20℃; for 2h; Condensation; | 100% |
In diethyl ether for 2h; Heating; | 100% |
In diethyl ether at 20℃; for 2h; | 79% |
triphenylphosphine
hexadecanyl bromide
(1-hexadecyl)triphenylphosphonium bromide
Conditions | Yield |
---|---|
In toluene Reflux; | 100% |
In toluene at 90℃; for 48h; | 79% |
In acetonitrile for 36h; Heating; | 68% |
triphenylphosphine
diazodiphenylmethane
diphenyldiazomethane triphenylphosphazine
Conditions | Yield |
---|---|
In benzene at 30℃; for 0.00333333h; | 100% |
In acetonitrile at 30℃; Rate constant; | |
In acetonitrile at 30℃; Kinetics; Thermodynamic data; effect of 4,4'-disubstitution on the reactivity; |
Conditions | Yield |
---|---|
for 0.00833333h; Heating; microwave irradiation; | 100% |
In toluene at 0℃; for 4h; Reflux; | 100% |
In dichloromethane at 20℃; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
In benzene at 30℃; for 0.00333333h; | 100% |
With benzene | |
In acetonitrile | |
In acetonitrile Yield given; |
Conditions | Yield |
---|---|
With selenium In toluene for 6h; Heating; | 100% |
With 4-phenyl-1,2,3-selenadiazole In benzene for 1h; Heating; | 100% |
With selenium In chloroform-d1 at 20℃; | 100% |
Conditions | Yield |
---|---|
With iodine In diethyl ether at 20℃; for 1h; | 100% |
With iodine In diethyl ether; toluene | 96% |
With iodine | |
With 1,2-Diiodoethane In acetonitrile at 60℃; for 0.5h; | |
With iodine In dichloromethane at 0℃; for 2h; |
Conditions | Yield |
---|---|
With CuO2H In acetonitrile at 70℃; for 6h; | 100% |
With CuO2H In acetonitrile at 70℃; for 6h; | 100% |
With periodate form of Amberlyst A26 In chloroform at 25℃; for 2h; | 100% |
p-Methoxybenzyl bromide
triphenylphosphine
((4-methoxyphenyl)methyl)triphenylphosphonium bromide
Conditions | Yield |
---|---|
In benzene for 24h; Ambient temperature; | 100% |
In toluene at 110℃; | 99% |
In toluene for 10h; Inert atmosphere; Reflux; | 98% |
Conditions | Yield |
---|---|
In toluene at 110℃; Inert atmosphere; | 100% |
In toluene Inert atmosphere; Reflux; | 98% |
In toluene for 18h; Inert atmosphere; Reflux; | 98% |
4-Methylbenzyl chloride
triphenylphosphine
(4-methylbenzyl)triphenylphosphonium chloride
Conditions | Yield |
---|---|
In acetonitrile for 4.5h; Reflux; | 100% |
In acetonitrile for 4.5h; Reflux; | 100% |
In xylene for 18h; Heating; | 86% |
1-bromomethyl-4-bromobenzene
triphenylphosphine
4-bromobenzyl triphenylphosphonium bromide
Conditions | Yield |
---|---|
In chloroform for 4h; Heating / reflux; | 100% |
In acetonitrile for 4.5h; Reflux; | 100% |
In acetone at 20℃; for 12h; | 99% |
1-bromo-4-butene
triphenylphosphine
but-3-en-1-yltriphenylphosphonium bromide
Conditions | Yield |
---|---|
In toluene for 24h; Inert atmosphere; Reflux; | 100% |
In N,N-dimethyl-formamide for 3h; Heating; | 84% |
In acetonitrile at 23℃; for 23h; Reflux; Inert atmosphere; | 81% |
triphenylphosphine
prenyl bromide
(3-methylbut-2-enyl)triphenylphosphonium bromide
Conditions | Yield |
---|---|
In toluene at 110℃; Inert atmosphere; | 100% |
In benzene at 20℃; for 20h; | 96% |
In toluene Ambient temperature; | 93% |
[14C]methyl iodide
triphenylphosphine
-methyltriphenylphosphonium iodide
Conditions | Yield |
---|---|
In benzene at 22℃; for 37h; | 100% |
In diethyl ether Methylation; | 95% |
In benzene for 24h; | 90% |
(E)-1-bromo-2-hexene
triphenylphosphine
<(E)-hex-2-enyl>triphenylphosphonium bromide
Conditions | Yield |
---|---|
In benzene for 5h; Heating; | 100% |
Conditions | Yield |
---|---|
In toluene for 8h; Reflux; | 100% |
In acetonitrile for 16h; Heating; | 95.6% |
In toluene for 120h; Heating; | 92% |
iodomethane-d3
triphenylphosphine
(methyl-d3)triphenylphosphonium iodide
Conditions | Yield |
---|---|
In tetrahydrofuran for 1h; Reflux; | 100% |
In tetrahydrofuran for 1h; Schlenk technique; Reflux; | 99% |
In tetrahydrofuran for 1h; Schlenk technique; Inert atmosphere; Reflux; | 99% |
Conditions | Yield |
---|---|
In chlorobenzene for 48h; Heating; | 100% |
In toluene Reflux; | 100% |
In o-xylene Heating; | 98.7% |
1-Bromotetradecane
triphenylphosphine
(n-tetradecyl)triphenylphosphonium bromide
Conditions | Yield |
---|---|
In toluene Reflux; | 100% |
at 140℃; for 7h; | 92% |
In benzene for 48h; Substitution; Heating; | 92% |
6-bromohexanoic acid
triphenylphosphine
(5-carboxypentyl)triphenylphosphonium bromide
Conditions | Yield |
---|---|
In acetonitrile for 16h; Heating; | 100% |
at 100℃; for 4h; | 100% |
In acetonitrile for 24h; Heating; | 99% |
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