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inquiryFounded in 2008, East Chemsources Limited is a professional manufacturer and supplier in food and chemical field in China. Through more than ten years development, our company has developed from single product at first to provide solution to final
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inquiryProduct Name: Benzyltriphenylphosphonium chloride Synonyms: (phenylmethyl)triphenyl-phosphoniuchloride;(phenylmethyl)triphenylphosphoniumchloride;Benzyltriphenylchlorophosphine;benzyltriphenylphosphonidechloride;benzyltriphenyl-phospho
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inquiryProduct Description Product name Benzyltriphenylphosphonium chloride CAS 1100-88-5 Assay 99% Appearance
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inquiryLIDE PHARMACEUTICALS LIMITED is a professional chemicals and APIs leading manufacturer in China. Our core business line covers APIs, Intermediates, Herb extract, etc.
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inquiryOur advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
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inquiryName: Triphenyl(phenylmethyl)-phosphonium chloride CAS:1100-88-5 MF: C25H22ClP Appearance:White Powder Storage:Store in cool and dry place, away from sun light. Package:25KG Application:Water Treatment Chemicals Transportation:By sea or by air Po
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inquiryBenzyltriphenylphosphonium chloride CAS:1100-88-5 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quali
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inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
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inquiry1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
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inquiryWe are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
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inquirySuperior quality Appearance:white powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:Used as Pharmaceutical Intermediates Transportation:BY AI
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inquiryProduct name: Benzyltriphenylphosphonium Chloride CAS No.: 1100-88-5 Molecule Formula:C25H22ClP Molecule Weight:388.87 Purity: 99.0% Package: 25kg/drum Description:White to off-white solid Manufacture Standards:Enterprise Standard
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inquiryProduct Name: Benzyltriphenylphosphonium chloride CAS: 1100-88-5 MF: C25H22ClP MW: 388.87 EINECS: 214-154-3 Benzyltriphenylphosphonium chloride Structure Benzyltriphenylphosphonium chloride Chemical Properties Melting point ≥3
Cas:1100-88-5
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inquiryZhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed produc
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inquiryConditions | Yield |
---|---|
In toluene at 110℃; Inert atmosphere; | 100% |
In toluene Inert atmosphere; Reflux; | 98% |
In toluene for 18h; Inert atmosphere; Reflux; | 98% |
benzyltrimethylammonium chloride
triphenylphosphine
benzyltriphenylphosphonium chloride
Conditions | Yield |
---|---|
at 250℃; for 0.166667h; Irradiation; | 95% |
chloromethyltriphenylphosphonium chloride
Benzyltriphenylphosphonium dimethyldithiocarbamate
A
benzyltriphenylphosphonium chloride
B
Dimethylthiocarbamoylsulfanylmethyl-triphenyl-phosphonium; chloride
Conditions | Yield |
---|---|
In 1,2-dimethoxyethane for 2.5h; Ambient temperature; | A 80% B 50% |
methyl chloroformate
triphenyl(phenylmethylene)phosphorane
A
benzyltriphenylphosphonium chloride
B
<α-(methoxycarbonyl)benzylidene>triphenylphosphorane
Conditions | Yield |
---|---|
In benzene Ambient temperature; |
Conditions | Yield |
---|---|
With hydrogenchloride for 12h; Heating; Yield given; |
phenyldiazomethane
triphenylphosphine
benzyltriphenylphosphonium chloride
Conditions | Yield |
---|---|
With copper(l) chloride |
[α-(phenylphosphanyl)benzylidene]triphenylphosphorane
benzyltriphenylphosphonium chloride
Conditions | Yield |
---|---|
With hydrogenchloride In tetrahydrofuran; diethyl ether at 0℃; for 0.5h; |
[α-(phenylphosphanyl)benzylidene]triphenylphosphorane
A
benzyltriphenylphosphonium chloride
B
phenylphosphane
C
tetraphenyl-cyclotetraphosphane
Conditions | Yield |
---|---|
With hydrogenchloride In diethyl ether; dichloromethane at 0℃; for 0.0833333h; Further byproducts given; |
benzyltriphenylphosphonium chloride
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 89 percent / LiAlH4 / tetrahydrofuran / -40 °C 2: 1 M HCl / tetrahydrofuran; diethyl ether / 0.5 h / 0 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: n-butyl-lithium / hexane; benzene 2: benzene / Ambient temperature View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: benzene / Ambient temperature 2: n-butyl-lithium / hexane; benzene 3: benzene / Ambient temperature View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: benzene / Ambient temperature 2: n-butyl-lithium / hexane; benzene 3: benzene / Ambient temperature View Scheme |
Conditions | Yield |
---|---|
thermal decompn.; |
dichlorotriphenyl-λ4-phosphane
benzylmagnesium chloride
benzyltriphenylphosphonium chloride
Conditions | Yield |
---|---|
Stage #1: chloro(triphenyl)phosphonium chloride; benzylmagnesium chloride In tetrahydrofuran; dichloromethane at -41℃; for 0.75h; Inert atmosphere; Stage #2: With hydrogenchloride In diethyl ether; water for 0.166667h; Solvent; Temperature; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: oxalyl dichloride / 1 h / 20 °C / Inert atmosphere 2.1: dichloromethane; tetrahydrofuran / 0.75 h / -41 °C / Inert atmosphere 2.2: 0.17 h View Scheme |
poly(methacrylic acid)
benzyltriphenylphosphonium chloride
phenylmethanethiol
3-benzylthio-2-methylpropanoic acid
Conditions | Yield |
---|---|
With sodium hydroxide; sodium bicarbonate | 100% |
benzyltriphenylphosphonium chloride
Conditions | Yield |
---|---|
In tetrahydrofuran; hexane | 98.7% |
benzyltriphenylphosphonium chloride
iron(III) chloride
((C6H5)3PCH2C6H5)(1+)*FeCl4(1-)=((C6H5)3PCH2C6H5)FeCl4
Conditions | Yield |
---|---|
In water to aq. soln. of phosphonium salt was added aq. soln. of FeCl3 with stirring at room temp., crystalline solid formed; filtn., drying, recrystn. from n-butanol; elem. anal.; | 98.3% |
benzyltriphenylphosphonium chloride
Conditions | Yield |
---|---|
With sodium periodate at 20℃; for 0.333333h; | 98% |
Conditions | Yield |
---|---|
Stage #1: benzyltriphenylphosphonium chloride With n-butyllithium In hexane; water at -78 - 0℃; Stage #2: C48H42O6 In tetrahydrofuran; hexane at 25℃; for 3h; | 98% |
Conditions | Yield |
---|---|
With water; sodium hydroxide at 20℃; Reagent/catalyst; | 98% |
Multi-step reaction with 2 steps 1: 1.) BuLi / 1) THF, hexane, room temperature, 30 min; 2) THF, hexane, room temperature, 3 h 2: 1 h / 850 °C / 0 - 0.01 Torr View Scheme | |
Multi-step reaction with 2 steps 1: 1.) BuLi / 1) THF, hexane, room temperature, 30 min; 2) THF, hexane, room temperature, 3 h 2: 1 h / 850 °C / 0 - 0.01 Torr View Scheme | |
Multi-step reaction with 3 steps 1: NaH, Dimethylsulfoxide 2: 60 percent / dimethylsulfoxide / 0.5 h / Ambient temperature 3: 0.03 h / 180 °C View Scheme |
benzyltriphenylphosphonium chloride
Conditions | Yield |
---|---|
With sodium nitrate In water at 20℃; | 98% |
Conditions | Yield |
---|---|
In dichloromethane; water | 98% |
benzyltriphenylphosphonium chloride
triphenyl(phenylmethylene)phosphorane
Conditions | Yield |
---|---|
With n-butyllithium In hexane | 97% |
With sodium ethanolate | |
With n-butyllithium In diethyl ether for 0.5h; |
Conditions | Yield |
---|---|
In toluene addn. of butylamine to WOCl4 and phosphonium salt soln. under N2; refluxing, 6h; evapn.; extn. (CH2Cl2); filtration; diffusion of hexane into soln.; crystn.; elem. anal.; | 97% |
benzyltriphenylphosphonium chloride
Conditions | Yield |
---|---|
With sodium persulfate In water at 20℃; for 0.333333h; | 96% |
cis-bis(dimethylsulfoxide)dichloroplatinum(II)
benzyltriphenylphosphonium chloride
triphenylbenzylphosphonium-Pt(dimethyl sulfoxide)Cl3
Conditions | Yield |
---|---|
In acetonitrile addn. of org. ligand to suspn. of Pt-complex (20°C); solvent removal (vac., room temp.); oily residue crystn. under a layer of ethanol, ppt. filtered out, washed with ethanol and ether and air-dried (75°C); elem. anal.; | 96% |
trichlorotris(tetrahydrofuran)chromium(III)
benzyltriphenylphosphonium chloride
1,2-bis-(2-propylphosphino)benzene
benzyltriphenylphosphonium tetrachloro{o-phenylenebis(isopropylphosphine)}chromate(III)
Conditions | Yield |
---|---|
In toluene addn. of C6H4(Pi-PrH)2 to a soln. of CrCl3(thf)3 and (PPh3(CH2Ph))Cl in toluene (1:1:1 molar ratio) under stirring (under O2-free N2 or Ar), refluxing (12 h), pptn.; washing (toluene, 2 times); elem. anal.; | 96% |
Li(1+)*C6F5(1-)=Li(C6F5)
benzyltriphenylphosphonium chloride
thallium (III) chloride
(C6H5)3PCH2C6H5(1+)*[Tl(C6F5)4](1-)=((C6H5)3PCH2C6H5)[Tl(C6F5)4]
Conditions | Yield |
---|---|
In diethyl ether TlCl3 added to LiC6F5 soln. at -78°C, stirred for 15 min, allowed to warm to room temp., stirred for 3 h under N2, a few drops of H2O added, Ph3BzPCl added; exposed to air for 10 min, filtered, evapd., recrystd. (CH2Cl2/hexane);elem. anal.; | 96% |
benzyltriphenylphosphonium chloride
Conditions | Yield |
---|---|
In dichloromethane (N2, Schlenk) to a soln. of complex in CH2Cl2 was added solid C6H5CH2P(C6H5)3Cl, stirred at room temp.; volatiles were removed under reduced pressure, the foam was washed with toluene; elem. anal.; | 96% |
benzyltriphenylphosphonium chloride
(+/-)-1,1-dimethylethyl 4-oxo-2-(phenylmethyl)-1-piperidinecarboxylate
2-Benzyl-4-[1-phenyl-meth-(E)-ylidene]-piperidine-1-carboxylic acid tert-butyl ester
Conditions | Yield |
---|---|
Stage #1: benzyltriphenylphosphonium chloride With potassium tert-butylate In tetrahydrofuran deprotonation; Stage #2: (+/-)-1,1-dimethylethyl 4-oxo-2-(phenylmethyl)-1-piperidinecarboxylate In tetrahydrofuran at 23℃; Wittig reaction; Further stages.; | 95% |
5-formyl-10-methoxybenzo[c]phenanthrene
benzyltriphenylphosphonium chloride
5-(β-phenylethenyl)-10-methoxybenzo[c]phenanthrene
Conditions | Yield |
---|---|
With sodium hydroxide In water for 0.25h; Wittig reaction; | 95% |
benzyltriphenylphosphonium chloride
2,3,4-tri-O-benzyl-D-arabinopyranose
Conditions | Yield |
---|---|
With sodium hydride; dimethyl sulfoxide In tetrahydrofuran at 45℃; Wittig olefination; | 95% |
benzyltriphenylphosphonium chloride
Conditions | Yield |
---|---|
In dichloromethane byproducts: tetrahydrothiophene; N2 atmosphere, stirring (15 min, room temp.); concn. (evapn.), pptn. on n-hexane addn.; elem. anal.; | 95% |
benzyltriphenylphosphonium chloride
(benzyltriphenylphosphonium){Pt(3,5-dimethylpyrazole)Cl3}
Conditions | Yield |
---|---|
With (N2H5)2SO4 In water water added to mixt. of hydrazine sulfate and Pt-complex, heated at 60-70°C for 5min, cooled, filtered, BzlPPh3Cl soln. added to filtrate, stirred for 10min; product filtered off, washed with hot water (3 times, alcohol, ether (3 times), dried in air at 90°C; elem. anal.; | 95% |
benzyltriphenylphosphonium chloride
Conditions | Yield |
---|---|
With chromium(VI) oxide; hydrogenchloride In water at 20℃; for 15h; | 94% |
benzyltriphenylphosphonium chloride
(4R,5R)-4-[tert-Butoxycarbonyl-((S)-2-methyl-3-oxo-propyl)-amino]-5-isobutoxy-azepane-1-carboxylic acid 2-trimethylsilanyl-ethyl ester
Conditions | Yield |
---|---|
Stage #1: benzyltriphenylphosphonium chloride With n-butyllithium In hexane; benzene at 20℃; for 1h; Wittig reaction; Stage #2: (4R,5R)-4-[tert-Butoxycarbonyl-((S)-2-methyl-3-oxo-propyl)-amino]-5-isobutoxy-azepane-1-carboxylic acid 2-trimethylsilanyl-ethyl ester In hexane; benzene at 20℃; for 5h; | A 94% B n/a |
benzyltriphenylphosphonium chloride
Conditions | Yield |
---|---|
With sodium hydride; dimethyl sulfoxide In tetrahydrofuran at 45℃; Wittig olefination; | 94% |
potassium tetrachloroplatinate(II)
benzyltriphenylphosphonium chloride
dimethyl sulfoxide
benzyltriphenylphosphonium trichloro(dimethylsulfoxide)platinate(II)
Conditions | Yield |
---|---|
In dimethyl sulfoxide byproducts: KCl; mixing Pt complex, P compd., DMSO, stirring at room temp. for 5 min; slow evapn., isolation of crystals, elem. anal.; | 94% |
Conditions | Yield |
---|---|
Stage #1: benzyltriphenylphosphonium chloride With potassium tert-butylate In dimethyl sulfoxide at 20℃; for 0.0333333h; Stage #2: 9,10-phenanthrenequinone In dimethyl sulfoxide at 20℃; for 0.5h; | 94% |
Conditions | Yield |
---|---|
In further solvent(s) to 150°C hot soln. of phosphonium salt in n-octanol added soln. of anhydrous ZnCl2 in n-octanol, temp. increased to 185-187°C, ppt. formed after 30 min; ppt. filtered at 150°C; recrystn. from n-octanol or acetonitrile; elem. anal.; | 93.7% |
1,1,1-trifluoroacetophenone
benzyltriphenylphosphonium chloride
1,2-diphenyl-3,3,3-trifluoroprop-1-ene
Conditions | Yield |
---|---|
With sodium ethanolate In ethanol | 93.5% |
benzyltriphenylphosphonium chloride
Conditions | Yield |
---|---|
With n-butyllithium In diethyl ether; hexane Ph3P(CH2Ph)Br suspended in dry Et2O was treated under N2 with n-BuLi inhexane and stirred for 2 h, Rh-complex was added, the mixt. stirred at room temp. overnight and then heated under reflux for 5 h; the ether was removed in vacuo, residue washed with 3:2 MeOH-water and with a little cold MeOH, recrystd. from acetone; elem. anal.; | 93% |
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