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Cas:113-52-0
Min.Order:1 Gram
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Min.Order:5 Kiloliter
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inquiryCAS 113-52-0 Synonyms Imipramine hydrochloride,10,11-Dihydro-N,N-dimethyl-5H-dibenz[b,f]azepine-5-propanamine hydrochloride, 5-[3-(Dimethylamino)propyl]-10,11-dihydro-5H-dibenz[b,f]azepine hydrochloride;Imi
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Cas:113-52-0
Min.Order:10 Gram
Negotiable
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Min.Order:1 Kilogram
Negotiable
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Min.Order:1 Gram
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Min.Order:1 Kilogram
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inquiryAppearance:white powder Storage:Store in a cool,dry place and keep away from direct strong light Package:packaged in foil bags or tins Application:Use only for laboratory research Transportation:Sea,Air,DHL/TNT/FEdex/UPS/EMS Por
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Min.Order:1 Gram
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Cas:113-52-0
Min.Order:1 Gram
Negotiable
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Min.Order:0
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Imipramine hydrochloride
Conditions | Yield |
---|---|
Stage #1: In acetone for 0.5h; Heating / reflux; Stage #2: In di-isopropyl ether at 0 - 5℃; |
Conditions | Yield |
---|---|
In water E-2 M solns. were mixed; ppt. was filtered, thoroughly washed with distd. water, dried at room temp., elem. anal.; | 99.5% |
Conditions | Yield |
---|---|
In water E-2 M solns. were mixed; ppt. was filtered, thoroughly washed with distd. water, dried at room temp., elem. anal.; | 99.5% |
Conditions | Yield |
---|---|
In water at 20 - 62℃; for 19.95h; | 95.1% |
In water at 20 - 62℃; for 19.95h; | 95.1% |
Imipramine hydrochloride
N,N-dimethyl-formamide
2-Formylimipramine
Conditions | Yield |
---|---|
With trichlorophosphate at 100℃; for 4h; Formylation; Vilsmeier Reaction; | 59% |
Imipramine hydrochloride
orthoformic acid triethyl ester
[3-(2-{Bis-[5-(3-dimethylamino-propyl)-10,11-dihydro-5H-dibenzo[b,f]azepin-2-yl]-methyl}-10,11-dihydro-dibenzo[b,f]azepin-5-yl)-propyl]-dimethyl-amine
Conditions | Yield |
---|---|
With tetrafluoroboric acid diethyl ether In diethyl ether; dichloromethane for 6h; Ambient temperature; | 8% |
Imipramine hydrochloride
A
desipramine
B
9,10-dihydrodibenzazepine
C
10-Hydroxyimipramine
Conditions | Yield |
---|---|
In water Ambient temperature; M. griseo-cyanus (ATCC 1207a); further microbial agents; | A 10 mg B n/a C n/a |
Imipramine hydrochloride
A
desipramine
B
9,10-dihydrodibenzazepine
C
10-Hydroxyimipramine
D
2-hydroxyimipramine
Conditions | Yield |
---|---|
In water for 480h; Ambient temperature; C. blakesleeana (ATCC 8688a); further microbial agents; Further byproducts given; | A n/a B n/a C 30 mg D 88 mg |
Imipramine hydrochloride
A
9,10-dihydrodibenzazepine
B
10-Hydroxyimipramine
C
2-hydroxyimipramine
D
imipramine N-oxide
Conditions | Yield |
---|---|
In water; N,N-dimethyl-formamide for 480h; Ambient temperature; C. blakesleeana (ATCC 8688a); further microbial agents; Further byproducts given; | A n/a B 30 mg C 88 mg D n/a |
Imipramine hydrochloride
A
9,10-dihydrodibenzazepine
B
imipramine N-oxide
Conditions | Yield |
---|---|
In water; N,N-dimethyl-formamide for 360h; Ambient temperature; F. oxysporum f. sp. cepae (ATCC 11711); further microbial agents; | A 7 mg B n/a |
In water for 312h; Ambient temperature; A. flavipes (ATCC 16795); further microbial agents; | A n/a B 112 mg |
Imipramine hydrochloride
C19H20(2)H4N2*ClH
Conditions | Yield |
---|---|
With deuteroacetic acid; sulfuric acid-d2 at 100℃; for 1.5h; in sealed tube; Yield given; |
Imipramine hydrochloride
Conditions | Yield |
---|---|
With sulfuric acid |
Imipramine hydrochloride
Conditions | Yield |
---|---|
With iron(III) chloride; acetic acid at 75℃; for 0.0833333h; |
Conditions | Yield |
---|---|
at 280 - 326℃; Kinetics; |
Conditions | Yield |
---|---|
With NADP; cDNA-expressed human recombinant CYP1A2 In phosphate buffer at 37℃; for 0.25h; pH=7.4; Enzyme kinetics; Further Variations:; concentration; |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 59 percent / POCl3 / 4 h / 100 °C 2: m-CPBA; TFA / CH2Cl2 / 2 h / 5 - 20 °C 3: conc. HCl / methanol / 2 h View Scheme |
Imipramine hydrochloride
formic acid 5-(3-dimethylamino-propyl)-10,11-dihydro-5H-dibenzo[b,f]azepin-2-yl ester
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 59 percent / POCl3 / 4 h / 100 °C 2: m-CPBA; TFA / CH2Cl2 / 2 h / 5 - 20 °C View Scheme |
Imipramine hydrochloride
3-Hydroxy-2-naphthoic acid
imipramine xinafoate
Conditions | Yield |
---|---|
In water at 25 - 50℃; for 20h; |
Conditions | Yield |
---|---|
Stage #1: disodium pamoate; Imipramine hydrochloride In water; acetone at 20 - 55℃; Stage #2: In water at 40 - 70℃; | |
In water at 5℃; |
impramine
Imipramine hydrochloride
embonic acid disodium salt
imipramine pamoate
Conditions | Yield |
---|---|
With sodium hydroxide In water |
Conditions | Yield |
---|---|
With peroxidase from horseradish type VI; dihydrogen peroxide at 37℃; for 1h; pH=7; aq. phosphate buffer; Enzymatic reaction; |
Imipramine hydrochloride
Conditions | Yield |
---|---|
With zinc(II) chloride at 60 - 100℃; for 24h; Inert atmosphere; Sealed tube; |
Conditions | Yield |
---|---|
With NADP+; D-glucose-6- In aq. phosphate buffer; dimethyl sulfoxide at 37℃; for 1h; pH=7.4; Enzymatic reaction; |
Imipramine hydrochloride
2-hydroxynaphthalene-3-carboxylic acid sodium salt
Conditions | Yield |
---|---|
In water at 50℃; for 20h; | 12.7 g |
Conditions | Yield |
---|---|
With sodium hydroxide In water |
Imipramine hydrochloride
Conditions | Yield |
---|---|
In aq. phosphate buffer pH=7.4; UV-irradiation; |
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