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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
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inquiry1-Cyclohexylethanol cas 1193-81-3Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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inquiryConditions | Yield |
---|---|
With hydrogen In water at 100℃; under 15001.5 Torr; for 0.333333h; | 100% |
With ruthenium nanoparticles at 120℃; under 90009 Torr; for 2h; Ionic liquid; Autoclave; | 99% |
With ruthenium; hydrogen In water at 30℃; under 22801.5 Torr; for 12h; Autoclave; | 94% |
Conditions | Yield |
---|---|
Stage #1: Cyclohexyl methyl ketone With formic acid; tricarbonyl (4S,7S)-4,7-bis(benzyloxy)-1,3-diphenyl-4,5,6,7-tetrahydro-2H-inden-2-one iron; triethylamine for 0.166667h; Inert atmosphere; Stage #2: With trimethylamine-N-oxide at 60℃; for 48h; Reagent/catalyst; Concentration; Temperature; | 97% |
With sodium isopropylate; isopropyl alcohol; ruthenium complex C38H42N2O4P2Ru for 5h; Catalytic hydrogenation; Catalytic transfer hydrogenation; | 91% |
With methanol; sodium tetrahydroborate at 0 - 20℃; for 0.666667h; Inert atmosphere; | 88% |
rac-1-cyclohexylethanol
Conditions | Yield |
---|---|
With water; scandium tris(trifluoromethanesulfonate) In acetonitrile for 4h; Ambient temperature; | 97% |
methyltrichlorotitanium
cyclohexanone
A
1-Methylcyclohexanol
B
rac-1-cyclohexylethanol
Conditions | Yield |
---|---|
With Methyltitantrichlorid,Triphenylphosphin; cyclohexanecarbaldehyde In dichloromethane at -25℃; for 6h; Product distribution; other phosphane-complexes and reagents; | A 95% B 3% |
Conditions | Yield |
---|---|
With Methyltitantrichlorid,Triphenylphosphin; cyclohexanecarbaldehyde In dichloromethane at 0℃; for 6h; | A 95% B 3% |
2-methyl-1-oxaspiro[2.5]octane
A
1-ethylcyclohexanol
B
rac-1-cyclohexylethanol
Conditions | Yield |
---|---|
With bis(cyclopentadienyl)titanium (III) chloride; cyclohexa-1,4-diene In tetrahydrofuran Product distribution; Mechanism; Ambient temperature; other epoxides, reaction without cyclohexa-1,4-diene; | A 1.5% B 92% C 0.9% |
With bis(cyclopentadienyl)titanium (III) chloride; cyclohexa-1,4-diene In tetrahydrofuran Ambient temperature; | A 1.5% B 92% C 0.9% |
With bis(cyclopentadienyl)titanium (III) chloride; cyclohexa-1,4-diene In tetrahydrofuran for 0.666667h; Product distribution; Mechanism; other epoxides; other H-atom donors; var. temperature, var. time; | A 1.5% B 64% C 0.9% |
With bis(cyclopentadienyl)titanium (III) chloride; cyclohexa-1,4-diene In tetrahydrofuran for 0.25h; | A n/a B 64% C 0.9% |
With bis(cyclopentadienyl)titanium (III) chloride; cyclohexa-1,4-diene In tetrahydrofuran for 0.25h; Yields of byproduct given; | A n/a B n/a C 0.9% |
2-(2,6-dimethoxyphenoxy)-1-phenylethan-1-ol
A
1,3-dimethoxy-2-hydroxy-benzene
B
ethylbenzene
C
rac-1-cyclohexylethanol
Conditions | Yield |
---|---|
With Ni0.85Ru0.15; hydrogen In water at 95℃; under 760.051 Torr; for 16h; Reagent/catalyst; | A 92% B 58% C 22% |
rac-1-cyclohexylethanol
Conditions | Yield |
---|---|
With water; boric acid at 20℃; for 1h; | 90% |
methyltrichlorotitanium
cyclohexanecarbaldehyde
A
n-hexan-2-one
B
rac-1-cyclohexylethanol
Conditions | Yield |
---|---|
With n-hexan-2-one; Methyltitantrichlorid,Triphenylphosphin In dichloromethane at -25℃; for 6h; Product distribution; other phosphane-complexes and reagents; | A 6% B 89% |
cyclohexanecarbaldehyde
A
1-Methylcyclohexanol
B
rac-1-cyclohexylethanol
Conditions | Yield |
---|---|
With n-hexan-2-one; Methyltitantrichlorid,Triphenylphosphin In dichloromethane at -25℃; for 6h; | A 6% B 89% |
2-methyl-4,7-dihydro-1,3-dioxepine
cyclohexylmagnesium bromide
A
rac-1-cyclohexylethanol
B
(2Z)-4-cyclohexyl-1-hydroxy-2-butene
Conditions | Yield |
---|---|
1,2-bis(diphenylphosphino)ethane nickel(II) chloride for 8h; Ambient temperature; Yields of byproduct given; | A n/a B 88% |
methyltriisopropoxytitanium(IV)
cyclohexanecarbaldehyde
rac-1-cyclohexylethanol
Conditions | Yield |
---|---|
In diethyl ether at 0℃; for 0.5h; | 85% |
In dichloromethane at 22℃; for 0.5h; | 95 % Spectr. |
2-methyl-1-oxaspiro[2.5]octane
rac-1-cyclohexylethanol
Conditions | Yield |
---|---|
With manganese; cyclohexa-1,4-diene; titanocene dichloride; 2,4,6-collidine hydrochloride In tetrahydrofuran for 16h; | 81% |
With bis(cyclopentadienyl)titanium dichloride; collidine hydrochloride; cyclohexa-1,4-diene; zinc In tetrahydrofuran for 30h; Ambient temperature; | 76% |
dimethyldichlorotitanium(IV)
cyclohexanecarbaldehyde
rac-1-cyclohexylethanol
Conditions | Yield |
---|---|
In dichloromethane at -40℃; for 1h; | 78% |
Conditions | Yield |
---|---|
With bis(acetylacetonate)nickel(II); triphenylphosphine In tetrahydrofuran; hexane at 0℃; for 11h; | 76% |
With 2,7-dimethyl-1,8-biphenylenediol 1.) CH2Cl2, hexane, r.t., 30 min, 2.) CH2Cl2, hexane, -78 deg C, 1 h; Yield given. Multistep reaction; |
Conditions | Yield |
---|---|
In diethyl ether; toluene Heating; Yields of byproduct given; | A n/a B 75% C n/a |
dimethyl zinc(II)
buta-1,3-diene
cyclohexanecarbaldehyde
A
rac-1-cyclohexylethanol
Conditions | Yield |
---|---|
bis(acetylacetonate)nickel(II) In tetrahydrofuran; hexane at 25℃; for 1h; Addition; | A 10% B 73% C 17% |
acetophenone
A
ethyl-cyclohexane
B
ethylbenzene
C
1-Phenylethanol
D
rac-1-cyclohexylethanol
Conditions | Yield |
---|---|
With hydrogen; Pd APII Deloxan at 200℃; under 90007.2 Torr; | A n/a B 69% C n/a D n/a |
With hydrogen; Pd APII Deloxan In various solvent(s) at 90℃; under 90007.2 Torr; Product distribution; various temp. and pressures; | |
With carbon dioxide; hydrogen at 180℃; under 90009 Torr; Supercritical conditions; Flow reactor; | A 17 %Spectr. B 41 %Spectr. C 14 %Spectr. D 28 %Spectr. |
2-phenoxy-1-phenylethanone
A
1-Phenylethanol
B
rac-1-cyclohexylethanol
C
cyclohexanol
D
phenol
Conditions | Yield |
---|---|
With isopropyl alcohol In aq. buffer at 60℃; for 9h; pH=8; Electrochemical reaction; | A 9% B 63% C 69% D 28% |
rac-1-cyclohexylethanol
acetic anhydride
1-cyclohexylethan-1-yl acetate
Conditions | Yield |
---|---|
With dmap In ethyl acetate | 100% |
With copper(II) bis(trifluoromethanesulfonate) In dichloromethane for 0.5h; Ambient temperature; | 96% |
With copper(II) bis(trifluoromethanesulfonate) In dichloromethane at 20℃; for 1h; | 96% |
Conditions | Yield |
---|---|
In diethyl ether at 0 - 20℃; | 100% |
Conditions | Yield |
---|---|
With aluminum oxyhydroxide; ruthenium In toluene at 110℃; for 12h; | 99% |
With nickel(II) triflate; cyclohexanone; 1,2-bis-(dicyclohexylphosphino)ethane In toluene at 110℃; for 12h; Schlenk technique; | 99% |
[(η5-(4-HOCH2C6H4)Ph3C4CO)2H]Ru2((CO)4)(μ-H)-SiO2 In toluene at 110℃; for 8h; | 97% |
Conditions | Yield |
---|---|
aluminum oxide; cesium fluoride at 129.85℃; for 0.75h; | 98% |
With immobilized 1,5,7-triazabicyclo[4.4.0]dec-5-ene on magnetic γ-Fe2O3 nanoparticles at 125℃; for 6h; | 96% |
Conditions | Yield |
---|---|
N,N'-dibromo-N,N'-1,2-ethanediylbis-(benzenesulfonamide) at 20℃; for 7.5h; | 96% |
Stage #1: rac-1-cyclohexylethanol With Iron(III) nitrate nonahydrate; sodium iodide In dichloromethane at 20℃; Stage #2: 1,1,1,3,3,3-hexamethyl-disilazane In dichloromethane at 20℃; | 95% |
With boric acid In acetonitrile at 20℃; for 1.1h; | 95% |
rac-1-cyclohexylethanol
Conditions | Yield |
---|---|
With γ-Fe2O3-immobilized 1,5,7-triazabicyclo[4.4.0]dec-5-ene nanoparticles (MNPs-TBD) at 125℃; for 6h; | 96% |
rac-1-cyclohexylethanol
Conditions | Yield |
---|---|
Stage #1: rac-1-cyclohexylethanol With sodium hydride In 1,4-dioxane at 20℃; for 1h; Stage #2: With triethylamine sulfurtrioxide In 1,4-dioxane at 20℃; | 95% |
rac-1-cyclohexylethanol
1-Cyclohexylethyl α-<1-(9-anthryl)-2,2,2-trifluoroethoxy>acetate
Conditions | Yield |
---|---|
With pyridine In tetrahydrofuran | 94% |
4-chlorophenyl acetate
rac-1-cyclohexylethanol
(R)-1-cyclohexylethyl acetate
Conditions | Yield |
---|---|
With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; Candida antarctica B lipase; [RuCl2(p-cymene)]2; (E)-2-((1-hydroxy-2-methylpropan-2-ylimino)methyl)phenol In toluene at 70℃; for 72h; Inert atmosphere; Enzymatic reaction; optical yield given as %ee; enantioselective reaction; | 94% |
With Novozym 435; In toluene at 70℃; for 48h; |
Isopropenyl acetate
rac-1-cyclohexylethanol
(R)-1-cyclohexylethyl acetate
Conditions | Yield |
---|---|
With dicarbonylchlorido(pentabenzylcyclopentadienyl)ruthenium; potassium tert-butylate; sodium carbonate In tetrahydrofuran; toluene at 23℃; for 3h; Inert atmosphere; dynamic kinetic resolution; Enzymatic reaction; optical yield given as %ee; enantioselective reaction; | 94% |
With Candida antarctica lipase B; potassium phosphate; C38H24O3Ru In toluene at 50℃; for 20h; Molecular sieve; Inert atmosphere; optical yield given as %ee; enantioselective reaction; | 90% |
With Candida antarctica lipase B; potassium phosphate; C38H24O3Ru In toluene at 50℃; for 20h; Dynamic kinetic resolution; Molecular sieve; Inert atmosphere; Enzymatic reaction; optical yield given as %ee; | 90% |
With Candida antarctica lipase B; potassium tert-butylate; sodium carbonate; [chlorodicarbonyl(η-pentaphenylcyclopentadienyl)]Ru(II) In toluene at 20℃; for 17h; | 98 % Chromat. |
Stage #1: Isopropenyl acetate; rac-1-cyclohexylethanol With Novozym 435 In toluene at 60℃; for 1h; Enzymatic reaction; Stage #2: In toluene at 60℃; for 18h; | n/a |
rac-1-cyclohexylethanol
benzoic acid hydrazide
N′-(1-cyclohexylethyl)benzohydrazide
Conditions | Yield |
---|---|
With nickel(II) triflate; 1,3-bis(dicyclohexylphosphine)propane In tert-Amyl alcohol at 120℃; for 24h; Inert atmosphere; Glovebox; Schlenk technique; Molecular sieve; | 93% |
With nickel(II) triflate; 1,1,1,3',3',3'-hexafluoro-propanol; 1,3-bis(dicyclohexylphosphine)propane In tert-Amyl alcohol at 120℃; for 24h; Inert atmosphere; Schlenk technique; Molecular sieve; Sealed tube; | 93% |
rac-1-cyclohexylethanol
(R)-dichlorprop
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In diethyl ether for 4.5h; Ambient temperature; | 92% |
rac-1-cyclohexylethanol
1,3-dicyclohexylbutan-1-one
Conditions | Yield |
---|---|
With [RuCl2(p-cymene)(iPr2-imy)]; tricyclohexylphosphine tetrafluoroborate; potassium hydroxide In toluene at 110℃; for 24h; Schlenk technique; Inert atmosphere; | 92% |
Conditions | Yield |
---|---|
With (R)-3,3'-bis(2,4,6-triisopropylphenyl)binol phosphoric acid; (C5(CH3)5)Ir(NHCH(C6H5)CH(C6H5)NSO2C6(CH3)5) In tert-Amyl alcohol for 24h; Inert atmosphere; Glovebox; Molecular sieve; Reflux; enantioselective reaction; | 92% |
rac-1-cyclohexylethanol
p-toluenesulfonyl chloride
1-cyclohexylethyl 4-methylbenzenesulfonate
Conditions | Yield |
---|---|
With trimethylamine hydrochloride; triethylamine In dichloromethane at 0℃; Inert atmosphere; | 92% |
With dmap; triethylamine In dichloromethane at 20℃; for 2h; | 86.3% |
Conditions | Yield |
---|---|
With bis-[(trifluoroacetoxy)iodo]benzene In dichloromethane at 20℃; for 2h; Irradiation; | 92% |
Conditions | Yield |
---|---|
With p-toluenesulfonyl chloride at 20℃; for 0.166667h; neat (no solvent); | 91% |
With silica triflate In hexane for 0.0833333h; Heating; | 90% |
rac-1-cyclohexylethanol
Conditions | Yield |
---|---|
phosphomolybdic acid hydrate at 20℃; for 3.25h; | 90% |
Fe(HSO4)3 at 20℃; for 2.5h; | 74% |
Conditions | Yield |
---|---|
Stage #1: 3,4-dihydro-2H-pyran With 2Br3(1-)*C18H36N2O6*2H(1+) In acetonitrile at 20℃; for 0.0166667h; Stage #2: rac-1-cyclohexylethanol In acetonitrile at 20℃; for 0.0666667h; | 90% |
Stage #1: 3,4-dihydro-2H-pyran With C12H24KO6(1+)*Br3H(1-) In acetonitrile at 20℃; for 0.0166667h; Stage #2: rac-1-cyclohexylethanol In acetonitrile at 20℃; for 0.666667h; | 86% |
With Iron(III) nitrate nonahydrate; sodium iodide In dichloromethane at 20℃; for 0.166667h; | 84% |
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