Our Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
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inquirymeso-Tetraphenyl-tetrabenzoporphine palladium complex CAS:119654-64-7 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, special
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiryGMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,
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inquiryHigh quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:Beijing or Guangzhou
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inquiry1.Our services:A.Supply sampleB.The packing also can be according the customers` requirmentC.Any inquiries will be replied within 24 hoursD.we provide Commerical Invoice, Packing List, Bill of loading, COA , Health certificate and Origin certificate.
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inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
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inquiryAppearance:solid or liquid Storage:sealed in cool and dry place Package:As customer's requested Application:Pharma Intermediate Transportation:by courier/air/sea Port:Any port in China
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inquiryMESO-TETRAPHENYL-TETRABENZOPORPHINEAppearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:pharmaceutical intermediate Transportation:by air, by sea, by express
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
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inquiryGood Quality Package:1kg/bag Application:Medical or chemical Transportation:Air/Train/Sea Port:Shenzhen
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inquiryfactory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
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inquiryStrict quality control system and PHD We has passed through the ISO9001:2016 Quality System Certificate, we have strict quality control system. we have about 300 employees, including 90 full-time PHD 15 PHD and masters above, 153 undergraduates, w
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inquiryPalladium,[6,13,20,27-tetraphenyl-29H,31H-tetrabenzo[b,g,l,q]porphinato(2-)-kN29,kN30,kN31,kN32]-, (SP-4-1)- Storage:keep in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/pharma intermediate Transp
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inquirycadmium(II) 5,10,15,20-tetraphenyl tetrabenzoporphyrinate
palladium(II) 5,10,15,20-tetraphenyltetrabenzoporphyrinate
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide for 0.00833333h; Reflux; | 80% |
palladium diacetate
meso-tetraphenyltetrabenzoporphyrin
palladium(II) 5,10,15,20-tetraphenyltetrabenzoporphyrinate
Conditions | Yield |
---|---|
In dichloromethane; N,N-dimethyl-formamide at 150℃; for 1h; | 64% |
In dichloromethane; N,N-dimethyl-formamide at 150℃; for 0.75h; Inert atmosphere; | 47.9% |
meso-tetraphenyltetrabenzoporphyrin
palladium(II) 5,10,15,20-tetraphenyltetrabenzoporphyrinate
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide for 0.0833333h; Reflux; | 25% |
sodium phenylacetate
palladium(II) 5,10,15,20-tetraphenyltetrabenzoporphyrinate
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: water / pH 3.0 2: melt / 1 h / 360 °C / Inert atmosphere 3: hydrogenchloride / dichloromethane; water / 0.5 h 4: dichloromethane; N,N-dimethyl-formamide / 0.75 h / 150 °C / Inert atmosphere View Scheme |
phenylacetic acid
palladium(II) 5,10,15,20-tetraphenyltetrabenzoporphyrinate
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: sodium hydroxide / water / pH 8.0 2: water / pH 3.0 3: melt / 1 h / 360 °C / Inert atmosphere 4: hydrogenchloride / dichloromethane; water / 0.5 h 5: dichloromethane; N,N-dimethyl-formamide / 0.75 h / 150 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1: 1 h / 360 °C / Inert atmosphere 2: hydrogenchloride / dichloromethane; water / 0.75 h 3: dichloromethane; N,N-dimethyl-formamide / 1 h / 150 °C View Scheme |
palladium(II) 5,10,15,20-tetraphenyltetrabenzoporphyrinate
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: melt / 1 h / 360 °C / Inert atmosphere 2: hydrogenchloride / dichloromethane; water / 0.5 h 3: dichloromethane; N,N-dimethyl-formamide / 0.75 h / 150 °C / Inert atmosphere View Scheme |
phenylacetonitrile
palladium(II) 5,10,15,20-tetraphenyltetrabenzoporphyrinate
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: sodium hydroxide / water / 5 h / 115 - 120 °C / Inert atmosphere 2: 1 h / 360 °C / Inert atmosphere 3: hydrogenchloride / dichloromethane; water / 0.75 h 4: dichloromethane; N,N-dimethyl-formamide / 1 h / 150 °C View Scheme |
meso-tetraphenyltetrabenzoporphyrin
palladium(II) 5,10,15,20-tetraphenyltetrabenzoporphyrinate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: N,N-dimethyl-formamide 2: N,N-dimethyl-formamide / 0.01 h / Reflux View Scheme |
palladium(II) 5,10,15,20-tetraphenyltetrabenzoporphyrinate
palladium 2-bromo-6,13,20,27-tetraphenyltetrabenzo[b:g:l:q]porphyrin
Conditions | Yield |
---|---|
With tetramethylammonium bromide In chloroform for 8h; Reflux; regioselective reaction; | 63% |
palladium(II) 5,10,15,20-tetraphenyltetrabenzoporphyrinate
(22,23,72,73,122,123,172,173-octabromo-5,10,15,20-tetraphenyltetrabenzoporphyrinato)palladium(II)
Conditions | Yield |
---|---|
With bromine; tetramethylammonium bromide In chloroform for 4h; Reflux; regioselective reaction; | 46% |
palladium(II) 5,10,15,20-tetraphenyltetrabenzoporphyrinate
bromine
tetramethylammonium bromide
(22,23,72,73,122,123,172,173-octabromo-5,10,15,20-tetraphenyltetrabenzoporphyrinato)palladium(II)
Conditions | Yield |
---|---|
In chloroform soln. of Me4NBr in CHCl3 stirred for 10 min; excess of Br2 added; mixt. stirred for 20 min; soln. of Pd complex in CHCl3 added; mixt. heated for2 h with stirring under reflux; cooled to room temp.; washed (Na2S2O3, H2O, satd. NaCl); dried; evapd. ...; cooled to room temp.; washed (Na2S2O3, H2O, satd. NaCl); org. phase dried (Na2SO4); evapd.; monitored by NMR spectroscopy, mass spectroscopy; | A n/a B 43% |
palladium(II) 5,10,15,20-tetraphenyltetrabenzoporphyrinate
(22,23,72,73,122,123,172,173-octabromo-5,10,15,20-tetraphenyltetrabenzoporphyrinato)palladium(II)
Conditions | Yield |
---|---|
With bromine; tetramethylammonium bromide In chloroform for 4h; Reflux; regioselective reaction; |
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