As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
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inquiryHigh purity 4,4-Difluorocyclohexanecarboxylic acid CAS 122665-97-8 with factory price Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermed
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inquiryColorcom is a global leader in industrial chemical manufacturing and is continuously innovating and transforming to exceed client expectations and industry standards. Colorcom prides itself on superior customer and technical focus, while focusing on
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inquiry4,4-Difluorocyclohexanecarboxylic acid Basic information Product Name: 4,4-Difluorocyclohexanecarboxylic acid Synonyms: 4,4-DIFLUOROCYCLOHEXANECARBOXYLIC ACID;Cyclohexanecarboxylic acid, 4,4-difluoro-;4,4-DIFLUOROCYCLOHEXYLCARBOXYLIC ACID;Marav
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inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
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inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
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inquiry4,4-Difluorocyclohexanecarboxylic acid CAS:122665-97-8 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high q
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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inquiryFast Delivery 122665-97-8 low price 4,4-Difluorocyclohexanecarboxylic acid in stock Molecular Formula C7H10F2O2 Molar Mass 164.15 Density 1.24±0.1 g/cm3(Predicted) Melting Point 103-107 °C
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Min.Order:1 Gram
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquirySourcing Leveraging our vast network of suppliers and local industry expertise we can source quality industrial and speciality chemicals, supporting you through the entire sales cycle to ensure you receive the perfect Chemlyte solution. Market
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiryWe are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
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inquiryEstablished in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site
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inquiryWhy is SINOWAY: 1) Specialized in pharmaceutical and healthcare industrial for 34 years. 2) ISO 9001:2015 & SGS audited supplier . 3) Accept various payment terms : T.T 30-60 days. 4) We have warehouse in USA with quickly shipment . 5) We c
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
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inquiryCAS 122665-97-8 Name 4,4-Difluorocyclohexanecarboxylic Acid Appearance White powder Application Pharmaceutical intermediate Appearance: White powder
Cas:122665-97-8
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inquiryOur Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an
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inquiryProduct Name: 4,4-Difluorocyclohexanecarboxylic acid Synonyms: 4,4-DIFLUOROCYCLOHEXANECARBOXYLIC ACID;Cyclohexanecarboxylic acid, 4,4-difluoro-;4,4-DIFLUOROCYCLOHEXYLCARBOXYLIC ACID;Maraviroc Intermediate 1;4,4-diflurocyclohexane carboxylic aci
Cas:122665-97-8
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inquiryHANGZHOU THINK CHEMICAL CO., LTD. (THINKCHEM) is an integrative corporation of trade, research and contract manufacture. With about ten years of business experiences on the marketing & distribution, thinkchem specializes in exp
ethyl 4,4-difluorocyclohexane-1-carboxylate
4,4-difluorocyclohexanecarboxylic acid
Conditions | Yield |
---|---|
With water; lithium hydroxide In tetrahydrofuran at 20℃; | 97% |
With ethanol; sodium hydroxide at 0 - 20℃; for 18h; | 94% |
With sodium hydroxide In ethanol at 0 - 20℃; for 18h; | 94% |
ethyl 4-oxocyclohexane-1-carboxylate
4,4-difluorocyclohexanecarboxylic acid
Conditions | Yield |
---|---|
With 4-tert-butyl-2,6-dimethylphenylsulfur trifluoride; pyridine hydrogenfluoride In dichloromethane at 0 - 20℃; for 5h; Inert atmosphere; | 27% |
Multi-step reaction with 2 steps 1: diethylaminosulfur trifluoride / CH2Cl2 / 0 °C 2: 65 percent / NaOH / tetrahydrofuran; H2O View Scheme | |
Multi-step reaction with 2 steps 1.1: diethylaminosulfur trifluoride / CH2Cl2 / 0 °C 1.2: OSO4; NMO / acetone; H2O 2.1: 65 percent / NaOH / tetrahydrofuran; H2O View Scheme |
4,4-difluorocyclohexanecarboxylic acid
Conditions | Yield |
---|---|
With hydrogenchloride; water pH=< 1; |
ethyl 4-oxocyclohexane-1-carboxylate
A
4,4-difluorocyclohexanecarboxylic acid
B
4-fluorocyclohex-3-ene-1-carboxylic acid
Conditions | Yield |
---|---|
Stage #1: ethyl 4-oxocyclohexane-1-carboxylate With diethylamino-sulfur trifluoride at -10 - 20℃; for 24h; Inert atmosphere; Large scale; Stage #2: With sodium hydroxide In tetrahydrofuran; ethanol at 0 - 60℃; pH=11; Large scale; |
4,4-difluorocyclohexanecarboxylic acid
4,4-difluorocyclohexane-1-carbonyl chloride
Conditions | Yield |
---|---|
With thionyl chloride In toluene at 92℃; for 2.5h; Inert atmosphere; Large scale; | 100% |
With thionyl chloride In toluene Reflux; | 100% |
With thionyl chloride at 85℃; for 3h; | 98% |
4,4-difluorocyclohexanecarboxylic acid
(4,4-difluorocyclohexyl)methanol
Conditions | Yield |
---|---|
With sodium tetrahydroborate In tetrahydrofuran at 20℃; for 1h; | 98% |
Multi-step reaction with 2 steps 1: sulfuric acid / 16 h / 0 - 70 °C 2: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere View Scheme |
4,4-difluorocyclohexanecarboxylic acid
4-{3-[2-methyl-5-(1-methylethyl)-1H-imidazol-1-yl]-8-azabicyclo[3.2.1]oct-8-yl}-2-phenyl-1-butanamine
trifluoroacetic acid
Conditions | Yield |
---|---|
Stage #1: 4,4-difluorocyclohexanecarboxylic acid With N-ethyl-N,N-diisopropylamine; HATU In dichloromethane at 20℃; for 0.166667h; Inert atmosphere; Stage #2: 4-{3-[2-methyl-5-(1-methylethyl)-1H-imidazol-1-yl]-8-azabicyclo[3.2.1]oct-8-yl}-2-phenyl-1-butanamine In dichloromethane at 20℃; for 18h; Inert atmosphere; Stage #3: trifluoroacetic acid In water; acetonitrile | 96% |
4,4-difluorocyclohexanecarboxylic acid
N-(2-chloro-6-methylphenyl)-2-((2-methyl-6-(piperazin-1-yl)pyrimidin 4-yl)amino)thiazole-5-carboxamide
Conditions | Yield |
---|---|
With dicyclohexyl-carbodiimide; ethyl cyanoglyoxylate-2-oxime In tetrahydrofuran at 63 - 65℃; for 4h; | 96% |
4,4-difluorocyclohexanecarboxylic acid
N,0-dimethylhydroxylamine
4,4-difluoro-N-methoxy-N-methylcyclohexane-1-carboxamide
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; HATU In N,N-dimethyl-formamide at 16℃; for 16h; Concentration; | 95.09% |
With N-ethyl-N,N-diisopropylamine; HATU In N,N-dimethyl-formamide at 16℃; for 16h; | 1.2 g |
4,4-difluorocyclohexanecarboxylic acid
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; | 95% |
4,4-difluorocyclohexanecarboxylic acid
1-hydroxy-pyrrolidine-2,5-dione
2,5-dioxopyrrolidin-1-yl 4,4-difluorocyclohexanecarboxylate
Conditions | Yield |
---|---|
With dicyclohexyl-carbodiimide In tetrahydrofuran at 0 - 20℃; for 1h; | 94% |
Stage #1: 4,4-difluorocyclohexanecarboxylic acid With dicyclohexyl-carbodiimide In tetrahydrofuran at 0 - 20℃; Stage #2: 1-hydroxy-pyrrolidine-2,5-dione In tetrahydrofuran at 20℃; | 94% |
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; for 12h; Inert atmosphere; |
Conditions | Yield |
---|---|
Stage #1: 4,4-difluorocyclohexanecarboxylic acid With N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In dichloromethane at 20℃; for 0.25h; Stage #2: 4-carbethoxypiperidine With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 18h; | 94% |
4,4-difluorocyclohexanecarboxylic acid
2,2,2-trichloroethyl (4,4-difluorocyclohexyl)carbamate
Conditions | Yield |
---|---|
With dmap; copper diacetate In acetonitrile at 80℃; for 3h; Schlenk technique; Sealed tube; | 94% |
4,4-difluorocyclohexanecarboxylic acid
(S)-3-methyl-piperazine-1-carboxylic acid tert-butyl ester
(R)-tert-butyl 4-(4,4-difluorocyclohexanecarbonyl)-3-methylpiperazine-1-carboxylate
Conditions | Yield |
---|---|
With 1-hydroxy-7-aza-benzotriazole; sodium hydrogencarbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide for 15h; | 92% |
4,4-difluorocyclohexanecarboxylic acid
aniline
Conditions | Yield |
---|---|
With tris(2,4-pentanedionato)ruthenium(III); hydrogen; bis(trifluoromethanesulfonyl)amide; [2-((diphenylphospino)methyl)-2-methyl-1,3-propanediyl]bis[diphenylphosphine] In dibutyl ether at 160℃; under 45004.5 Torr; for 18h; Autoclave; | 91% |
4,4-difluorocyclohexanecarboxylic acid
Conditions | Yield |
---|---|
Stage #1: 4,4-difluorocyclohexanecarboxylic acid With thionyl chloride In dichloromethane for 15h; Reflux; Stage #2: (S)-(+)-β-phenyl-β-alanine methyl ester hydrochloride With sodium hydrogencarbonate In dichloromethane; water for 0.5h; Cooling with ice; | 91% |
4,4-difluorocyclohexanecarboxylic acid
methanol
methyl 4,4-difluorocyclohexane-1-carboxylate
Conditions | Yield |
---|---|
With sulfuric acid at 0 - 70℃; for 16h; | 90.82% |
sulfuric acid for 16h; Reflux; |
4,4-difluorocyclohexanecarboxylic acid
Conditions | Yield |
---|---|
With lithium aluminium deuteride In tetrahydrofuran at 20℃; | 88.1% |
4,4-difluorocyclohexanecarboxylic acid
4,4-difluoro-N-[(1S)-3-[(1R,5S)-3-(3-methyl-5-propan-2-yl-1,2,4-triazol-4-yl)-8-azabicyclo[3.2.1]octan-8-yl]-1-phenylpropyl]cyclohexane-1-carboxamide
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In dichloromethane at 0 - 20℃; Inert atmosphere; Molecular sieve; | 87% |
4,4-difluorocyclohexanecarboxylic acid
4,4-difluorocyclohexanecarboxamide
Conditions | Yield |
---|---|
Stage #1: 4,4-difluorocyclohexanecarboxylic acid With 4-methyl-morpholine; carbonochloridic acid, butyl ester In tetrahydrofuran at -70℃; for 0.25h; Inert atmosphere; Stage #2: With ammonium hydroxide In water at 20℃; | 86% |
Stage #1: 4,4-difluorocyclohexanecarboxylic acid With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane at 20℃; for 1.5h; Stage #2: With ammonium hydroxide In tetrahydrofuran for 0.5h; | 77% |
Stage #1: 4,4-difluorocyclohexanecarboxylic acid With 4-methyl-morpholine; isobutyl chloroformate In tetrahydrofuran at -70℃; for 0.5h; Stage #2: With ammonium hydroxide In tetrahydrofuran at 0℃; | 40% |
4,4-difluorocyclohexanecarboxylic acid
(4-{1-amino-3-[3-(3-isopropyl-5-methyl-[1,2,4]triazol-4-yl)-8-azabicyclo[3.2.1]oct-8-yl]propyl}phenyl)carbamic acid tert-butyl ester
(4-{1-(4,4-difluorocyclohexylcarbonylamino)-3-[3-(3-isopropyl-5-methyl-[1,2,4]triazol-4-yl)-8-azabicyclo[3.2.1]oct-8-yl]propyl}phenyl)carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
Stage #1: 4,4-difluorocyclohexanecarboxylic acid With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In dichloromethane for 0.25h; Inert atmosphere; Cooling with ice; Molecular sieve; Stage #2: (4-{1-amino-3-[3-(3-isopropyl-5-methyl-[1,2,4]triazol-4-yl)-8-azabicyclo[3.2.1]oct-8-yl]propyl}phenyl)carbamic acid tert-butyl ester In dichloromethane at 20℃; for 4h; Inert atmosphere; Molecular sieve; | 85% |
4,4-difluorocyclohexanecarboxylic acid
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In dichloromethane for 4h; | 84% |
4,4-difluorocyclohexanecarboxylic acid
trifluoroacetic acid
Conditions | Yield |
---|---|
Stage #1: benzyl 2-{bis[(tert-butoxy)carbonyl]amino}prop-2-enoate With dipotassium hydrogenphosphate; 10-(3,5-dimethoxyphenyl)-9-mesityl-1,3,6,8-tetramethoxyacridin-10-ium tetrafluoroborate In N,N-dimethyl-formamide for 0.333333h; Sealed tube; Inert atmosphere; Stage #2: 4,4-difluorocyclohexanecarboxylic acid In N,N-dimethyl-formamide at 25℃; for 20h; Inert atmosphere; Sealed tube; Irradiation; Stage #3: trifluoroacetic acid In dichloromethane at 25℃; for 1.5h; Sealed tube; | 83% |
Conditions | Yield |
---|---|
With tert-Butyl peroxybenzoate; 9-(2-chlorophenyl)acridine; copper(I) trifluoromethanesulfonate * 1/2 toluene; 1,4-diazabicyclo [2.2.2] octane-1,4-diium-1,4-disulfinate In dichloromethane Irradiation; | 83% |
4,4-difluorocyclohexanecarboxylic acid
C6H4NCH2CHCCH2
Conditions | Yield |
---|---|
With hydrogenchloride; cerium(III) chloride heptahydrate; tetrabutyl-ammonium chloride In 2,2,2-trifluoroethanol; water for 17h; Schlenk technique; Inert atmosphere; Electrochemical reaction; Irradiation; | 82% |
With ammonium peroxydisulfate; [4,4’-bis(1,1-dimethylethyl)-2,2’-bipyridine-N1,N1‘]bis [3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-N]phenyl-C]iridium(III) hexafluorophosphate In dimethyl sulfoxide at 20℃; Irradiation; Inert atmosphere; | 78% |
With bis-[(trifluoroacetoxy)iodo]benzene In acetonitrile at 20℃; for 12h; Inert atmosphere; Irradiation; Schlenk technique; | 67% |
With 2-Picolinic acid; ferrous(II) sulfate heptahydrate; sodium chlorate In water; dimethyl sulfoxide at 20℃; for 24h; Inert atmosphere; Irradiation; | 57% |
4,4-difluorocyclohexanecarboxylic acid
N-hydroxyphthalimide
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 25℃; | 81% |
With dmap; diisopropyl-carbodiimide In dichloromethane for 1h; | 79% |
With dmap; diisopropyl-carbodiimide In dichloromethane at 20℃; for 0.5h; | 76% |
4,4-difluorocyclohexanecarboxylic acid
3-(4-fluorophenyl)-3H-1,2,3-oxadiazol-1-ium-5-olate
Conditions | Yield |
---|---|
With tris(2,2′-bipyrazine-N1,N1′)ruthenium(II) hexafluorophosphate In acetonitrile at 20℃; for 24h; Inert atmosphere; Schlenk technique; Irradiation; Sealed tube; | 81% |
Conditions | Yield |
---|---|
With copper (II)-fluoride; 1,4-diazabicyclo [2.2.2] octane-1,4-diium-1,4-disulfinate; 9-mesitylacridine In dichloromethane Irradiation; | 81% |
Conditions | Yield |
---|---|
With 6,6'-dimethyl-2,2'-bipyridine; nickel(II) bromide trihydrate; di-tert-butyl dicarbonate; sodium iodide; magnesium chloride; zinc In N,N-dimethyl acetamide at 30℃; for 24h; regioselective reaction; | 77% |
4,4-difluorocyclohexanecarboxylic acid
(S)-3-(4-(7-chloroquinolin-4-yl)piperazin-1-yl)-1-phenylpropan-1-amine
N-((S)-3-(4-(7-chloroquinolin-4-yl)piperazin-1-yl)-1-phenylpropyl)-4,4-difluorocyclohexanecarboxamide
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In dichloromethane at 25℃; for 4h; | 76% |
4,4-difluorocyclohexanecarboxylic acid
methyl (2S)-2-amino-3-phenylpropanoate hydrochloride
Conditions | Yield |
---|---|
Stage #1: 4,4-difluorocyclohexanecarboxylic acid With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 0℃; for 0.333333h; Stage #2: methyl (2S)-2-amino-3-phenylpropanoate hydrochloride at 20℃; for 16h; | 76% |
4,4-difluorocyclohexanecarboxylic acid
1,1-bis(phenylsulfonyl)ethylene
Conditions | Yield |
---|---|
With piperazine; 9-(2-chlorophenyl)acridine; tetrakis(acetonitrile)copper(I)tetrafluoroborate In dichloromethane at 25 - 27℃; for 14h; Irradiation; | 76% |
4,4-difluorocyclohexanecarboxylic acid
(S)-3-((1R,3R,5S)-3-(3-isopropyl-5-methyl-4H-1,2,4-triazol-4-yl)-8-azabicyclo[3.2.1]octan-8-yl)-1-phenylpropan-1-amine
maraviroc
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In dichloromethane at 20℃; for 12h; | 75% |
With polimer bound carbodiimide In dichloromethane at 20℃; for 1h; | 49% |
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