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Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe

Benz[cd]indol-2(1H)-one

Cas:130-00-7

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality Benz[Cd]Indol-2(1H)-One supplier in China

Cas:130-00-7

Min.Order:0 Metric Ton

Negotiable

Type:Manufacturers

inquiry

Henan Allgreen Chemical Co.,Ltd

high quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai

Benzo[cd]indol-2(1H)-one

Cas:130-00-7

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

inquiry

Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply Benz[cd]indol-2(1H)-one

Cas:130-00-7

Min.Order:1

Negotiable

Type:Other

inquiry

Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

Factory Price OLED 99% 130-00-7 Benz[cd]indol-2(1H)-one Manufacturer

Cas:130-00-7

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

inquiry

Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

Benz[cd]indol-2(1H)-one

Cas:130-00-7

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

China Gold Supplier CAS 130-00-7 with competitive price

Cas:130-00-7

Min.Order:10 Gram

FOB Price: $146.0 / 176.0

Type:Trading Company

inquiry

Hebei Sankai Chemical Technology Co., Ltd

1. Product advantages High purity, all above 98.5%, no impurities after dissolution We will test each batch to ensure quality OEM and private brand services designed for free Various cap colors available We can also provide MT1 peptide powd

Benz[cd]indol-2(1H)-one

Cas:130-00-7

Min.Order:1 Kilogram

FOB Price: $50.0 / 100.0

Type:Trading Company

inquiry

Henan Sinotech Import&Export Corporation

CAS NO.: 130-00-7 Molecular weight: 169.19 Dried product initial melting point: 173°C Appearance: uniform light yellow powder Purity: ≥96% Moisture: ≤0.5% Use: an intermediate to synthesize vat dyes and organic pigments Appearance:uniform l

1,8-Naphtaholactam

Cas:130-00-7

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Other

inquiry

Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

1,8-Naphthostyril (1,8-Naphtholactam)

Cas:130-00-7

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

inquiry

Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

Benz[cd]indol-2(1H)-one 130-00-7

Cas:130-00-7

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Minstar Chemical Co., Ltd

Product Name: Benz[cd]indol-2(1H)-one CAS: 130-00-7 MF: C11H7NO MW: 169.18 EINECS: 204-973-4 Mol File: 130-00-7.mol Benz[cd]indol-2(1H)-one Structure Benz[cd]indol-2(1H)-one Chemical Properties Melting point 173-178 °C(lit

Benz[cd]indol-2(1H)-one

Cas:130-00-7

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Fonlynn Health Technology Co., Ltd.

Packing: According to customer requirements Delivery time: In stock or depands Port of shipment: Ningbo/Shanghai/Qingdao OEM/ODM:Welcome Sample:We can offer our existing samples at once Appearance:light yellow Powder / Refer to COA Storage:Refe

Benz[cd]indol-2(1H)-one 96.1(HPLC) cas 130-00-7

Cas:130-00-7

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

Our Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con

130-00-7 Benz[cd]indol-2(1H)-one

Cas:130-00-7

Min.Order:1 Kilogram

FOB Price: $15.0 / 50.0

Type:Trading Company

inquiry

Baoji Guokang Healthchem co.,ltd

Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese

Benz[cd]indol-2(1H)-one

Cas:130-00-7

Min.Order:1 Kilogram

FOB Price: $119.0 / 123.0

Type:Trading Company

inquiry

Qingdao Beluga Import and Export Co., LTD

Benz[cd]indol-2(1H)-one CAS:130-00-7 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic int

Benz[cd]indol-2(1H)-one CAS:130-00-7

Cas:130-00-7

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Benz[cd]indol-2(1H)-one

Cas:130-00-7

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Quanhe Biotechnology Co. LTD

1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s

Benz[cd]indol-2(1H)-one

Cas:130-00-7

Min.Order:1 Kilogram

FOB Price: $160.0 / 200.0

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

Benz[cd]indol-2(1H)-one

Cas:130-00-7

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

Benz[cd]indol-2(1H)-one

Cas:130-00-7

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Benz[cd]indol-2(1H)-one

Cas:130-00-7

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

Benz[cd]indol-2(1H)-one

Cas:130-00-7

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

SHANGHAI SYSTEAM BIOCHEM CO., LTD

We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov

1,8-Naphthostyril (1,8-Naphtholactam)

Cas:130-00-7

Min.Order:100 Gram

FOB Price: $100.0 / 2000.0

Type:Lab/Research institutions

inquiry

Henan Tianfu Chemical Co., Ltd.

Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung, LG, Merck, Thermo Fisher Scientific and so o

130-00-7 Benz[cd]indol-2(1H)-one

Cas:130-00-7

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

Benz[cd]indol-2(1H)-one

Cas:130-00-7

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

inquiry

Hangzhou Huarong Pharm Co., Ltd.

We Huarong Pharm can provide Customized Synthesis & Process R&D & APIs and intermediates Production & Quality Research & Registration Application, especially our GMP validation service which complies with SFDA, FDA, WHO and EU EMPA. O

Benz[cd]indol-2(1H)-one

Cas:130-00-7

Min.Order:0

Negotiable

Type:Trading Company

inquiry

TAIZHOU ZHENYU BIOTECHNOLOGY CO., LTD

Zhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed

Benz[cd]indol-2(1H)-one

Cas:130-00-7

Min.Order:1 Kilogram

FOB Price: $2.0

Type:Lab/Research institutions

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

Benz[cd]indol-2(1H)-one

Cas:130-00-7

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

Benz[cd]indol-2(1H)-one

Cas:130-00-7

Min.Order:1 Metric Ton

FOB Price: $1.5

Type:Trading Company

inquiry

Hunan chemfish Pharmaceutical co.,Ltd

Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea

Benz[cd]indol-2(1H)-one

Cas:130-00-7

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Synthetic route

1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl 4-methylbenzenesulfonate
5551-72-4

1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl 4-methylbenzenesulfonate

1,8-naphtholactam
130-00-7

1,8-naphtholactam

Conditions
ConditionsYield
Stage #1: 1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl 4-methylbenzenesulfonate With sodium hydroxide In ethanol; water for 3h; Reflux;
Stage #2: With hydrogenchloride In water at 75℃;
Stage #3: In ethanol; water for 3h; Reflux;
94%
With sodium hydroxide In ethanol; water at 20℃; for 3h; Reflux;83%
With sodium hydroxide In ethanol; water for 3h; Reflux;83%
Stage #1: 1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl 4-methylbenzenesulfonate With sodium hydroxide In ethanol; water for 3h; Reflux;
Stage #2: With hydrogenchloride In ethanol; water at 20℃; for 0.5h;
82%
With water; sodium hydroxide In ethanol for 3h; Reflux;82%
N-hydroxy-1,8-naphthalenedicarboximide
7797-81-1

N-hydroxy-1,8-naphthalenedicarboximide

1,8-naphtholactam
130-00-7

1,8-naphtholactam

Conditions
ConditionsYield
With sodium hydroxide In ethanol; water for 3h; Reflux;94%
With sodium hydroxide In water for 2h; Reflux;91.7%
With p-toluenesulfonyl chloride for 1h; Heating;1.38 g
Multi-step reaction with 2 steps
1.1: 1 h / 95 °C
2.1: sodium hydroxide / ethanol; water / 3 h / Reflux
2.2: 0.5 h / 20 °C
View Scheme
1,8-Naphthalic anhydride
81-84-5

1,8-Naphthalic anhydride

1,8-naphtholactam
130-00-7

1,8-naphtholactam

Conditions
ConditionsYield
Stage #1: 1,8-Naphthalic anhydride With hydroxylamine hydrochloride In pyridine for 1h; Heating;
Stage #2: With p-toluenesulfonyl chloride In pyridine for 1h; Heating; Further stages.;
91%
With hydroxylamine; p-toluenesulfonyl chloride In pyridine Beckmann rearrangement;64%
Multi-step reaction with 2 steps
1.1: hydroxylamine hydrochloride; pyridine / 1 h / Reflux
1.2: 1 h / 80 °C / Reflux
2.1: sodium hydroxide / ethanol; water / 3 h / Reflux
2.2: 75 °C
2.3: 3 h / Reflux
View Scheme
(Z)-2-benzylidene-1,2-dihydrobenzo[cd]indole

(Z)-2-benzylidene-1,2-dihydrobenzo[cd]indole

1,8-naphtholactam
130-00-7

1,8-naphtholactam

Conditions
ConditionsYield
With 3-chloro-benzenecarboperoxoic acid In dichloromethane at 20℃; for 2h;87%
1,2-dichloro-benzene
95-50-1

1,2-dichloro-benzene

1-Naphthyl isocyanate
86-84-0

1-Naphthyl isocyanate

1,8-naphtholactam
130-00-7

1,8-naphtholactam

Conditions
ConditionsYield
AlCl3 In (2S)-N-methyl-1-phenylpropan-2-amine hydrate; water80%
N-(8-(2-oxo-2-phenylethyl)naphthalen-1-yl)quinoline-2-carboxamide

N-(8-(2-oxo-2-phenylethyl)naphthalen-1-yl)quinoline-2-carboxamide

1,8-naphtholactam
130-00-7

1,8-naphtholactam

Conditions
ConditionsYield
With lithium hydroxide monohydrate; dihydrogen peroxide In tetrahydrofuran; water at 0 - 20℃; for 24h;80%
N-(1-naphthalen-1-yl)pyrazine-2-carboxamide
320582-41-0

N-(1-naphthalen-1-yl)pyrazine-2-carboxamide

benzene 1,3,5-triyl triformate

benzene 1,3,5-triyl triformate

1,8-naphtholactam
130-00-7

1,8-naphtholactam

Conditions
ConditionsYield
With triethylamine; silver carbonate; cobalt(II) chloride; Trimethylacetic acid In 1,4-dioxane at 130℃; for 20h; Inert atmosphere; Sealed tube;47%
8-nitro-1-naphthalenecarboxylic acid
2216-13-9

8-nitro-1-naphthalenecarboxylic acid

acetic acid
64-19-7

acetic acid

A

1,8-naphtholactam
130-00-7

1,8-naphtholactam

B

2-methylnaphtho[1,2-d]oxazole-9-carboxylic acid
1384846-98-3

2-methylnaphtho[1,2-d]oxazole-9-carboxylic acid

C

2-oxo-1,2-dihydrobenzo[c,d]indol-6-yl acetate
1384846-99-4

2-oxo-1,2-dihydrobenzo[c,d]indol-6-yl acetate

Conditions
ConditionsYield
With zinc for 1h; Reflux;A 46%
B 12%
C 27%
1,8-Naphthalimide
81-83-4

1,8-Naphthalimide

1,8-naphtholactam
130-00-7

1,8-naphtholactam

Conditions
ConditionsYield
With sodium hydroxide; sodium hypochlorite
Multi-step reaction with 2 steps
1: aqueous NaOH; NaClO
2: NaOH-solution; water / und Erhitzen der Reaktionsloesung mit Essigsaeure
View Scheme
ethanol
64-17-5

ethanol

8-amino-[1]naphthoic acid
129-02-2

8-amino-[1]naphthoic acid

1,8-naphtholactam
130-00-7

1,8-naphtholactam

8-amino-[1]naphthoic acid
129-02-2

8-amino-[1]naphthoic acid

1,8-naphtholactam
130-00-7

1,8-naphtholactam

Conditions
ConditionsYield
With ethanol
With water
With hydrogenchloride; water
8-bromonaphthalene-1-carboxylic acid
1729-99-3

8-bromonaphthalene-1-carboxylic acid

1,8-naphtholactam
130-00-7

1,8-naphtholactam

Conditions
ConditionsYield
With ammonia; water at 150℃;
With ammonium nitrate; ammonia; copper; potassium nitrate Reagens 4:Wasser;
Multi-step reaction with 2 steps
1: aqueous ammonia / 150 °C
2: hydrochloric acid; water
View Scheme
8-cyano-naphthalene-1-sulfonic acid
83-20-5

8-cyano-naphthalene-1-sulfonic acid

1,8-naphtholactam
130-00-7

1,8-naphtholactam

Conditions
ConditionsYield
at 200℃;
at 200℃;
Multi-step reaction with 2 steps
1: potassium hydroxide; water / 150 - 200 °C
View Scheme
8-chlorocarbamoyl-[1]naphthoic acid
112071-06-4

8-chlorocarbamoyl-[1]naphthoic acid

1,8-naphtholactam
130-00-7

1,8-naphtholactam

Conditions
ConditionsYield
With sodium hydroxide; water und Erhitzen der Reaktionsloesung mit Essigsaeure;
8-carbamoyl-naphthalene-1-sulfonic acid

8-carbamoyl-naphthalene-1-sulfonic acid

sodium formate
141-53-7

sodium formate

1,8-naphtholactam
130-00-7

1,8-naphtholactam

8-carbamoyl-naphthalene-1-sulfonic acid

8-carbamoyl-naphthalene-1-sulfonic acid

sodium acetate
127-09-3

sodium acetate

1,8-naphtholactam
130-00-7

1,8-naphtholactam

1-Naphthyl isocyanate
86-84-0

1-Naphthyl isocyanate

1,8-naphtholactam
130-00-7

1,8-naphtholactam

Conditions
ConditionsYield
With aluminium chloride-sodium chloride melt at 155 - 160℃;
Multi-step reaction with 2 steps
1: AlCl3; NaCl / 150 - 160 °C
2: hydrochloric acid; water
View Scheme
AlCl3 In 1,2-dichloro-benzene
With aluminium trichloride; 1,2-dichloro-benzene at 160℃;
5-methoxybenzo[cd]indol-2(1H)-one
408314-99-8

5-methoxybenzo[cd]indol-2(1H)-one

ammonia
7664-41-7

ammonia

1,8-naphtholactam
130-00-7

1,8-naphtholactam

Conditions
ConditionsYield
With sodium
1,8-Naphthalimide
81-83-4

1,8-Naphthalimide

alkali hypobromite

alkali hypobromite

1,8-naphtholactam
130-00-7

1,8-naphtholactam

Conditions
ConditionsYield
in der Waerme;
2-(3-nitro-benzoyloxy)-benz[de]isoquinoline-1,3-dione
111063-75-3

2-(3-nitro-benzoyloxy)-benz[de]isoquinoline-1,3-dione

aqueous KOH-solution

aqueous KOH-solution

A

1,8-naphtholactam
130-00-7

1,8-naphtholactam

B

N-hydroxy-1,8-naphthalenedicarboximide
7797-81-1

N-hydroxy-1,8-naphthalenedicarboximide

C

3-nitrobenzoic acid
121-92-6

3-nitrobenzoic acid

1,8-naphtholactam
130-00-7

1,8-naphtholactam

benzyl chloride
100-44-7

benzyl chloride

1-benzyl-1H-benzo[cd]indol-2-one
22743-02-8

1-benzyl-1H-benzo[cd]indol-2-one

Conditions
ConditionsYield
With sodium hydroxide; butyltrialkylammonium nitrate at 93℃; for 0.25h; Alkylation;99%
1,8-naphtholactam
130-00-7

1,8-naphtholactam

methyl iodide
74-88-4

methyl iodide

1-methylbenz[cd]indole-2(1H)-one
1710-20-9

1-methylbenz[cd]indole-2(1H)-one

Conditions
ConditionsYield
With sodium hydroxide; butyltrialkylammonium nitrate at 80℃; for 0.333333h; Alkylation;99%
Stage #1: 1,8-naphtholactam With sodium hydride In N,N-dimethyl-formamide at 20℃; for 0.25h;
Stage #2: methyl iodide In N,N-dimethyl-formamide at 80℃; for 12h;
94%
With potassium tert-butylate In N,N-dimethyl-formamide for 1.16667h;91%
1 ,6-dibromohexane
629-03-8

1 ,6-dibromohexane

1,8-naphtholactam
130-00-7

1,8-naphtholactam

1-(6-bromohexyl)benzo[cd]indol-2(1H)-one
627078-56-2

1-(6-bromohexyl)benzo[cd]indol-2(1H)-one

Conditions
ConditionsYield
With 1,4-diaza-bicyclo[2.2.2]octane; tetrabutylammomium bromide; potassium carbonate; sodium hydroxide In acetonitrile Microwave irradiation;97%
With tetrabutylammomium bromide; potassium carbonate for 0.00833333h; Microwave irradiation;78%
Stage #1: 1,8-naphtholactam With sodium hydride In N,N-dimethyl-formamide at 60℃; for 1h;
Stage #2: 1 ,6-dibromohexane In N,N-dimethyl-formamide at 110℃; for 3h;
50%
1,8-naphtholactam
130-00-7

1,8-naphtholactam

methyl chloroformate
79-22-1

methyl chloroformate

1-methoxycarbonylbenzo-2-indolone
54264-97-0

1-methoxycarbonylbenzo-2-indolone

Conditions
ConditionsYield
With triethylamine In benzene96%
1,4-butane sultone
1633-83-6

1,4-butane sultone

1,8-naphtholactam
130-00-7

1,8-naphtholactam

1-(4-sulfonatobutyl)-1,2-dihydrobenzo[c,d]indol-2-one, potassium salt
1151666-52-2

1-(4-sulfonatobutyl)-1,2-dihydrobenzo[c,d]indol-2-one, potassium salt

Conditions
ConditionsYield
Stage #1: 1,8-naphtholactam With potassium hydroxide In 1-methyl-pyrrolidin-2-one at 20℃; for 0.5h;
Stage #2: 1,4-butane sultone In 1-methyl-pyrrolidin-2-one at 90℃; for 10h;
96%
Stage #1: 1,8-naphtholactam With potassium hydroxide In 1-methyl-pyrrolidin-2-one at 20℃; for 0.5h;
Stage #2: 1,4-butane sultone In 1-methyl-pyrrolidin-2-one at 90℃; for 10h;
96%
Stage #1: 1,8-naphtholactam With potassium hydroxide In 1-methyl-pyrrolidin-2-one at 20℃; for 0.5h;
Stage #2: 1,4-butane sultone In N,N-dimethyl-formamide at 80℃; for 12h;
96%
With 1-methyl-pyrrolidin-2-one; potassium hydroxide at 23 - 80℃;95%
Stage #1: 1,8-naphtholactam With potassium hydroxide In 1-methyl-pyrrolidin-2-one at 90℃; for 0.5h;
Stage #2: 1,4-butane sultone In 1-methyl-pyrrolidin-2-one at 90℃; for 10h;
95%
1,8-naphtholactam
130-00-7

1,8-naphtholactam

ethyl iodide
75-03-6

ethyl iodide

1-ethylbenzo[cd]indole-2(1H)-one
1830-56-4

1-ethylbenzo[cd]indole-2(1H)-one

Conditions
ConditionsYield
Stage #1: 1,8-naphtholactam With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0℃; for 0.166667h; Inert atmosphere;
Stage #2: ethyl iodide In N,N-dimethyl-formamide; mineral oil at 20℃; Inert atmosphere;
96%
Stage #1: 1,8-naphtholactam With sodium hydride In N,N-dimethyl-formamide at 0℃; for 0.166667h;
Stage #2: ethyl iodide In N,N-dimethyl-formamide at 20℃;
96%
With sodium hydride In N,N-dimethyl-formamide at 0 - 20℃; for 4.5h;92%
1,8-naphtholactam
130-00-7

1,8-naphtholactam

6-bromo-benzo[cd]indol-2(1H)-one
24856-00-6

6-bromo-benzo[cd]indol-2(1H)-one

Conditions
ConditionsYield
With bromine In chloroform at 0 - 20℃; for 24h;95%
With bromine In chloroform at 20℃; for 60h;94%
With bromine In chloroform at 20℃; for 48h; Temperature; Cooling;90.93%
1,8-naphtholactam
130-00-7

1,8-naphtholactam

6-nitrobenzindol-2(1H)-one
34599-42-3

6-nitrobenzindol-2(1H)-one

Conditions
ConditionsYield
With Iron(III) nitrate nonahydrate; copper nitrate hemi(pentahydrate); acetic anhydride; acetic acid at 35℃; for 5h;95%
With aluminum(III) nitrate nonahydrate; bismuth(III) nitrate; acetic anhydride; acetic acid at 35℃; for 6h;92%
With nitric acid; acetic acid for 4h;74%
2-ethylhexyl bromide
18908-66-2

2-ethylhexyl bromide

1,8-naphtholactam
130-00-7

1,8-naphtholactam

1-(2-ethylhexyl)benzo[cd]indol-2(1H)-one

1-(2-ethylhexyl)benzo[cd]indol-2(1H)-one

Conditions
ConditionsYield
With potassium hydroxide In acetonitrile at 80℃; for 48h;95%
1,8-naphtholactam
130-00-7

1,8-naphtholactam

benzo[c,d]indole-2(1H)-thione
4734-98-9

benzo[c,d]indole-2(1H)-thione

Conditions
ConditionsYield
With pyridine; tetraphosphorus decasulfide Reflux;93%
With pyridine; tetraphosphorus decasulfide Reflux;93%
With pyridine; tetraphosphorus decasulfide Reflux;93%
1,8-naphtholactam
130-00-7

1,8-naphtholactam

bromoacetic acid methyl ester
96-32-2

bromoacetic acid methyl ester

C14H11NO3

C14H11NO3

Conditions
ConditionsYield
With potassium hydrogencarbonate In N,N-dimethyl-formamide at 20℃; for 16h;93%
1,8-naphtholactam
130-00-7

1,8-naphtholactam

1-Iodooctane
629-27-6

1-Iodooctane

1-octylbenzo[cd]indol-2(1H)-one

1-octylbenzo[cd]indol-2(1H)-one

Conditions
ConditionsYield
With 18-crown-6 ether; sodium hydroxide In water; 1,2-dichloro-benzene at 120℃; for 1.5h;93%
1,8-naphtholactam
130-00-7

1,8-naphtholactam

bis(triphenylphosphine)platinum(II) dichloride
10199-34-5, 14056-88-3, 15604-36-1

bis(triphenylphosphine)platinum(II) dichloride

dichloromethane
75-09-2

dichloromethane

[(C11H6NO)2Pt(P(C6H5)3)2]*CH2Cl2

[(C11H6NO)2Pt(P(C6H5)3)2]*CH2Cl2

Conditions
ConditionsYield
With NaN(Si(CH3)3)2 In tetrahydrofuran byproducts: HN(SiMe3)2, NaCl; addn. of NaN(SiMe3)2 soln. (THF) to benzo(cd)indol-2(1H)-on soln. (THF),addn. of Au(PPh3)Cl suspn. (THF), 30 min room temp. stirring (Ar); pptn. (hexane), filtration, vac. drying, recrystn. (CHCl3/hexane), elem.anal.;92%
1-bromo-butane
109-65-9

1-bromo-butane

1,8-naphtholactam
130-00-7

1,8-naphtholactam

1-butylbenzo[c,d]indol-2(1H)-one
39273-39-7

1-butylbenzo[c,d]indol-2(1H)-one

Conditions
ConditionsYield
With sodium hydroxide; butyltrialkylammonium nitrate at 90℃; for 0.333333h; Alkylation;91%
1,8-naphtholactam
130-00-7

1,8-naphtholactam

Iododecane
2050-77-3

Iododecane

1-decylbenzindol-2(1H)-one
124596-35-6

1-decylbenzindol-2(1H)-one

Conditions
ConditionsYield
With sodium hydroxide In water; N,N-dimethyl-formamide at 90℃; for 4h;90%
1,8-naphtholactam
130-00-7

1,8-naphtholactam

boron trifluoride diethyl etherate
109-63-7

boron trifluoride diethyl etherate

C23H16BrN3

C23H16BrN3

C34H20BBrF2N4

C34H20BBrF2N4

Conditions
ConditionsYield
Stage #1: 1,8-naphtholactam; C23H16BrN3 In 1,2-dichloro-ethane at 90℃; Inert atmosphere;
Stage #2: boron trifluoride diethyl etherate With triethylamine In toluene at 120℃;
90%
1,8-naphtholactam
130-00-7

1,8-naphtholactam

1-bromo-octane
111-83-1

1-bromo-octane

1-octylbenzo[cd]indol-2(1H)-one

1-octylbenzo[cd]indol-2(1H)-one

Conditions
ConditionsYield
With sodium hydroxide; butyltrialkylammonium nitrate at 93℃; for 0.333333h; Alkylation;89%
formaldehyd
50-00-0

formaldehyd

1,8-naphtholactam
130-00-7

1,8-naphtholactam

1-(2-Methoxyphenyl)piperazine
35386-24-4

1-(2-Methoxyphenyl)piperazine

1-[4-(2-methoxy-phenyl)-piperazin-1-ylmethyl]-1H-benzo[cd]indol-2-one

1-[4-(2-methoxy-phenyl)-piperazin-1-ylmethyl]-1H-benzo[cd]indol-2-one

Conditions
ConditionsYield
In ethanol Heating;88%
1,3-propanesultone
1120-71-4

1,3-propanesultone

1,8-naphtholactam
130-00-7

1,8-naphtholactam

triethylammonium acetate
5204-74-0

triethylammonium acetate

C14H13NO4S*C6H15N

C14H13NO4S*C6H15N

Conditions
ConditionsYield
Stage #1: 1,3-propanesultone; 1,8-naphtholactam With potassium tert-butylate In N,N-dimethyl-formamide at 20℃; for 2.16667h;
Stage #2: triethylammonium acetate In water; acetonitrile
87%
1,8-naphtholactam
130-00-7

1,8-naphtholactam

5-nitrobenzindol-2(1H)-one
65300-69-8

5-nitrobenzindol-2(1H)-one

Conditions
ConditionsYield
With sulfuric acid; nitric acid at 20℃; for 1.5h;85%
1,8-naphtholactam
130-00-7

1,8-naphtholactam

1-Bromo-2-iodobenzene
583-55-1

1-Bromo-2-iodobenzene

C17H10BrNO

C17H10BrNO

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In toluene at 100℃; for 3h; Inert atmosphere;85%
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In toluene at 100℃; for 3h; Inert atmosphere;85%
1,8-naphtholactam
130-00-7

1,8-naphtholactam

1-bromo-2-iodo-4-nitrobenzene
63037-63-8

1-bromo-2-iodo-4-nitrobenzene

C17H9BrN2O3

C17H9BrN2O3

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In toluene at 100℃; for 3h; Inert atmosphere;85%
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In toluene at 100℃; for 3h; Inert atmosphere;85%
1,8-naphtholactam
130-00-7

1,8-naphtholactam

malononitrile
109-77-3

malononitrile

2-(1,2-dihydrobenzo[c,d]indol-2-yliden)malononitrile
118739-11-0

2-(1,2-dihydrobenzo[c,d]indol-2-yliden)malononitrile

Conditions
ConditionsYield
With trichlorophosphate In toluene at 80 - 100℃; for 3h;84.1%
With trichlorophosphate In toluene at 100℃; for 4h; Knoevenagel condensation;83%
With trichlorophosphate In toluene at 100℃; for 4h;83%
With trichlorophosphate In toluene at 80 - 100℃; for 3.5h;71.9%
1,8-naphtholactam
130-00-7

1,8-naphtholactam

(triphenylphosphine)gold(I) chloride
14243-64-2

(triphenylphosphine)gold(I) chloride

[(C11H6NO)AuP(C6H5)3]
527673-01-4

[(C11H6NO)AuP(C6H5)3]

Conditions
ConditionsYield
With NaN(Si(CH3)3)2 In tetrahydrofuran; dichloromethane byproducts: HN(SiMe3)2, NaCl; addn. of NaN(SiMe3)2 soln. (THF) to benzo(cd)indol-2(1H)-on soln. (CH2Cl2), room temp. stirring, addn. of Au(PPh3)Cl soln. (CH2Cl2), (Ar); filtration, vac. evapn., elem. anal.;84%
1,8-naphtholactam
130-00-7

1,8-naphtholactam

N,N-diethylethylenediamine
100-36-7

N,N-diethylethylenediamine

N'-Benzo[cd]indol-2-yl-N,N-diethyl-ethane-1,2-diamine
102146-87-2

N'-Benzo[cd]indol-2-yl-N,N-diethyl-ethane-1,2-diamine

Conditions
ConditionsYield
With titanium tetrachloride In tetrahydrofuran; benzene83%
1,4-dibromo-butane
110-52-1

1,4-dibromo-butane

1,8-naphtholactam
130-00-7

1,8-naphtholactam

1(4-bromo-butyl)benzo[cd]indol-2(1H)-one
627078-54-0

1(4-bromo-butyl)benzo[cd]indol-2(1H)-one

Conditions
ConditionsYield
With potassium carbonate In acetonitrile at 85℃; for 5h;82%
Stage #1: 1,8-naphtholactam With sodium hydride In N,N-dimethyl-formamide at 60℃; for 1h;
Stage #2: 1,4-dibromo-butane In N,N-dimethyl-formamide at 110℃; for 3h;
65%
With sodium hydride In N,N-dimethyl-formamide Alkylation;

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