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DiiodosilaneAppearance:ask Storage:keep in dry and cool condition Package:foil aluminium bag/vacuum packing Application:intermediates Transportation:By express (Door to door) such as FEDEX, DHL, EMS for small amount. By air(airport to airport) or by
Conditions | Yield |
---|---|
In pentane at -70 - 35℃; for 16h; Temperature; Solvent; Inert atmosphere; Large scale; | 77% |
at 40℃; under 1277.21 - 2311.54 Torr; for 0.08h; Temperature; | 45.3 g |
phosphorous
iodosilane
A
diiodosilane
B
P(SiH3)I2
C
monosilane
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: H2; heating in evacuated, sealed tube to 100°C;; |
phosphorus
iodosilane
A
diiodosilane
B
P(SiH3)I2
C
monosilane
Conditions | Yield |
---|---|
byproducts: H2; at 100°C; |
Conditions | Yield |
---|---|
byproducts: H2; at 20°C; | A <1 B n/a C n/a D n/a |
hydrogen iodide
monosilane
A
diiodosilane
B
triiodo silane
C
silicon tetraiodide
D
iodosilane
Conditions | Yield |
---|---|
aluminium(III) iodide In neat (no solvent) reaction at 80°C and 500 Torr;; fractional distillation and condensation;; | |
aluminium(III) iodide In neat (no solvent) reaction at 80°C and 500 Torr;; fractional distillation and condensation;; |
Conditions | Yield |
---|---|
In not given according to Fritz, G., Kummer D., Chem. Ber., 94 (1961) p. 1143; at -40°C; |
Conditions | Yield |
---|---|
In toluene at 20 - 29℃; for 18h; Temperature; Solvent; |
diiodosilane
bis(trifluoromethylseleno)mercury
bis(trifluoromethylseleno)silane
Conditions | Yield |
---|---|
In decalin stirring, 20°C, 1 h; | 78% |
diiodosilane
2S-benzyloxymethyl-4S acetoxy-1,3 dioxolane
B
2S-benzyloxymethyl-4S-iodo-1,3 dioxolane
Conditions | Yield |
---|---|
In dichloromethane; toluene |
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: SiH4, Si2H6, H2; at ambient temp.;; | |
In neat (no solvent) byproducts: SiH4, Si2H6, H2; at ambient temp.;; |
Conditions | Yield |
---|---|
In neat (no solvent) | 0% |
Conditions | Yield |
---|---|
In neat (no solvent) | 0% |
Conditions | Yield |
---|---|
In benzene under Ar; H2SiI2 is added to a slurry of Ag2Se in benzene, refluxed for5 d; filtd., the filtrate is distd.; |
Conditions | Yield |
---|---|
In diethyl ether excess of Na(Co(CO)4), -23°C; |
Conditions | Yield |
---|---|
In benzene HgSe, benzene and H2SiI2 are condensed into a tube at -196°C, warmed to room temp., heated to 120°C, filtd. under inert gas, benzene is evapd., the residue is warmed to 40°C, benzene is added, evacuated, warmed (40°C, 24 h); cooled to -10°C, elem. anal.; |
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