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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality 5,6-Diamino-1,10-Phenanthroline

Cas:168646-54-6

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 5,6-Diamino-1,10-Phenanthroline

Cas:168646-54-6

Min.Order:1

Negotiable

Type:Other

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Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

Factory Price OLED 99% 168646-54-6 5,6-diamino-1,10-phenanthroline Manufacturer

Cas:168646-54-6

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

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Dayang Chem (Hangzhou) Co.,Ltd.

Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities

5,6-DIAMINO-1,10-PHENANTHROLINE

Cas:168646-54-6

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Factory direct supply CAS 168646-54-6 with best quality

Cas:168646-54-6

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Hebei Sankai Chemical Technology Co., Ltd

1. Product advantages ♦ High purity, all above 98.5%, no impurities after dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available ♦ W

5,6-Diamino-1,10-phenanthroline CAS168646-54-6

Cas:168646-54-6

Min.Order:1 Kilogram

FOB Price: $5.0 / 9.0

Type:Trading Company

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Henan Sinotech Import&Export Corporation

Product Name 5,6-diamino-1,10-phenanthroline Structural formula CAS No. 168646-54-6 mp:>350°C(lit.) purity:>95% inventory condition: spot Appearance:White powder Storage:Store in coo

5,6-diamino-1,10-phenanthroline

Cas:168646-54-6

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Other

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Hebei Nengqian Chemical Import and Export Co., LTD

Our Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con

5,6-Diamino-1,10-phenanthroline CAS:168646-54-6

Cas:168646-54-6

Min.Order:1 Kilogram

FOB Price: $1.0 / 10.0

Type:Trading Company

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

5,6-Diamino-1,10-phenanthroline 168646-54-6

Cas:168646-54-6

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Shanghai Minstar Chemical Co., Ltd

Product Name: 5,6-diamino-1,10-phenanthroline CAS: 168646-54-6 MF: C12H10N4 MW: 210.23 EINECS: Product Categories: Mol File: 168646-54-6.mol 5,6-diamino-1,10-phenanthroline Structure 5,6-diamino-1,10-phenanthroline Chemical P

5,6-diamino-1,10-phenanthroline

Cas:168646-54-6

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Qingdao Beluga Import and Export Co., LTD

5,6-diamino-1,10-phenanthroline CAS:168646-54-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality

5,6-diamino-1,10-phenanthroline CAS:168646-54-6

Cas:168646-54-6

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

5,6-Diamino-1,10-phenanthroline

Cas:168646-54-6

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

5,6-Diamino-1,10-phenanthroline

Cas:168646-54-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

5,6-Diamino-1,10-Phenanthroline

Cas:168646-54-6

Min.Order:0

Negotiable

Type:Manufacturers

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

5,6-Diamino-1,10-phenanthroline

Cas:168646-54-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

5,6-Diamino-1,10-Phenanthroline

Cas:168646-54-6

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

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Jiangsu Qianyu Molecular Technology Co., LTD.

Our Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an

Best Offer5,6-Diamino-1,10-phenanthroline

Cas:168646-54-6

Min.Order:0

Negotiable

Type:Trading Company

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Xiamen Jenny Chemical Technology Co., Ltd.

GMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,

5,6-diamino-1,10-phenanthroline

Cas:168646-54-6

Min.Order:1 Milligram

Negotiable

Type:Trading Company

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EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

5,6-Diamino-1,10-Phenanthroline

Cas:168646-54-6

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

5,6-Diamino-1,10-Phenanthroline

Cas:168646-54-6

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

5,6-Diamino-1,10-Phenanthroline

Cas:168646-54-6

Min.Order:1 Metric Ton

FOB Price: $1.5

Type:Trading Company

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Hunan chemfish Pharmaceutical co.,Ltd

Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea

5,6-diamino-1,10-phenanthroline

Cas:168646-54-6

Min.Order:0

Negotiable

Type:Manufacturers

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Suzhou Health Chemicals Co., Ltd.

High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use

5,6-Diamino-1,10-phenanthroline

Cas:168646-54-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Golden Pharma Co., Limited

GOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation

5,6-Diamino-1,10-phenanthroline

Cas:168646-54-6

Min.Order:1 Kilogram

Negotiable

Type:Other

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Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

5,6-Diamino-1,10-Phenanthroline

Cas:168646-54-6

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Trading Company

inquiry

Hebei Mojin Biotechnology Co.,Ltd

1, High quality with competitive price:2, Fast and safe delivery3.Excellent pre-sales and after-sales service4. Well-trained and professional technologist and sales with rich experience in the field for 5-10 yearsAppearance:see detailed specification

5,6-Diamino-1,10-phenanthroline

Cas:168646-54-6

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Win-Win chemical Co.Ltd

Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

5,6-Diamino-1,10-phenanthroline cas no. 168646-54-6 95%

Cas:168646-54-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

GIHI CHEMICALS CO.,LIMITED

Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe

5,6-diamino-1,10-phenanthroline

Cas:168646-54-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

JINHUA HUAYI CHEMICAL CO., LTD.

Jinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands

5,6-Diamino-1,10-Phenanthroline

Cas:168646-54-6

Min.Order:100 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Acmec Biochemical Technology Co., Ltd.

Acmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea

Acmec 5,6-Diamino-1,10-phenanthroline 1g

Cas:168646-54-6

Min.Order:1 bottle

Negotiable

Type:Lab/Research institutions

inquiry

Synthetic route

1,10-phenanthroline-5,6-dioxime

1,10-phenanthroline-5,6-dioxime

1,10-o-phenanthroline-5,6-diamine
168646-54-6

1,10-o-phenanthroline-5,6-diamine

Conditions
ConditionsYield
With hydrogen; palladium on activated charcoal In ethanol at 20℃; under 3750.3 Torr; for 24h;89%
1,10-phenanthroline-5,6-dione dioxime

1,10-phenanthroline-5,6-dione dioxime

1,10-o-phenanthroline-5,6-diamine
168646-54-6

1,10-o-phenanthroline-5,6-diamine

Conditions
ConditionsYield
With sodium dithionite In ammonium hydroxide; ethanol at 85℃; for 0.75h;86%
With palladium 10% on activated carbon; hydrazine In ethanol at 70℃; for 3h;82%
Stage #1: 1,10-phenanthroline-5,6-dione dioxime With palladium on activated charcoal; hydrazine In ethanol at 70℃; for 24h; Inert atmosphere;
Stage #2: With sodium dithionite; ammonia In ethanol for 0.75h; Reflux;
78%
5-amino-6-nitro-1,10-phenanthroline
168646-53-5

5-amino-6-nitro-1,10-phenanthroline

1,10-o-phenanthroline-5,6-diamine
168646-54-6

1,10-o-phenanthroline-5,6-diamine

Conditions
ConditionsYield
With hydrazine hydrate; palladium on activated charcoal83%
With hydrazine hydrate; palladium on activated charcoal In ethanol for 2h; Heating;65%
With palladium 10% on activated carbon; hydrazine hydrate In 1,4-dioxane; ethanol for 1.5h;22%
(5E,6Z)-1,10-phenanthroline-5,6-dione dioxime

(5E,6Z)-1,10-phenanthroline-5,6-dione dioxime

1,10-o-phenanthroline-5,6-diamine
168646-54-6

1,10-o-phenanthroline-5,6-diamine

Conditions
ConditionsYield
With hydrazine hydrate; palladium on activated charcoal In ethanol for 12h; Heating;83%
phenanthrene-9,10-dione dioxime
14090-76-7

phenanthrene-9,10-dione dioxime

1,10-o-phenanthroline-5,6-diamine
168646-54-6

1,10-o-phenanthroline-5,6-diamine

Conditions
ConditionsYield
With palladium on activated charcoal; hydrazine In ethanol Reflux;70%
1,10-phenanthroline-5,6-dione
27318-90-7

1,10-phenanthroline-5,6-dione

1,10-o-phenanthroline-5,6-diamine
168646-54-6

1,10-o-phenanthroline-5,6-diamine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 83 percent / Na2CO3; NH2OH*HCl / ethanol / 5 h / Heating
2: 89 percent / H2 / Pd/C / ethanol / 24 h / 20 °C / 3750.3 Torr
View Scheme
Multi-step reaction with 2 steps
1: 95 percent / NH2OH*HCl, BaCO3 / ethanol / 12 h / Heating
2: 83 percent / hydrazine hydrate / 10percent Pd/C / ethanol / 12 h / Heating
View Scheme
Multi-step reaction with 2 steps
1: hydroxylamine hydrochloride; barium carbonate / ethanol
2: hydrazine hydrate / ethanol
View Scheme
5-Nitro-1,10-phenanthroline
4199-88-6

5-Nitro-1,10-phenanthroline

1,10-o-phenanthroline-5,6-diamine
168646-54-6

1,10-o-phenanthroline-5,6-diamine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: hydroxylamine hydrochloride / ethanol / Heating
View Scheme
Multi-step reaction with 2 steps
1: NH3, KMnO4 / 2 h / -29 °C
2: 65 percent / N2H4*H2O / Pd/C / ethanol / 2 h / Heating
View Scheme
Multi-step reaction with 2 steps
1: hydroxylamine hydrochloride; potassium hydroxide / ethanol / Reflux
2: palladium on activated charcoal; hydrazine
View Scheme
1,10-Phenanthroline
66-71-7

1,10-Phenanthroline

1,10-o-phenanthroline-5,6-diamine
168646-54-6

1,10-o-phenanthroline-5,6-diamine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 85 percent / H2SO4, HNO3, NaBr / 100 °C
2: 95 percent / NH2OH*HCl, BaCO3 / ethanol / 12 h / Heating
3: 83 percent / hydrazine hydrate / 10percent Pd/C / ethanol / 12 h / Heating
View Scheme
Δ-[(bpy)2Ru(pq)]*2PF6

Δ-[(bpy)2Ru(pq)]*2PF6

1,10-o-phenanthroline-5,6-diamine
168646-54-6

1,10-o-phenanthroline-5,6-diamine

Δ-[Ru(2,2'-bipyridine)2(tetrapyrido[3,2-a:2',3'-c:3'',2''-h:2''',3'''-j]phenazine)][PF6]2*1.5H2O

Δ-[Ru(2,2'-bipyridine)2(tetrapyrido[3,2-a:2',3'-c:3'',2''-h:2''',3'''-j]phenazine)][PF6]2*1.5H2O

Conditions
ConditionsYield
In methanol; acetonitrile under Ar atm. to refluxing soln. Ru complex in MeCN was added soln. phendiamine in MeOH and stirred at 80°C for 6 h; react. mixt. was cooled to room temp. and filtered, solvent was removed in vacuo, residue was triturated with MeCN, filtered, and evapd. to dryness; elem. anal.;99%
[Ru(2,2'-bipyridine)2(1,10-phenanthroline-5,6-dione)](PF6)2

[Ru(2,2'-bipyridine)2(1,10-phenanthroline-5,6-dione)](PF6)2

1,10-o-phenanthroline-5,6-diamine
168646-54-6

1,10-o-phenanthroline-5,6-diamine

Λ-[Ru(2,2'-bipyridine)2(tetrapyrido[3,2-a:2',3'-c:3'',2''-h:2''',3'''-j]phenazine)][PF6]2*1.5H2O

Λ-[Ru(2,2'-bipyridine)2(tetrapyrido[3,2-a:2',3'-c:3'',2''-h:2''',3'''-j]phenazine)][PF6]2*1.5H2O

Conditions
ConditionsYield
In methanol; acetonitrile under Ar atm. to refluxing soln. Ru complex in MeCN was added soln. phendiamine in MeOH and stirred at 80°C for 6 h; react. mixt. was cooled to room temp. and filtered, solvent was removed in vacuo, residue was triturated with MeCN, filtered, and evapd. to dryness; elem. anal.;96%
1,8-Naphthalic anhydride
81-84-5

1,8-Naphthalic anhydride

1,10-o-phenanthroline-5,6-diamine
168646-54-6

1,10-o-phenanthroline-5,6-diamine

C24H12N4O

C24H12N4O

Conditions
ConditionsYield
With acetic acid at 140℃; for 24h; Inert atmosphere;94%
ammonium hexafluorophosphate

ammonium hexafluorophosphate

[(1,10-phenanthroline-5,6-dione)bis(2.2'-bipyridyl)ruthenium(II)] dichloride

[(1,10-phenanthroline-5,6-dione)bis(2.2'-bipyridyl)ruthenium(II)] dichloride

1,10-o-phenanthroline-5,6-diamine
168646-54-6

1,10-o-phenanthroline-5,6-diamine

[Ru(2,2'-bipyridine)2(tetrapyrido[3,2-a:2',3'-c:3'',2''-h:2''',3'''-j]phenazine)](PF6)2

[Ru(2,2'-bipyridine)2(tetrapyrido[3,2-a:2',3'-c:3'',2''-h:2''',3'''-j]phenazine)](PF6)2

Conditions
ConditionsYield
Stage #1: [(1,10-phenanthroline-5,6-dione)bis(2.2'-bipyridyl)ruthenium(II)] dichloride; 1,10-o-phenanthroline-5,6-diamine In methanol; acetonitrile for 6h; Reflux; Inert atmosphere;
Stage #2: ammonium hexafluorophosphate In water; acetonitrile at 20℃; for 0.5h;
93%
benzaldehyde
100-52-7

benzaldehyde

1,10-o-phenanthroline-5,6-diamine
168646-54-6

1,10-o-phenanthroline-5,6-diamine

2-phenyl-1H-imidazo[4,5-f ][1,10]phenanthroline
171565-44-9

2-phenyl-1H-imidazo[4,5-f ][1,10]phenanthroline

Conditions
ConditionsYield
With acetic acid In ethanol; toluene for 6h; Inert atmosphere; Reflux;91.55%
With acetic acid In ethanol; toluene for 6h; Inert atmosphere; Reflux;91.55%
With acetic acid In ethanol; toluene for 6h; Inert atmosphere; Reflux;91.55%
ammonium hexafluorophosphate

ammonium hexafluorophosphate

[Os(2,2'-bipyridine)2(1,10-phenanthroline-5,6-dione)](PF6)2

[Os(2,2'-bipyridine)2(1,10-phenanthroline-5,6-dione)](PF6)2

1,10-o-phenanthroline-5,6-diamine
168646-54-6

1,10-o-phenanthroline-5,6-diamine

[(2,2'-bipyridine)2Os(tetrapyrido[3,2-a:2',3'-c:3'',2''-h:2''',3'''-j]phenazine)](PF6)2 * 5 H2O

[(2,2'-bipyridine)2Os(tetrapyrido[3,2-a:2',3'-c:3'',2''-h:2''',3'''-j]phenazine)](PF6)2 * 5 H2O

Conditions
ConditionsYield
In methanol; acetonitrile addn. of 2 equiv. diaminophenanthroline (in MeOH) to Os-complex (in boiling MeCN), heating to 80°C for 6 h, cooling to room temp., filtration, washing of residue (MeCN), pptn. on addn. of concd. aq. NH4PF6 to filtrate; collection (filtration), washing (water, EtOH, Et2O), drying (vac.); elem. anal.;90%
1,10-o-phenanthroline-5,6-diamine
168646-54-6

1,10-o-phenanthroline-5,6-diamine

pyrene-4,5-dione
6217-22-7

pyrene-4,5-dione

C28H16N4

C28H16N4

Conditions
ConditionsYield
In ethanol for 8h; Reflux;90%
1,10-o-phenanthroline-5,6-diamine
168646-54-6

1,10-o-phenanthroline-5,6-diamine

[1,2,5]selenadiazole[3,4-f][1,10]phenanthroline
1263320-32-6

[1,2,5]selenadiazole[3,4-f][1,10]phenanthroline

Conditions
ConditionsYield
With selenium(IV) oxide In ethanol; water for 1h; Reflux;90%
With selenium(IV) oxide In ethanol at 90℃; for 6h;67.3%
With selenium(IV) oxide In ethanol for 6h; Reflux;67.8%
With selenium(IV) oxide In ethanol for 6h; Reflux;
2,3-dihydroxybenzaldehyde
24677-78-9

2,3-dihydroxybenzaldehyde

1,10-o-phenanthroline-5,6-diamine
168646-54-6

1,10-o-phenanthroline-5,6-diamine

3-(1H-imidazo[4,5-f][1,10]phenanthrolin-2-yl)benzene-1,2-diol

3-(1H-imidazo[4,5-f][1,10]phenanthrolin-2-yl)benzene-1,2-diol

Conditions
ConditionsYield
In ethanol at 70 - 80℃; for 24h;89%
1,10-o-phenanthroline-5,6-diamine
168646-54-6

1,10-o-phenanthroline-5,6-diamine

C24H26O4

C24H26O4

12,15-dimethoxy-10b,16b-dimethyl-10,10a,10b,10c,11,16,16a,16b,16c,17-decahydro-10,17:11,16-dimethanonaphtho<2'',3'':3',4'>cyclobuta<1',2':3,4>cyclobuta<1,2-I>dipyrido<3,2-a:2',3'-c>phenazine

12,15-dimethoxy-10b,16b-dimethyl-10,10a,10b,10c,11,16,16a,16b,16c,17-decahydro-10,17:11,16-dimethanonaphtho<2'',3'':3',4'>cyclobuta<1',2':3,4>cyclobuta<1,2-I>dipyrido<3,2-a:2',3'-c>phenazine

Conditions
ConditionsYield
In ethanol; chloroform for 4h; Heating; in the dark;88%
3,8-bis(4-tert-butyl-phenyl)-1,10-phenanthroline-5,6-dione

3,8-bis(4-tert-butyl-phenyl)-1,10-phenanthroline-5,6-dione

1,10-o-phenanthroline-5,6-diamine
168646-54-6

1,10-o-phenanthroline-5,6-diamine

3,16-di(4-tert-butyl-phenyl)-tetrapyridophenazine

3,16-di(4-tert-butyl-phenyl)-tetrapyridophenazine

Conditions
ConditionsYield
In methanol for 48h; Reflux; Inert atmosphere;88%
rhenium(I) pentacarbonyl chloride
14099-01-5

rhenium(I) pentacarbonyl chloride

1,10-o-phenanthroline-5,6-diamine
168646-54-6

1,10-o-phenanthroline-5,6-diamine

fac-Re(5,6-diamino-1,10-phenanthroline)(CO)3Cl

fac-Re(5,6-diamino-1,10-phenanthroline)(CO)3Cl

Conditions
ConditionsYield
In toluene for 18h; Reflux;88%
2-chloro-1,3-dimethylimidazolinium chloride
37091-73-9

2-chloro-1,3-dimethylimidazolinium chloride

1,10-o-phenanthroline-5,6-diamine
168646-54-6

1,10-o-phenanthroline-5,6-diamine

C22H26N8

C22H26N8

Conditions
ConditionsYield
With triethylamine In acetonitrile for 6h; Cooling with ice; Reflux; Inert atmosphere; Schlenk technique;88%
1,10-o-phenanthroline-5,6-diamine
168646-54-6

1,10-o-phenanthroline-5,6-diamine

o-phthalic dicarboxaldehyde
643-79-8

o-phthalic dicarboxaldehyde

isoindolylimidazo[4,5,f][1,10]phenanthroline

isoindolylimidazo[4,5,f][1,10]phenanthroline

Conditions
ConditionsYield
Stage #1: 1,10-o-phenanthroline-5,6-diamine With hydrogenchloride In ethanol; water at 80℃; for 1h;
Stage #2: o-phthalic dicarboxaldehyde In ethanol; water for 8h; Reflux;
88%
1,10-o-phenanthroline-5,6-diamine
168646-54-6

1,10-o-phenanthroline-5,6-diamine

1,6-bis(N,N-dimethylaminophenyl)hexa-1,5-diyne-3,4-dione

1,6-bis(N,N-dimethylaminophenyl)hexa-1,5-diyne-3,4-dione

6,7-bis(dimetylphenylsilylethynyl)pyrazino[2,3-f][1,10]phenanthroline

6,7-bis(dimetylphenylsilylethynyl)pyrazino[2,3-f][1,10]phenanthroline

Conditions
ConditionsYield
In acetic acid at 20℃; for 1h;87%
1,10-o-phenanthroline-5,6-diamine
168646-54-6

1,10-o-phenanthroline-5,6-diamine

2,4-Dihydroxybenzaldehyde
95-01-2

2,4-Dihydroxybenzaldehyde

4-(1H-imidazo[4,5-f][1,10]phenanthrolin-2-yl)benzene-1,3-diol

4-(1H-imidazo[4,5-f][1,10]phenanthrolin-2-yl)benzene-1,3-diol

Conditions
ConditionsYield
In ethanol at 70 - 80℃; for 24h;85%
4-morpholinonaphthalene-1,2-dione
4569-83-9

4-morpholinonaphthalene-1,2-dione

1,10-o-phenanthroline-5,6-diamine
168646-54-6

1,10-o-phenanthroline-5,6-diamine

4-(benzo[h]dipyrido[3,2-a:2',3'-c]phenazin-14-yl)morpholine

4-(benzo[h]dipyrido[3,2-a:2',3'-c]phenazin-14-yl)morpholine

Conditions
ConditionsYield
With acetic acid In methanol Reflux;84.03%
2,3-dioxo-5,10,15,20-tetramesitylchlorin
1160942-39-1

2,3-dioxo-5,10,15,20-tetramesitylchlorin

1,10-o-phenanthroline-5,6-diamine
168646-54-6

1,10-o-phenanthroline-5,6-diamine

(pyrazo[5′,6′-e]-1′,10′-phenanthroline)[b]meso-tetramesitylporphyrin-phenanthroline

(pyrazo[5′,6′-e]-1′,10′-phenanthroline)[b]meso-tetramesitylporphyrin-phenanthroline

Conditions
ConditionsYield
With trifluoroacetic acid In dichloromethane Inert atmosphere; Reflux;84%
N,N,N',N'-tetramethylchlorformamidinium chloride
56043-45-9, 13829-06-6

N,N,N',N'-tetramethylchlorformamidinium chloride

1,10-o-phenanthroline-5,6-diamine
168646-54-6

1,10-o-phenanthroline-5,6-diamine

C22H30N8

C22H30N8

Conditions
ConditionsYield
With triethylamine In acetonitrile for 6h; Cooling with ice; Reflux; Inert atmosphere; Schlenk technique;84%
1,10-o-phenanthroline-5,6-diamine
168646-54-6

1,10-o-phenanthroline-5,6-diamine

1,4-Dibromo-butane-2,3-dione
6305-43-7

1,4-Dibromo-butane-2,3-dione

2,3-bis(bromomethyl)pyrazino[2,3-f][1,10]phenanthroline

2,3-bis(bromomethyl)pyrazino[2,3-f][1,10]phenanthroline

Conditions
ConditionsYield
In methanol for 5h; Heating;83%
di-tert-butyl dicarbonate
24424-99-5

di-tert-butyl dicarbonate

1,10-o-phenanthroline-5,6-diamine
168646-54-6

1,10-o-phenanthroline-5,6-diamine

tert-butyl (6-amino-1,10-phenanthrolin-5-yl)carbamate

tert-butyl (6-amino-1,10-phenanthrolin-5-yl)carbamate

Conditions
ConditionsYield
In methanol; dichloromethane at 20℃; for 24h;83%
4--1,2-naphthoquinone
123135-53-5

4--1,2-naphthoquinone

1,10-o-phenanthroline-5,6-diamine
168646-54-6

1,10-o-phenanthroline-5,6-diamine

4-(benzo[h]dipyrido[3,2-a:2',3'-c]phenazin-14-yl)-N,N-diethylaniline

4-(benzo[h]dipyrido[3,2-a:2',3'-c]phenazin-14-yl)-N,N-diethylaniline

Conditions
ConditionsYield
With acetic acid In methanol Reflux;82.23%
3,5-di-tert-butyl-2-hydroxybenzaldehyde
37942-07-7

3,5-di-tert-butyl-2-hydroxybenzaldehyde

1,10-o-phenanthroline-5,6-diamine
168646-54-6

1,10-o-phenanthroline-5,6-diamine

N,N'-bis(3,5-di-tert-butylsalicylidene)-5,6-(1,10-phenanthroline)diamine

N,N'-bis(3,5-di-tert-butylsalicylidene)-5,6-(1,10-phenanthroline)diamine

Conditions
ConditionsYield
With orthoformic acid triethyl ester In ethanol for 2h; Heating;81%
1,10-o-phenanthroline-5,6-diamine
168646-54-6

1,10-o-phenanthroline-5,6-diamine

5-(4-nitrophenylazo)salicylaldehyde
32041-64-8

5-(4-nitrophenylazo)salicylaldehyde

2-(1H-imidazo[4,5-f][1,10]phenanthrolin-2-yl)-4-((4-nitrophenyl)diazenyl)phenol

2-(1H-imidazo[4,5-f][1,10]phenanthrolin-2-yl)-4-((4-nitrophenyl)diazenyl)phenol

Conditions
ConditionsYield
In ethanol for 8h; Reflux;81%
1-(chloro(piperidin-1-yl)methylene)piperidin-1-ium chloride
95072-47-2

1-(chloro(piperidin-1-yl)methylene)piperidin-1-ium chloride

1,10-o-phenanthroline-5,6-diamine
168646-54-6

1,10-o-phenanthroline-5,6-diamine

C34H46N8

C34H46N8

Conditions
ConditionsYield
With triethylamine In acetonitrile for 6h; Cooling with ice; Reflux; Inert atmosphere; Schlenk technique;81%
tetrakis(acetonitrile)copper(I) perchlorate
14057-91-1

tetrakis(acetonitrile)copper(I) perchlorate

dichloromethane
75-09-2

dichloromethane

1,10-o-phenanthroline-5,6-diamine
168646-54-6

1,10-o-phenanthroline-5,6-diamine

bis[2-(diphenylphosphino)phenyl] ether
166330-10-5

bis[2-(diphenylphosphino)phenyl] ether

C48H38CuN4OP2(1+)*ClO4(1-)*2.5CH2Cl2

C48H38CuN4OP2(1+)*ClO4(1-)*2.5CH2Cl2

Conditions
ConditionsYield
at 20℃; for 1h; Inert atmosphere; Schlenk technique;81%

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