CAS No.100-52-7,Benzaldehyde Suppliers,MSDS download

: 292638-84-7
styrene

: 100-52-7
benzaldehyde

Conditions

Conditions	Yield
With sodium periodate; C31H29Br2N3Ru*CH2Cl2 In water; ethyl acetate; acetonitrile at 25℃; for 0.5h; Activation energy; Reagent/catalyst; Solvent; Temperature; Inert atmosphere; Schlenk technique;	100%
With ruthenium trichloride; [bis(acetoxy)iodo]benzene In dichloromethane; water at 30℃; for 1.5h; Catalytic behavior; Reagent/catalyst; Solvent;	99.8%
With sodium periodate; C22H23ClIN2Os(1+)*F6P(1-) In water; tert-butyl alcohol at 60℃; Catalytic behavior; Reagent/catalyst; Schlenk technique; Inert atmosphere;	97%

: 588-59-0
stilbene

: 100-52-7
benzaldehyde

Conditions

Conditions	Yield
With oxygen In dichloromethane at 20℃; for 2h; visible light irradiation;	100%
With sodium periodate; [η5-C5H5Ru(CO)2NH2C6H11]BF4 In water; acetonitrile at 60℃; for 1h; Catalytic behavior; Schlenk technique; Inert atmosphere;	100%
With dihydrogen peroxide In acetonitrile at 65℃; for 6h;	96%

: 611-71-2, 611-72-3, 17199-29-0, 90-64-2
MANDELIC ACID

: 100-52-7
benzaldehyde

Conditions

Conditions	Yield
With dinitratocerium (IV) chromate In benzene for 0.666667h; Heating;	100%
With tris paraperiodate In benzene for 1.5h; Heating;	100%
With pyridine chromium peroxide In dichloromethane for 0.25h; Product distribution; Ambient temperature; effect of various chromium(VI) based oxidants;	100%

: 108-88-3
toluene

: 100-52-7
benzaldehyde

Conditions

Conditions	Yield
With laccase from Coriolus versicolor MTCC-138; 2,2'-azino-bis(3-ethylbenzothiazoline-6-sulfonic acid) diammonium salt In 1,4-dioxane for 0.5h; pH=4.5; Green chemistry; Enzymatic reaction;	100%
With nickel-doped graphene carbon nitride nanoparticles; air In ethanol at 25℃; for 8h; Reagent/catalyst; Solvent; Irradiation; Green chemistry;	98%
With water at 20℃; for 3h; Reagent/catalyst;	98%

: 100-46-9
benzylamine

: 100-52-7
benzaldehyde

Conditions

Conditions	Yield
With dinitratocerium (IV) chromate In benzene for 1.25h; Heating;	100%
With 2,2'-bipyridylchromium peroxide for 0.4h; Product distribution; effect of various chromium(VI) based oxidants;	100%
With barium ferrate(VI) In benzene for 1h; Product distribution; Heating;	100%

: 100-51-6
benzyl alcohol

: 100-52-7
benzaldehyde

Conditions

Conditions	Yield
With bis(pyridine)silver(I) permanganate In benzene for 0.5h;	100%
With pyridine chromium peroxide In dichloromethane for 0.5h; Ambient temperature;	100%
With manganese(IV) oxide; Pyridine-2,6-dicarboxylic acid In water; acetonitrile at 20℃; for 20h;	100%

: 286-28-2
cyclohexene sulfide

: 39245-63-1
cis-2-methyl-3-phenyloxaziridine

A: 4143-42-4
(Z)-azomethane

B: 13849-02-0, 84878-02-4, 84878-03-5, 84878-04-6
N,N'-bis(methyl)sulphur di-imide

C: 100-52-7
benzaldehyde

D: 110-83-8
cyclohexene

Conditions

Conditions	Yield
In chloroform Mechanism; Ambient temperature; via thionitrosomethane, CH3NS (also used: other oxaziridines and episulfides);	A n/a B 83% C 100% D 100%

...Expand

: 19202-00-7
(2,3-dihydro-4H-benzo[b][1,4]oxazin-4-yl)(phenyl)methanone

A: 5735-53-5
1,4-benzoxazine

B: 100-52-7
benzaldehyde

Conditions

Conditions	Yield
With sodium bis(2-methoxyethoxy)aluminium dihydride In ethyl acetate; benzene at -40℃;	A 100% B 100%

: 936-51-6
2-phenyl-1,3-dioxolane

: 100-52-7
benzaldehyde

Conditions

Conditions	Yield
1,3-di(NCS)-tetrabutyldistannoxane In diethylene glycol dimethyl ether; water at 100℃; for 2h; Deprotection of acetal;	100%
Tetrabutyl-1,3-diisothiocyanato-distannoxane In diethylene glycol dimethyl ether; water at 100℃; for 2h;	100%
With 4-phenyl-2,2,5,5-tetramethyl-3-imidazolin-1-yloxy-3-oxide; 15-crown-5; KCrO5Cl In acetonitrile at 60℃; for 7h; Product distribution; Further Variations:; Reagents;	100%

: 93-56-1
phenylethane 1,2-diol

: 62820-00-2
4-cyano-N,N-dimethylaniline-N-oxide

A: 50-00-0
formaldehyd

B: 4714-62-9
4-cyano-N-methylaniline

C: 100-52-7
benzaldehyde

D: 1197-19-9
4-cyano-N,N-dimethylaniline

Conditions

Conditions	Yield
With chloro(5,10,15,20-tetraphenylporphyrinato)chromium(III) In acetonitrile for 0.666667h; Rate constant; Ambient temperature; Irradiation; oxygen transfer was investigated, different irradiation time;	A n/a B n/a C 100% D 100%

...Expand

: 93-56-1
phenylethane 1,2-diol

: 100-52-7
benzaldehyde

Conditions

Conditions	Yield
With tris paraperiodate In benzene for 1.5h; Heating;	100%
With N-iodo-succinimide In tetrahydrofuran for 3h; Ambient temperature; in the dark;	98%
With calcium hypochlorite; water; aluminum oxide for 0.00555556h; microwave irradiation;	98%

: 5425-44-5
2-Phenyl-[1,3]dithiane

: 100-52-7
benzaldehyde

Conditions

Conditions	Yield
With K-10 clay supported copper(II) nitrate trihydrate In dichloromethane for 5h; Ambient temperature; K-10 clay supported iron(III) nitrate nonahydrate; mild cleavege of thioacetals into the corresponding carbonyl compounds;	100%
With K-10 clay supported iron(III) nitrate nonahydrate In dichloromethane for 5h; Ambient temperature; with K-10 clay-supported copper(II) nitrate trihydrate;	100%
With dihydrogen peroxide; iodine; sodium dodecyl-sulfate In water at 20℃; for 0.75h; Micellar solution;	100%

: 103-30-0
(E)-1,2-diphenyl-ethene

: 100-52-7
benzaldehyde

Conditions

Conditions	Yield
With 1,2,3,4,5-pentafluoro-6-iodosylbenzene; iron(III) perchlorate In acetonitrile at -10℃; for 0.0833333h;	100%
With air; [Pt(2,2':6',2'':6'',2'''-quaterpyridine)](CF3SO3)2; Nafion In acetonitrile at 20℃; for 5h; Irradiation;	100%
With sodium periodate; osmium(VIII) oxide In tetrahydrofuran; water at 20℃;	99%

: 768-49-0
(2-methyl-1-propenyl)-benzene

: 100-52-7
benzaldehyde

Conditions

Conditions	Yield
With sodium nitrite In water; acetic acid 1.) 0 deg C 2.) 60 deg C, 0,5 h;	100%
With oxygen at 25℃; under 1500.15 Torr; for 24h; pH=6; aq. buffer; Enzymatic reaction; chemoselective reaction;

: 14642-79-6
benzyloxy-trimethylsilane

: 100-52-7
benzaldehyde

Conditions

Conditions	Yield
With benzyltriphenylphosphonium chlorate; aluminium trichloride In acetonitrile for 0.25h; Heating;	100%
With nitrogen dioxide at 20℃; for 0.0833333h;	100%
With N-benzyl-N,N-dimethyl anilinium peroxodisulfate In acetonitrile for 0.0833333h; Reflux;	99%

: 774-48-1
(diethoxymethyl)benzene

: 100-52-7
benzaldehyde

Conditions

Conditions	Yield
With water at 80℃; for 2h;	100%
With iodo trichloro silane for 0.333333h; Ambient temperature;	95%
With iodo trichloro silane for 0.333333h; Product distribution; Mechanism; Ambient temperature; other acyclic and cyclic acetals and ketals;	95%

: 1666-17-7
benzaldehyde p-toluenesulfonylhydrazone

: 100-52-7
benzaldehyde

Conditions

Conditions	Yield
With copper(II) sulfate In tetrahydrofuran; methanol; water for 24h; Heating;	100%
With Cr-MCM-41 zeolite on silica gel for 0.1h; microwave irradiation;	96%
With copper(II) nitrate In tetrachloromethane at 25℃; for 2h; regeneration of aldehydes and ketones from tosylhydrazones; further tosylhydrazones;	92%

: 935-05-7
benzyl nitrite

: 100-52-7
benzaldehyde

Conditions

Conditions	Yield
With nitric acid In dichloromethane at 20℃; for 1h;	100%
With sulfuric acid In dichloromethane; water for 0.5h; in air;	100%
With dimethyl sulfoxide at 70℃; for 6h;	87.9%
With Amberlyst-15 In 1,4-dioxane at 40℃; Kinetics; Concentration; Temperature;

: 1125-88-8
benzaldehyde dimethyl acetal

: 100-52-7
benzaldehyde

Conditions

Conditions	Yield
sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate In water at 30℃; for 0.0833333h;	100%
With water at 80℃; for 2h;	100%
With water at 90℃; Inert atmosphere;	100%

: 581-55-5
benzylidene 1,1-diacetate

: 100-52-7
benzaldehyde

Conditions

Conditions	Yield
With [NO(1+)18-crown-6H(NO3)2(1-)]; silica gel In dichloromethane at 20℃; for 0.0833333h;	100%
With sulphated zirconia In acetonitrile at 60℃; for 0.45h; Microwave irradiation;	100%
With aluminum oxide at 35℃; for 0.0111111h; microwave irradiation;	98%

: 5418-20-2
benzaldehyde dibenzyldithioacetal

A: 150-60-7
dibenzyl disulphide

B: 100-52-7
benzaldehyde

Conditions

Conditions	Yield
With hydrogenchloride; sodium nitrate In tetrachloromethane; water for 5h; Ambient temperature; other reagent;	A n/a B 100%

: 119111-63-6
1-(N,N-dibenzylamino)cyclopropanecarboxylic acid

A: 100-52-7
benzaldehyde

B: 119111-75-0
1-(N-benzylamino)cyclopropanecarboxylic acid hydrochloride

Conditions

Conditions	Yield
With pivaloyl chloride In chloroform Ambient temperature;	A 100% B 63%

: 1574-10-3
benzaldehyde semicarbazone

: 100-52-7
benzaldehyde

Conditions

Conditions	Yield
With Oxone; silica gel In dichloromethane for 0.333333h; Reflux;	100%
With benzyltriphenylphosphonium dichromate; silica gel for 0.166667h;	97%
With hexaaquairon(III) perchlorate for 2h;	96%

: 83080-95-9
1-Acetamido-N-benzyloxy-6,7-dihydro-5H-dibenzazepin

A: 100-52-7
benzaldehyde

B: 83081-01-0
1-Acetamido-5H-dibenzazepin-N-oxid

C: 83081-02-1
11-Acetamido-5H-dibenzazepin-N-oxid

Conditions

Conditions	Yield
With dihydrogen peroxide In acetic acid for 1.66667h; Ambient temperature; Yield given. Title compound not separated from byproducts;	A 100% B n/a C n/a

...Expand

: 588-64-7
benzaldehyde phenylhydrazone

: 100-52-7
benzaldehyde

Conditions

Conditions	Yield
With copper(II) sulfate In tetrahydrofuran; methanol; water for 6h; Heating;	100%
With baker's yeast; phosphate buffer In ethanol at 37℃; for 12h;	98%
With CuCl*Kieselghur; oxygen In dichloromethane at 20℃; for 0.416667h;	98%

: 1927-62-4
tetrahydro-2-(benzyloxy)-2H-pyran

: 100-52-7
benzaldehyde

Conditions

Conditions	Yield
With aluminium trichloride; benzyltriphenylphosphonium chlorate In acetonitrile at 20℃; for 3h;	100%
With aluminium trichloride; tetramethylammonium chlorochromate In acetonitrile for 0.75h; Heating;	98%
With β‐cyclodextrin; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In water; acetone at 20℃; for 1h;	96%

: 7540-93-4
2-hydroxy-1,2,3-triphenyl-propan-1-one

A: 451-40-1
phenyl benzyl ketone

B: 119-53-9
2-hydroxy-2-phenylacetophenone

C: 100-52-7
benzaldehyde

Conditions

Conditions	Yield
With tetra-n-butylammonium cyanide In tetrahydrofuran for 1h; Heating;	A 100% B 38% C 6%

...Expand

: 174869-02-4
α-(2-cyanoethyl)benzoin

A: 5343-98-6
4-oxo-4-phenylbutanenitrile

B: 119-53-9
2-hydroxy-2-phenylacetophenone

C: 100-52-7
benzaldehyde

Conditions

Conditions	Yield
With tetra-n-butylammonium cyanide In tetrahydrofuran for 1h; Ambient temperature;	A 100% B 75% C 2%

...Expand

: 772-01-0
2-phenyl-1,3-dioxane

: 100-52-7
benzaldehyde

Conditions

Conditions	Yield
With 4-phenyl-2,2,5,5-tetramethyl-3-imidazolin-1-yloxy-3-oxide; 15-crown-5; KCrO5Cl In acetonitrile at 60℃; for 7h; Product distribution; Further Variations:; Reagents;	100%
indium(III) chloride In methanol; water for 1.16667h; Heating;	93%
With water; sodium acetate; Pyridine hydrobromide In methanol at 20℃; for 24h; Reagent/catalyst;	9%

: 36236-72-3
4-chloromethyl-2-phenyl[1,3]dioxolane

: 100-52-7
benzaldehyde

Conditions

Conditions	Yield
With 4-phenyl-2,2,5,5-tetramethyl-3-imidazolin-1-yloxy-3-oxide; 15-crown-5; KCrO5Cl In acetonitrile at 60℃; for 7h; Product distribution; Further Variations:; Reagents;	100%

: 110-89-4
piperidine

: 100-52-7
benzaldehyde

: 2538-76-3
1,1'-benzylidenedipiperidine

Conditions

Conditions	Yield
With copper(II) bis(trifluoromethanesulfonate) In water at 20℃; for 0.0333333h;	100%
In ethanol at 25℃; for 0.5h;	95%
With aluminum oxide In diethyl ether at 20℃;	90%

: 110-91-8
morpholine

: 100-52-7
benzaldehyde

: 6425-08-7
4,4'-(phenylmethylene)bismorpholine

Conditions

Conditions	Yield
With copper(II) bis(trifluoromethanesulfonate) In water at 20℃; for 0.0333333h;	100%
In benzene at 20℃; for 16h; Inert atmosphere;	99%
In benzene Reflux;	95%

: 95-20-5
2-methyl-1H-indole

: 100-52-7
benzaldehyde

: 17371-59-4
2-methyl-3-((2-methyl-1H-indol-3-yl)(phenyl)methyl)-1H-indole

Conditions

Conditions	Yield
With C62H58N8O20Y2Zn2 In ethanol; water for 2h; Friedel-Crafts Alkylation;	100%
With tris(hydroxymethyl)methane ammonium hydrogensulphate In neat (no solvent) at 20℃; for 0.0833333h; Green chemistry;	99%
With ruthenium trichloride In methanol at 20℃; for 0.05h;	98%

: 4231-74-7
N-methyl-N-(pyridin-2-yl)hydrazine

: 100-52-7
benzaldehyde

: 4231-75-8
(E)-2-benzylidene-1-methyl-1-(pyridin-2-yl)hydrazine

Conditions

Conditions	Yield
In ethanol for 6h; Reflux;	100%
With water

: 59-48-3
2-oxoindole

: 100-52-7
benzaldehyde

: 3359-49-7, 23772-61-4, 23782-37-8
3-benzylideneoxindole

Conditions

Conditions	Yield
With UiO-66 metal organic framework nanoparticles In neat (no solvent) at 80℃; for 2h; Friedel-Crafts Alkylation; Sealed tube; Darkness;	100%
With pyrrolidine In ethanol for 2h; Reflux;	94%
With [1-(3-sulfonic acid)]propyl-3-methylimidazolium hydrogen sulfate at 80℃; for 1h;	93%

: 21531-96-4
4-aminourazole

: 100-52-7
benzaldehyde

: 4114-10-7
4-benzylidenamino-[1,2,4]triazolidine-3,5-dione

Conditions

Conditions	Yield
In water for 0.5h; Reflux;	100%
With water

: 78-81-9
isobutylamine

: 100-52-7
benzaldehyde

: 27845-49-4, 6852-57-9
benzylideneisobutylamine

Conditions

Conditions	Yield
at 20℃; for 2h;	100%
	91%

: 108-94-1
cyclohexanone

: 100-52-7
benzaldehyde

: 5682-83-7
2-Benzylidenecyclohexanone

Conditions

Conditions	Yield
Stage #1: cyclohexanone With sodium hydroxide In ethanol; water at 0 - 5℃; Stage #2: benzaldehyde In ethanol; water	100%
With CaO modified with benzyl bromide In methanol at 65℃; under 760.051 Torr; for 3h; Reagent/catalyst; Concentration; Temperature; Time;	95.8%
With N,N-Dimethyltrimethylsilylamine; magnesium bromide ethyl etherate at 20℃; for 16h; Inert atmosphere; neat (no solvent);	93%

: 108-24-7
acetic anhydride

: 100-52-7
benzaldehyde

: 581-55-5
benzylidene 1,1-diacetate

Conditions

Conditions	Yield
With poly(4-vinylpyridine)-supported sulfuric acid In dichloromethane at 20℃; for 0.25h; Green chemistry; chemoselective reaction;	100%
With SBA-15-Ph-PrSO3H at 20℃; for 0.0833333h; Green chemistry;	100%
With poly(4-vinylpyridinium) perchlorate In neat (no solvent) at 20℃; for 0.0333333h; Time; Green chemistry; chemoselective reaction;	100%

: 141-97-9
ethyl acetoacetate

: 100-52-7
benzaldehyde

: 57-13-6
urea

: 123237-03-6, 5395-36-8
ethyl 6-methyl-4-phenyl-3,4-dihydropyrimidin-2(1H)-one-5-carboxylate

Conditions

Conditions	Yield
With copper(II) bis(trifluoromethanesulfonate) In ethanol at 100℃; for 1h; Biginelli reaction; Microwave irradiation; Inert atmosphere;	100%
With Cl7Fe2(1-)C6H9N2O2(1+); C8H15N2(1+)C4H12B(1-) at 80℃; for 2h; Reagent/catalyst; Biginelli Pyrimidone Synthesis;	99%
With guanidine In neat (no solvent) at 80℃; for 2h; Biginelli Pyrimidone Synthesis;	99%

...Expand

: 141-97-9
ethyl acetoacetate

: 100-52-7
benzaldehyde

: 1165-06-6
Diethyl 2,6-dimethyl-4-phenyl-1,4-dihydropyridine-3,5-dicarboxylate

Conditions

Conditions	Yield
With ammonia for 3h; Heating;	100%
With C23H3BF16N2O; ammonium acetate In toluene at 100℃; for 10h; Hantzsch Dihydropyridine Synthesis;	100%
With ammonium carbonate In water at 55 - 60℃; for 3.5h; Hantzsch pyridine synthesis;	99%

: 134-32-7
1-amino-naphthalene

: 100-52-7
benzaldehyde

: 890-51-7
N-benzylidenenaphthalen-1-amine

Conditions

Conditions	Yield
With aluminum oxide for 5h; Milling;	100%
In water at 20℃; for 2h;	80%
In dichloromethane for 10h; Reflux;	70%

: 109-80-8
1.3-propanedithiol

: 100-52-7
benzaldehyde

: 5425-44-5
2-Phenyl-[1,3]dithiane

Conditions

Conditions	Yield
With boron trifluoride diethyl etherate at 23℃; for 3h;	100%
With lithium tetrafluoroborate at 25℃; for 1h;	100%
With lithium bromide at 75 - 80℃; for 0.25h;	99%

: 107-10-8
propylamine

: 100-52-7
benzaldehyde

: 6852-55-7
N-benzylidenepropylamine

Conditions

Conditions	Yield
In toluene for 1h; Ambient temperature;	100%
at 26℃; for 24h;	96%
With aluminum oxide at 20℃; for 4h;	95%

n-butyllithium: n-butyllithium

: 100-52-7
benzaldehyde

: 583-03-9
1-Phenyl-1-pentanol

Conditions

Conditions	Yield
In tetrahydrofuran; hexane at -78 - 20℃;	100%
Stage #1: n-butyllithium With mischmetall tribromide In tetrahydrofuran; hexane at -78℃; for 1h; Stage #2: benzaldehyde In tetrahydrofuran; hexane at -78℃; for 3h; Imamoto reaction;	98%
In hexane at -78 - 20℃; for 1.16667h;	95%

: 75-52-5
nitromethane

: 100-52-7
benzaldehyde

: 141377-54-0, 145920-96-3, 149495-00-1, 15990-45-1
2-nitro-1-phenylethan-1-ol

Conditions

Conditions	Yield
palladium/alumina at 60℃; for 1h;	100%
With 1-butyl-4-aza-1-azoniabicyclo[2.2.2]octane hydroxide In neat (no solvent) at 20℃; for 0.166667h; Reagent/catalyst; Henry Nitro Aldol Condensation; Green chemistry;	99%
With 1-butyl-4-aza-1-azoniabicyclo[2.2.2]octane hydroxide In neat (no solvent) at 20℃; for 0.166667h; Catalytic behavior; Reagent/catalyst; Henry Nitro Aldol Condensation; Ionic liquid; Green chemistry;	99%

: 74-90-8
hydrogen cyanide

: 100-52-7
benzaldehyde

: 10020-96-9
(R)-Mandelonitrile

Conditions

Conditions	Yield
With (R)-oxynitrilase (almond meal); citric buffer pH 5.5 In ethyl acetate at 4℃; for 48h; Product distribution; other aldehydes and methyl ketones, also in micro-aqueous phase, var temp. and solvents;	100%
With (R)-oxynitrilase (almond meal) In ethyl acetate at 4℃; for 48h; 0.02 M citrate buffer pH 5.5;	100%
With (R)-hydroxynitrile lyase In tert-butyl methyl ether; dimethyl sulfoxide at 5℃; for 24h; pH=4; aq. citrate buffer; Enzymatic reaction; optical yield given as %ee; enantioselective reaction;	100%

: 24347-58-8
(R,R)-2,3-butandiol

: 100-52-7
benzaldehyde

: 75281-80-0
4,5-dimethyl-2-phenyl-(2α,4α,5β)-1,3-dioxolane

Conditions

Conditions	Yield
With toluene-4-sulfonic acid In benzene at 100℃; for 3h; Molecular sieve;	100%
With trifluoromethanesulfonate; 1-phenyl-1-trimethylsilyloxyethane In dichloromethane at -20℃; for 3h;	96%
With toluene-4-sulfonic acid; orthoformic acid triethyl ester at 140℃; for 2h;	85%

: 111-26-2
hexan-1-amine

: 100-52-7
benzaldehyde

Conditions

Conditions	Yield
at 20℃; for 2h;	100%
With ethanol; potassium carbonate
With aluminum oxide for 2h; Ambient temperature;

: 100-52-7
benzaldehyde

: 24469-50-9
t-butyl 3-benzylidenecarbazate

Conditions

Conditions	Yield
In tetrahydrofuran at 20℃; for 4h;	100%
In ethanol for 3h; Reflux;	100%
In ethanol	99%

: 139-65-1
4,4'-thiobisaniline

: 100-52-7
benzaldehyde

: 3430-68-0
N,N'-(thiobis(4,1-phenylene))bis(1-phenyl methanimine)

Conditions

Conditions	Yield
With piperidine In ethanol	100%
With acetic acid In ethanol for 4h; Reflux;	86%
With ethanol; zinc(II) chloride

: 64-10-8
phenyl carbamate

: 100-52-7
benzaldehyde

: 40848-82-6
1,1'-(phenylmethylene)bis(3-phenylurea)

Conditions

Conditions	Yield
In acetonitrile at 20℃; for 5h;	100%
With silica-bonded N-(propylsulfonyl)piperazine-N-sulfamic acid In toluene for 2.5h; Reflux;	78%

: 3536-96-7
vinylmagnesium chloride

: 100-52-7
benzaldehyde

: 4393-06-0
1-Phenyl-2-propen-1-ol

Conditions

Conditions	Yield
In tetrahydrofuran at 0℃; for 2h; Inert atmosphere;	100%
In tetrahydrofuran at -10 - 20℃; Schlenk technique;	95%
In tetrahydrofuran at -10℃; for 2h; Inert atmosphere;	93%

: 16466-97-0, 13254-27-8
1-propynylmagnesium bromide

: 100-52-7
benzaldehyde

: 32398-66-6
1-phenylbut-2-yn-1-ol

Conditions

Conditions	Yield
In tetrahydrofuran	100%
In tetrahydrofuran at 0 - 20℃;	86%
In tetrahydrofuran at 0 - 20℃; for 2h; Grignard Reaction; Schlenk technique; Inert atmosphere;	77%

: 52-89-1
l-cysteine hydrochloride

: 100-52-7
benzaldehyde

: 196930-46-8
(4R)-2-phenyl-1,3-thiazolidine-4-carboxylic acid

Conditions

Conditions	Yield
Stage #1: l-cysteine hydrochloride With sodium hydroxide In water Stage #2: benzaldehyde In ethanol; water at 20℃; for 3h;	100%
With potassium acetate In methanol; water at 0 - 25℃; for 6h;	98%
Stage #1: l-cysteine hydrochloride With potassium carbonate In water Stage #2: benzaldehyde In methanol; water at 25℃; for 3h;	98%

: 925-90-6
ethylmagnesium bromide

: 100-52-7
benzaldehyde

: 93-54-9
1-Phenyl-1-propanol

Conditions

Conditions	Yield
With methylaluminum bis(2,6-di-tert-butylphenoxide) In diethyl ether; toluene at -78℃; for 2h;	100%
In diethyl ether at 0 - 20℃;	87%
Stage #1: ethylmagnesium bromide; benzaldehyde In tetrahydrofuran at 30℃; for 24h; Inert atmosphere; Stage #2: With water In tetrahydrofuran Inert atmosphere;	73%

: 100-52-7
benzaldehyde

: 106-47-8
4-chloro-aniline

: 780-21-2
N-(4-chlorobenzylidene)aniline

Conditions

Conditions	Yield
With acetic acid In 1,2-dichloro-ethane at 20℃; for 24h; Inert atmosphere;	100%
With aqueous extract of pericarp of Sapindus trifoliatus fruits at 20℃; for 0.0333333h;	98%
sodium hydrogen sulfate; silica gel at 62 - 64℃; for 0.0208333h; microwave irradiation;	96%

: 100-52-7
benzaldehyde

: 126-81-8
dimedone

: 19744-83-3
3,3,6,6-tetramethyl-9-phenyl-3,4,5,6,7,9-hexahydro-1H-xanthene-1,8-(2H)-dione

Conditions

Conditions	Yield
With poly[(2-acrylamido-2-methylpropane sulfonic acid)-co-(acrylic acid)-co-(vinyl functionalized halloysite clay)] In water at 20℃; for 3h;	100%
With sulfated polyborate catalyst In neat (no solvent) at 100℃; for 0.05h; Catalytic behavior; Temperature; Green chemistry;	99%
With acetic acid at 110℃; for 0.25h; Microwave irradiation;	98%

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