minimum order qty. 10 gram
Cas:1125-88-8
Min.Order:10 Gram
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inquiryAs a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:1125-88-8
Min.Order:1 Kilogram
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:1125-88-8
Min.Order:1 Kilogram
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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Cas:1125-88-8
Min.Order:1 Gram
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:1125-88-8
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
Cas:1125-88-8
Min.Order:1 Gram
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inquiryBenzaldehyde dimethyl acetal Basic information Product Name: Benzaldehyde dimethyl acetal Synonyms: (dimethoxymethyl)-benzen;a,a-dimethoxytoluene;Benzene, (dimethox
Cas:1125-88-8
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:1125-88-8
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiryProduct Name Benzaldehyde dimethyl acetal Synonyms Benzaldehyde dimethyl acetal;Dimethoxytoluene CAS: 1125-88-8 MF: - MW: - EI
Cas:1125-88-8
Min.Order:5 Metric Ton
FOB Price: $1.0 / 2.0
Type:Other
inquiryWe are leading fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...)
Cas:1125-88-8
Min.Order:1 Kilogram
FOB Price: $4.0 / 5.0
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Cas:1125-88-8
Min.Order:1 Kilogram
FOB Price: $9.0 / 99.0
Type:Trading Company
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Cas:1125-88-8
Min.Order:100 Gram
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Type:Other
inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:1125-88-8
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryProduct Name: Benzaldehyde dimethyl acetal CAS: 1125-88-8 MF: C9H12O2 MW: 152.19 EINECS: 214-413-0 Mol File: 1125-88-8.mol Benzaldehyde dimethyl acetal Structure Benzaldehyde dimethyl acetal Chemical Properties Melting point 8
Cas:1125-88-8
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryBenzaldehyde dimethyl acetal CAS:1125-88-8 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organ
Cas:1125-88-8
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:1125-88-8
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryAppearance:white or light yellow crystalline powder Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for research and industrial manufacture. Transportation:By
Cas:1125-88-8
Min.Order:100 Gram
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Type:Lab/Research institutions
inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Cas:1125-88-8
Min.Order:10 Kilogram
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Type:Trading Company
inquiryAdvantage 1: The product passed the professional production process and quality inspection, the purity is 99% +. 2: Highly qualified engineers to provide technical documents and service. 3: We could provide sample for your test. 4: High qualit
Cas:1125-88-8
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:1125-88-8
Min.Order:0 Metric Ton
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Type:Lab/Research institutions
inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
Cas:1125-88-8
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Cas:1125-88-8
Min.Order:0
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Cas:1125-88-8
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryWe are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
Cas:1125-88-8
Min.Order:100 Gram
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Type:Lab/Research institutions
inquirySuperior quality, moderate price & quick delivery. Appearance:Clear colorless liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum, or as per your request. Application:For medicine , pesticide
Cas:1125-88-8
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:1125-88-8
Min.Order:1 Gram
FOB Price: $1.0
Type:Lab/Research institutions
inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:1125-88-8
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryGMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,
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Min.Order:1 Milligram
Negotiable
Type:Trading Company
inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:1125-88-8
Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
inquiryConditions | Yield |
---|---|
With [Sc2(C4O4)3]n In tetrachloromethane at 60℃; for 1h; | 100% |
With lithium tetrafluoroborate In methanol for 0.5h; Heating; | 100% |
indium(III) triflate In dichloromethane at 20℃; for 0.0833333h; | 99% |
Conditions | Yield |
---|---|
With trimethyl orthoformate at 20℃; for 0.5h; | 99% |
With cobalt(II) 2-propyliminomethyl-phenolate functionalized mesoporous silica for 2h; Reflux; | 99% |
With Zr6(µ3-O)4(µ3-OH)4(2,2-bis(trifluoromethyl)-4,4’-biphenyldicarboxylate)4[Cu(2,2'-bipyridine-5,5’-dicarboxylate)(MeCN)I](C6H3(NH-CO-C6H4-SO3H)(PhCOO)2) at 20℃; for 2h; Catalytic behavior; Reagent/catalyst; | 99% |
methanol
3,3,5-triphenyl-1,2,4-trioxolane
A
benzoic acid methyl ester
B
benzophenone
C
benzaldehyde dimethyl acetal
Conditions | Yield |
---|---|
With chlorosulfonic acid for 80h; | A 75% B 95% C 25% |
3,3,5-triphenyl-1,2,4-trioxolane
A
benzoic acid methyl ester
B
benzophenone
C
benzaldehyde dimethyl acetal
Conditions | Yield |
---|---|
With chlorosulfonic acid In methanol for 80h; | A 75% B 95% C 25% |
methanol
toluene
A
benzoic acid methyl ester
B
benzaldehyde dimethyl acetal
C
benzaldehyde
Conditions | Yield |
---|---|
With sodium perchlorate; Tris(2,4-dibromophenyl)amine In dichloromethane indirect electrochemical oxidation; Yields of byproduct given; | A 95% B n/a C n/a |
With lithium perchlorate direct electrochemical oxidation; Yield given. Yields of byproduct given. Title compound not separated from byproducts; |
methanol
3-chloro-3-phenyl-3H-diazirine
A
benzylidene dichloride
B
benzaldehyde dimethyl acetal
C
benzaldehyde
Conditions | Yield |
---|---|
at 80℃; for 6h; Mechanism; other 3-chloro-3-aryldiazirines; | A n/a B 95% C 1% |
at 80℃; for 6h; | A n/a B 95% C 1% |
Conditions | Yield |
---|---|
trimethylsilyl trifluoromethanesulfonate In dichloromethane at -78℃; for 3h; Product distribution; | 94% |
trimethylsilyl trifluoromethanesulfonate In dichloromethane at -78℃; for 3h; | 94% |
trimethylsilyl trifluoromethanesulfonate In dichloromethane at -78℃; for 3h; | 94% |
In dichloromethane at -78℃; for 0.0833333h; |
Conditions | Yield |
---|---|
With 2-Picolinic acid; ferrous(II) sulfate heptahydrate; dihydrogen peroxide at 20 - 60℃; for 12h; Schlenk technique; Molecular sieve; | 93% |
With potassium trifluoroacetate at 55 - 60℃; electrochemical oxidation; | 42 % Spectr. |
With tert.-butylhydroperoxide; C30H29ClN4ORu(2+)*2F6P(1-) at 50℃; Catalytic behavior; Kinetics; Reagent/catalyst; Schlenk technique; Molecular sieve; | 87 %Chromat. |
With zinc indium sulfide; phenylmethanethiol for 15h; Irradiation; | 81 %Chromat. |
Conditions | Yield |
---|---|
With 2-Picolinic acid; ferrous(II) sulfate heptahydrate; dihydrogen peroxide at 20 - 60℃; for 12h; Schlenk technique; Molecular sieve; | 93% |
Conditions | Yield |
---|---|
With N-Bromosuccinimide at 20℃; for 0.166667h; | 92% |
methanol
benzaldehyde
A
benzoic acid methyl ester
B
benzaldehyde dimethyl acetal
Conditions | Yield |
---|---|
With oxygen; Pd5-Bi2-Pb1-Fe1/(100)SiO2-MgO | A 90.3% B n/a |
With oxygen; Pd5-Bi2-Fe1/(100)SiO2-MgO | A 88.8% B n/a |
With oxygen; Pd5-Bi2-Pb1-Co1/(100)SiO2 | A 88.6% B n/a |
methanol
3-α-bromobenzyloxy-3-fluorodiazirine
benzaldehyde dimethyl acetal
Conditions | Yield |
---|---|
In acetonitrile at 25℃; Rate constant; Mechanism; also in the presence of HCl or bases, use of CD3OD/CD3CN, also with ethylene glycol or piperidine; | 90% |
methanol
[bis(acetoxy)iodo]benzene
benzaldehyde benzylidenehydrazone
A
iodobenzene
B
benzaldehyde dimethyl acetal
Conditions | Yield |
---|---|
With sodium methylate at 0 - 25℃; for 48h; Product distribution; Var. aldazines and alcohols; | A n/a B 88% |
methanol
benzaldehyde benzylidenehydrazone
benzaldehyde dimethyl acetal
Conditions | Yield |
---|---|
With [bis(acetoxy)iodo]benzene; sodium methylate at 0 - 25℃; for 48h; | 88% |
Conditions | Yield |
---|---|
trimethylsilyl iodide In dichloromethane 1.) -78 deg C, 3 h, 2.) RT, 4h; | 87% |
With hydrogenchloride |
Conditions | Yield |
---|---|
With bromine for 1h; Heating; | 87% |
Conditions | Yield |
---|---|
With N-Bromosuccinimide at 20℃; for 0.0833333h; | 86% |
trifluoroacetic acid-methyl ester
sodium methylate
benzaldehyde
benzaldehyde dimethyl acetal
Conditions | Yield |
---|---|
In methanol at 20℃; Inert atmosphere; | 85% |
methanol
chalcone epoxide
A
benzoic acid methyl ester
B
benzaldehyde dimethyl acetal
C
2-hydroxy-3-methoxy-1,3-diphenylpropan-1-one
Conditions | Yield |
---|---|
With tetraethylammonium bromide at 25℃; Product distribution; reaction in CH3OD and nitromethane (1:50); in acetic acid; retention/inversion products; | A 2% B 13% C 84% |
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid at 70℃; Addition; | 84% |
With toluene-4-sulfonic acid | 67% |
methanol
1,2-dimethoxyethylbenzene
A
benzaldehyde dimethyl acetal
B
1-phenyl-1,1,2-trimethoxyethane
Conditions | Yield |
---|---|
With potassium fluoride; 100 mA cm-2 at 60℃; Product distribution; various supporting electrolytes and anode materials; | A 82% B 10% |
With potassium fluoride at 60℃; 100 mA cm-2, Pt anode; | A 82% B 10% |
styrene
methanol
A
benzaldehyde dimethyl acetal
B
1,2-dimethoxyethylbenzene
C
1,4-dimethoxy-1,4-diphenylbutane
D
1-phenyl-1,2,2-trimethoxy ethane
Conditions | Yield |
---|---|
With potassium fluoride at 60℃; 100 mA cm-2, Pt anode; Further byproducts given; | A 1% B 80% C 3% D 5% |
With TPC at 60℃; 100 mA cm-2, C anode; | A 16% B 45% C 13% D 2% |
styrene
methanol
A
benzaldehyde dimethyl acetal
B
1,2-dimethoxyethylbenzene
C
1,4-dimethoxy-1,4-diphenylbutane
D
1-phenyl-1,2,2-trimethoxy ethane
E
meso-1,4-dimethoxy-2,3-diphenylbutane
F
1,4-dimethoxy-1,3-diphenylbutane
Conditions | Yield |
---|---|
With potassium fluoride; 100 mA cm-2 at 60℃; Product distribution; various supporting electrolytes and anode materials; | A 1% B 80% C 3% D 5% E 2% F 2% |
methanol
benzaldehyde
acetophenone
A
acetophenone dimethyl acetal
B
benzaldehyde dimethyl acetal
Conditions | Yield |
---|---|
With CoCl2 for 2h; Heating; | A n/a B 77% |
benzylidene dichloride
trimethyl orthoformate
benzaldehyde dimethyl acetal
Conditions | Yield |
---|---|
at 225℃; for 39h; | 76% |
With zinc(II) chloride at 20 - 25℃; for 1h; |
methanol
benzaldehyde
A
benzoic acid methyl ester
B
benzaldehyde dimethyl acetal
C
benzoic acid
Conditions | Yield |
---|---|
With Eco1a; dihydrogen peroxide In water at 20℃; for 17h; Reflux; | A 76% B 10% C 11% |
With dihydrogen peroxide; zinc(II) chloride In water at 20℃; | |
With oxygen at 179.84℃; under 7500.75 Torr; for 2h; Inert atmosphere; |
styrene
methanol
A
benzaldehyde dimethyl acetal
B
benzaldehyde
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; C29H25Cl2N4Ru(1+)*F6P(1-) at 50℃; for 6h; Reagent/catalyst; Schlenk technique; Molecular sieve; | A 73% B 7% |
With ozone; thiourea 1) -10-(-15) deg C, 65 min, CH3OH; 2) 0 deg C, 55 min; Yield given. Multistep reaction; |
α-chlorobenzyl methyl ether
trimethyl orthoformate
benzaldehyde dimethyl acetal
Conditions | Yield |
---|---|
at 20℃; for 24h; | 72% |
α-chlorobenzyl methyl ether
trimethyl orthoformate
A
Methyl formate
B
benzaldehyde dimethyl acetal
Conditions | Yield |
---|---|
A n/a B 72% |
methanol
Cyclohepta-1,3,5-triene
A
7-methoxy-1,3,5-cycloheptatriene
B
benzaldehyde dimethyl acetal
Conditions | Yield |
---|---|
With sodium methylate; tetraethylammonium tosylate at -10 - 0℃; anodic oxidation; | A 71% B 15% |
benzaldehyde dimethyl acetal
allyl-trimethyl-silane
4-methoxy-4-phenyl-1-butene
Conditions | Yield |
---|---|
With trimethylaluminum; aluminum tri-bromide; copper(I) bromide In dichloromethane; toluene at 20℃; for 3h; | 100% |
With 2,4-dinitrobenzenesulfonic acid In acetonitrile at 20℃; for 1h; Hosomi-Sakurai reaction; | 99% |
With 30% bis[triphenyl(3-sulfopropyl)phosphonium]HPW12O40/SiO2 In acetonitrile at 20℃; for 0.5h; Catalytic behavior; Reagent/catalyst; Solvent; Hosomi-Sakurai Reaction; Inert atmosphere; Green chemistry; chemoselective reaction; | 99% |
4-methoxy-5H-furan-2-one
benzaldehyde dimethyl acetal
methyl 5-(1-methoxybenzyl)tetronate
Conditions | Yield |
---|---|
zinc dibromide | 100% |
With n-butyllithium; boron trifluoride diethyl etherate 1.) ether, hexane, -78 deg C, 2.) ether, -78 deg C.; Yield given. Multistep reaction; |
1-styrenyloxytrimethylsilane
benzaldehyde dimethyl acetal
3-methoxy-1,3-diphenylpropan-1-one
Conditions | Yield |
---|---|
polymeric dicyanoketene acetal In acetonitrile for 6.5h; Substitution; Heating; | 100% |
With polymer-supported DCKA In acetonitrile for 6.5h; Heating; | 100% |
With Celite; polystyrene-bound super Broensted acid In toluene at 20℃; flow system; | 99% |
1-styrenyloxytrimethylsilane
benzaldehyde dimethyl acetal
1,3-diphenyl-propen-3-one
Conditions | Yield |
---|---|
With chloromethyl methyl ether; tin(ll) chloride In dichloromethane for 2h; Ambient temperature; | 100% |
1-(Trimethylsilyloxy)cyclohexene
benzaldehyde dimethyl acetal
(E)-2-benzylidenecyclohexanone
Conditions | Yield |
---|---|
With acetyl chloride; tin(ll) chloride In dichloromethane for 2h; Product distribution; Ambient temperature; effect of catalyst-activator system; | 100% |
With acetyl chloride; tin(ll) chloride In dichloromethane for 2h; Ambient temperature; | 100% |
benzaldehyde dimethyl acetal
tributyltin phenyl sulfide
(methoxy(phenylthio))methylbenzene
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate In hexane; toluene addn. of BF3*OEt2 in toluene to the acetal in toluene at -78°C and stirring for 1 h; GLC analysis; | 100% |
With boron trifluoride diethyl etherate In hexane; toluene at -78℃; for 1h; | 100 % Chromat. |
tert-butylisonitrile
benzaldehyde dimethyl acetal
2-methoxy-2-phenylacetonitrile
Conditions | Yield |
---|---|
With titanium tetrachloride at -78 - -30℃; | 100% |
With titanium tetrachloride In dichloromethane at -70 - 20℃; for 3h; | 96% |
Conditions | Yield |
---|---|
sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate In water at 30℃; for 0.0833333h; | 100% |
With water at 80℃; for 2h; | 100% |
With water at 90℃; Inert atmosphere; | 100% |
benzaldehyde dimethyl acetal
(2R,3S,4S,5R,6S)-2-Hydroxymethyl-6-phenylsulfanyl-tetrahydro-pyran-3,4,5-triol
(2R,4aR,6S,7R,8R,8aS)-2-Phenyl-6-phenylsulfanyl-hexahydro-pyrano[3,2-d][1,3]dioxine-7,8-diol
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In N,N-dimethyl-formamide at 60℃; pH=2 - 3; Inert atmosphere; | 100% |
With 1,3,5-trichloro-2,4,6-triazine In acetonitrile at 60℃; for 0.166667h; Sonication; Inert atmosphere; regioselective reaction; | 95% |
With iron(III) chloride In acetonitrile at 20℃; for 2.5h; regioselective reaction; | 92% |
benzaldehyde dimethyl acetal
2,2-Dimethyl-1,3-propanediol
5,5-dimethyl-2-phenyl-[1,3]dioxane
Conditions | Yield |
---|---|
With camphor-10-sulfonic acid In dichloromethane Inert atmosphere; | 100% |
With 4 A molecular sieve; camphor-10-sulfonic acid In dichloromethane for 0.5h; | 99% |
With camphor-10-sulfonic acid In dichloromethane Ambient temperature; | 97% |
benzaldehyde dimethyl acetal
(2R,4R,5R)-5-Methyl-hept-6-ene-2,4-diol
Conditions | Yield |
---|---|
With camphor-10-sulfonic acid In dichloromethane at 25℃; for 1.5h; | 100% |
benzaldehyde dimethyl acetal
(2R,4S,5S)-5-Methyl-hept-6-ene-2,4-diol
Conditions | Yield |
---|---|
With camphor-10-sulfonic acid In dichloromethane at 25℃; for 1.5h; | 100% |
benzaldehyde dimethyl acetal
Conditions | Yield |
---|---|
With camphor-10-sulfonic acid In benzene | 100% |
benzaldehyde dimethyl acetal
methyl beta-D-glucopyranoside
(2R,4aR,6R,7R,8R,8aS)-6-Methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxine-7,8-diol
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In N,N-dimethyl-formamide at 50℃; under 37.5038 Torr; for 2h; | 100% |
With (1S)-10-camphorsulfonic acid In acetonitrile at 20℃; for 4h; | 93% |
With iodine In acetonitrile at 20℃; for 1h; | 92% |
benzaldehyde dimethyl acetal
methyl α-D-galactopyranoside
methyl 4,6-O-benzylidene-α-D-galactopyranoside
Conditions | Yield |
---|---|
With camphor-10-sulfonic acid In chloroform at 65℃; | 100% |
With tetrafluoroboric acid In diethyl ether; N,N-dimethyl-formamide at 20℃; for 16h; | 96% |
With toluene-4-sulfonic acid; 1-butyl-3-methylimidazolium Tetrafluoroborate at 80℃; for 2h; | 92% |
benzaldehyde dimethyl acetal
((2R,3R,4R,5S,6R)-2-Ethoxy-4,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-3-yl)-carbamic acid allyl ester
((2R,4aR,6R,7R,8R,8aS)-6-Ethoxy-8-hydroxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl)-carbamic acid allyl ester
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In acetonitrile | 100% |
Conditions | Yield |
---|---|
With carbon tetrabromide; oxygen for 5h; Irradiation; | 100% |
With hydrogenchloride; dihydrogen peroxide | 95% |
With dihydrogen peroxide In water at 30℃; for 3h; Green chemistry; | 65% |
With oxygen at 90℃; under 3800.26 Torr; for 2h; |
Conditions | Yield |
---|---|
With trifluoroacetic acid In ethanol at 30℃; for 20h; | 100% |
benzaldehyde dimethyl acetal
(Z)-1-Trimethylsilanyl-5-trimethylsilanyloxy-pent-2-ene
Conditions | Yield |
---|---|
With trimethylsilyl trifluoromethanesulfonate In acetonitrile at -20℃; for 0.333333h; | 100% |
allyl 2-acetamido-2-deoxy-β-D-glucopyranoside
benzaldehyde dimethyl acetal
allyl 2-acetamido-(R)-4,6-O-benzylidene-2-deoxy-β-D-glucopyranoside
Conditions | Yield |
---|---|
With camphor-10-sulfonic acid In acetonitrile at 20℃; for 12h; | 100% |
With camphor-10-sulfonic acid In acetonitrile at 20℃; regioselective reaction; | 93% |
With toluene-4-sulfonic acid In acetonitrile for 2h; Ambient temperature; Yield given; | |
With camphor-10-sulfonic acid In acetonitrile at 20℃; |
benzaldehyde dimethyl acetal
(2R,3S,4R)-3-Benzyloxy-5-[4-(tert-butyl-dimethyl-silanyloxy)-3,5-dimethoxy-phenyl]-1,1-bis-ethylsulfanyl-pentane-2,4-diol
Conditions | Yield |
---|---|
With camphor-10-sulfonic acid In benzene for 0.333333h; Ambient temperature; | 100% |
benzaldehyde dimethyl acetal
(2R,3R,4S,5S,6R)-2-Dicyclohexylmethylsulfanyl-6-hydroxymethyl-tetrahydro-pyran-3,4,5-triol
(2R,4aR,6R,7R,8R,8aS)-6-Dicyclohexylmethylsulfanyl-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxine-7,8-diol
Conditions | Yield |
---|---|
With camphor-10-sulfonic acid In N,N-dimethyl-formamide at 57℃; under 20 Torr; for 3h; | 100% |
benzaldehyde dimethyl acetal
N-(2-hydroxycyclohexyl)-4-methylbenzenesulfonamide
Conditions | Yield |
---|---|
With 4 A molecular sieve; pyridinium p-toluenesulfonate In toluene for 48h; Heating; | 100% |
benzaldehyde dimethyl acetal
trans-2-(tert-butylamino)cyclohexan-1-ol
Conditions | Yield |
---|---|
With 4 Angstroem molecular sives; pyridinium p-toluenesulfonate In toluene for 100h; Heating; | 100% |
benzaldehyde dimethyl acetal
phenyl-β-D-glucopyranoside
phenyl 4,6-O-benzylidene-β-D-glucopyranoside
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In N,N-dimethyl-formamide at 50℃; for 12h; | 100% |
With sodium hydrogen sulfate; silica gel In acetonitrile at 20℃; for 4h; | 95% |
With toluene-4-sulfonic acid In N,N-dimethyl-formamide at 0℃; for 48h; | 95% |
benzaldehyde dimethyl acetal
acetophenone
allyl-trimethyl-silane
A
4-methoxy-4-phenyl-1-butene
Conditions | Yield |
---|---|
With trimethylsilyl trifluoromethanesulfonate In dichloromethane at -78℃; for 9h; parallel recognition; | A 100% B 95% |
benzaldehyde dimethyl acetal
ethyl (2R,3R,4S)-4-(t-butyldimethylsilyloxy)-2,3-dihydroxy-4-phenylbutanoate
ethyl (2R,3R,4S)-2,3-benzylidenedioxy-4-(t-butyldimethylsilyloxy)-4-phenylbutanoate
Conditions | Yield |
---|---|
With camphor-10-sulfonic acid In benzene for 1h; Heating; | 100% |
With camphor-10-sulfonic acid In benzene for 1h; Cyclization; Heating; | 95% |
benzaldehyde dimethyl acetal
6-O-(3-deoxy-3-tosylamido-α-D-glucopyranosyl)-2,5-dideoxy-5-epi-5-fluoro-1,3-di-N-tosylstreptamine
6-O-(4,6-O-benzylidene-3-deoxy-3-tosylamido-α-D-glucopyranosyl)-2,5-dideoxy-5-epi-5-fluoro-1,3-di-N-tosylstreptamine
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In N,N-dimethyl-formamide at 60℃; under 35 Torr; for 1h; | 100% |
benzaldehyde dimethyl acetal
ethyl (2S,3R)-3-hydroxy-2-methyl-2-(methylthio)-3-phenylpropanoate
Conditions | Yield |
---|---|
Stage #1: ethyl (2S,3R)-3-hydroxy-2-methyl-2-(methylthio)-3-phenylpropanoate With lithium borohydride In dichloromethane at 20℃; Stage #2: benzaldehyde dimethyl acetal With camphor-10-sulfonic acid In dichloromethane at 20℃; | 100% |
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