Our advangtage Production Method:It is obtained by the reaction of benzoic acid prepared by toluene oxidation with sodium bicarbonate, sodium carbonate or sodium hydroxide. Capacity: We have our own factory in China with 50,000mt. yearly capacity.
Cas:65-85-0
Min.Order:1 Metric Ton
FOB Price: $1430.0
Type:Trading Company
inquiryCharacter: It is white,silkete squama or acercse crystal. It has aslightle smell of benzoin of benzaldehyde. It sublimates at about 100°C,relative density is 1.316,boiliy point is 249.2°C, melting point is 121.7°C-123°C. It is diffi
Chinese Name: benzoic acid (also called benzoic acid), benzene carboxylic acid;benzoic acid English Name: Benzoic Acid Molecular formula: C7H6O2 Molecular weight: 122.12 CAS NO.:65-85-0 Use: Industrial grade: mainly used for dye interme
Item Standard Result Appearance White flake Conform Melting point 121.0~123.0℃
Cas:65-85-0
Min.Order:1 Metric Ton
FOB Price: $1700.0 / 2500.0
Type:Manufacturers
inquiry1.Product information Chemical Name: benzoic acid 99.5% CAS No. : 65-85-0 EINECS No. : 200-618-2 Molecular formula: C7H6O2 Molecular weight: 122.1214 Appearance and properties: scaly or needle crystal, with benzene and formaldehyde sme
hebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm
Cas:65-85-0
Min.Order:1 Metric Ton
FOB Price: $1.0 / 3.0
Type:Manufacturers
inquiry1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; ...... Appearance:White Crystalline Powder Storage:Store at RT. Package:1kg/foi
Cas:65-85-0
Min.Order:10 Kilogram
FOB Price: $100.0
Type:Trading Company
inquiryFood Grade Preservative Benzoin Extract Benzoic Acid Powder Xi'an Quanao Biotech Co., Ltd. is is a global chemical industry manufacturers and suppliers of pharmaceuticals and intermediates, peptide,Nootropis etc API, food and feed additives
Cas:65-85-0
Min.Order:100 Kilogram
FOB Price: $7.0 / 8.0
Type:Manufacturers
inquiryProduct description: Product name Benzoic acid CAS number 65-85-0 Assay ≥99% Appearance White crystal Capacity 5000mt/year Application Pharmaceutical, dyestuff, plasticizer,
Benzoic Acid CAS:65-85-0 Pharm Grade, Food Grade, Feed Grade, Industrial Grade Benzenecarboxylic acid; Benzeneformic acid; Benzenemethonic acid; Carboxybenzene; Oracylic acid; phenyl carboxylic acid; Phenylformic acid HANGZHOU THINK CHEMICAL
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Purity: 99% Excellent quality with competitive price Fast delivery Appearance:white crystals or powder Storage:Store in cool dry place Package:25 kg/drum Application:As the preservative, mainly use in fruit juice, drug, toothpaste, soft drink e
Cas:65-85-0
Min.Order:1 Metric Ton
Negotiable
Type:Manufacturers
inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:65-85-0
Min.Order:1 Gram
FOB Price: $0.1
Type:Manufacturers
inquiryADVANTAGE: 1. More than 3,000 Chinese medicine reference substances / standard products available from stock, issued on the same day, multiple cities can be delivered the next day 2. The products are provided with COA, HPLC, NMR, quality assurance,
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Benzoic acid Basic information description Chemical Properties history food preservatives Uses Hazard Preparation Product Name: Benzoic acid Synonyms: Benzyl acid;price benzoic acid;uniseptbza;FEMA 2131;CARBOXYBENZENE;DRACYLIC ACID;BENZENE CARBO
Cas:65-85-0
Min.Order:1 Metric Ton
FOB Price: $1200.0 / 1400.0
Type:Lab/Research institutions
inquiryOur advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:65-85-0
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiryName: Benzoic acid CAS No.: 65-85-0 Molecular Formula:C7H6O2 Appearance:Colorless clear liquid Storage: RT. Package:25kg/drum Application: food preservative. Transportation:By sea Port:Qingdao Port
Appearance:White flake Storage:R.T Package:25kg/Bag Application:Chemical reagents and preservatives Transportation:Express/Sea/Air Port:Any port in China
Cas:65-85-0
Min.Order:500 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryOur Adwantage: 1.We have stock so we can delivery quickly at the very day when receive the payment. 2.Best price, first class service, high successful delivery rate. A discount would be given when you make a large order. 3.High quality gua
Cas:65-85-0
Min.Order:10 Gram
Negotiable
Type:Other
inquiry1,In No Less five years exporting experience. 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Onchem specialized in APIs, chemical intermediate
Cas:65-85-0
Min.Order:25 Kilogram
FOB Price: $1.0
Type:Lab/Research institutions
inquiryWe are the manufacturers and suppliers of API in China, and warehouse in Germany and USA of California, which can quickly and safely deliver to your address 1.High quality and competitive price. 2.Free sample for your evaluation. 3.Promptly delivery
Cas:65-85-0
Min.Order:10 Gram
FOB Price: $1.32
Type:Trading Company
inquiryBenzoic acid Basic information Product Name: Benzoic acid Synonyms: 210;a 1 (acid);Acide benzoique;Benzoic aBenzoic acidcid;Mefenamic Acid Impurity D;Benzyl acid;SS Benzoic Acid;Glycopyrronium Bromide EP Impurity D CAS: 65-85-0 MF: C7H6O
Packing: According to customer requirements Delivery time: In stock or depands Port of shipment: Ningbo/Shanghai/Qingdao OEM/ODM:Welcome Sample:We can offer our existing samples at once Appearance:white crystalline powder Storage:keep in cool a
Cas:65-85-0
Min.Order:25 Kilogram
Negotiable
Type:Trading Company
inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
Cas:65-85-0
Min.Order:1 Kilogram
FOB Price: $186.0 / 210.0
Type:Trading Company
inquiryBenzoic acid CAS: 65-85-0 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediates
Cas:65-85-0
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Product Detail Minimum Order Qty. 10 Gram
Cas:65-85-0
Min.Order:10 Gram
Negotiable
Type:Trading Company
inquiryCompany information: Hebei Mojin Biotechnology Co., Ltd, Our company is a professional in carbomer,carbopol,lead acetate,meglumine diphenyl ethylamine and other chemical raw materials and chemical reagents research and development production ente
Cas:65-85-0
Min.Order:1 Kilogram
FOB Price: $10.0 / 30.0
Type:Trading Company
inquiryConditions | Yield |
---|---|
With 2,2,2-trichloroethylperoxycarbonic acid; dihydrogen peroxide In dichloromethane Ambient temperature; | 100% |
With potassium hydroxide; oxygen In 1,2-dimethoxyethane at 20℃; for 3.5h; | 100% |
With [Cu2C6H4(CHNCH2CH2N(CH2C5H4N)2)2](2+)*2ClO4(1-)=C36H38Cu2N8(ClO4)2; oxygen In acetone at -90.16℃; | 100% |
Conditions | Yield |
---|---|
With water at 45℃; pH=7.2; Microbiological reaction; aq. buffer; | 100% |
With potassium tert-butylate; water In isopropyl alcohol at 25℃; Inert atmosphere; | 100% |
With benzene-1,2-dicarboxylic acid at 250℃; under 7600 Torr; for 0.25h; microwave irradiation; | 99% |
Conditions | Yield |
---|---|
With barium permanganate In acetonitrile for 4h; Heating; | 100% |
With iodosylbenzene In water at 20℃; for 30h; Oxidation; | 100% |
With iodosylbenzene In water for 30h; sonication; | 100% |
Conditions | Yield |
---|---|
With sodium hydroxide at 166 - 168℃; under 5250.4 Torr; for 0.0166667h; Irradiation; | 100% |
With potassium carbonate; thiophenol In 1-methyl-pyrrolidin-2-one at 190℃; for 0.166667h; Substitution; | 100% |
With potassium hydroxide; Aliquat 336 at 200℃; for 0.0833333h; Product distribution; Further Variations:; Reagents; Solvents; Temperatures; microwave irradiation; | 98% |
Conditions | Yield |
---|---|
With barium permanganate In acetonitrile for 0.5h; Heating; | 100% |
With oxygen; sodium methylate; silver trifluoromethanesulfonate In tetrahydrofuran; methanol at 37℃; under 760.051 Torr; Sealed tube; | 98% |
With sodium periodate; manganese(II) 5,10,15,20-tetrakis(N-ethylpyridinium-4-yl)porphyrin In water at 60℃; for 4h; | 96% |
phenacyl benzoate
benzoic acid
Conditions | Yield |
---|---|
With potassium phosphate; tris(2,2-bipyridine)ruthenium(II) hexafluorophosphate; ascorbic acid In water; acetonitrile at 20℃; for 2h; Irradiation; | 100% |
With sodium hydrogen telluride In N,N-dimethyl-formamide for 0.333333h; Product distribution; Ambient temperature; | 1.11 g |
With tetrabutyl ammonium fluoride; phenylmethanethiol In tetrahydrofuran Product distribution; various concentrations, other solvent, other thiols; other educts; selective removal of phenacyl ester group in the presence of benzyl and 4-nitrobenzyl ester groups; |
Conditions | Yield |
---|---|
With aluminum oxide; potassium hydroxide In diethyl ether for 21h; Product distribution; Ambient temperature; other solvent; | A 100% B 80% |
Conditions | Yield |
---|---|
With 2,2'-azobis(isobutyronitrile) In benzene at 65 - 70℃; for 3h; | 100% |
With Fe3O4@SiO2-[(4-(5-O3Si-pentylcarbamoyl)-2-pyridinecarboxylato)CpRu(η3-C3H5)]PF6 In methanol at 30℃; for 1h; Inert atmosphere; chemoselective reaction; | 99% |
[(cyclopentadienyl)bis(acetonitrile)(triphenylphosphine)ruthenium(II)] hexafluorophosphate In methanol at 25℃; for 6h; Product distribution; Further Variations:; Solvents; Temperatures; | 98% |
Conditions | Yield |
---|---|
With hydrogen In methanol at 25℃; for 24h; Reagent/catalyst; Solvent; Temperature; chemoselective reaction; | 100% |
With hydrogen; palladium diacetate; pyrographite In tetrahydrofuran; methanol at 25℃; under 760.051 Torr; for 12h; | 99% |
With hydrogen; palladium diacetate; pyrographite In isopropyl alcohol at 25℃; under 760.051 Torr; for 14h; | 99% |
Conditions | Yield |
---|---|
With NH-pyrazole; air; sodium hydride In tetrahydrofuran for 5h; Ambient temperature; | 100% |
With iodopentafluorobenzene bis(trifluoroacetate) In water; benzene Mechanism; | 94% |
With methyl 3,5-bis((1H-1,2,4-triazol-1-yl)methyl)benzoate; oxygen; sodium acetate; nickel dibromide at 120℃; under 760.051 Torr; for 48h; | 94% |
Conditions | Yield |
---|---|
at -78℃; for 3h; | A 97% B 100% |
at -78℃; for 3h; Mechanism; further α-chloroacyltrimethylsilanes, further aldehydes; | A 97% B 100% |
MANDELIC ACID
benzoic acid
Conditions | Yield |
---|---|
With sodium perborate In acetic acid for 1.5h; steam bath; | 100% |
With (NMe4)*2H2O*CH3CN (L = ortho-phenylenebis(N'-methyloxamidate)); oxygen; pivalaldehyde In acetonitrile for 6h; Ambient temperature; | 98% |
With Oxone; 3,3'-diiodo-2,2',6,6'-tetramethoxy-4,4'-biphenyldicarboxylic acid In nitromethane; water at 30 - 35℃; for 14h; | 98% |
Conditions | Yield |
---|---|
Stage #1: para-chlorobenzoic acid With palladium/alumina; hydrogen; potassium carbonate In water at 60℃; Stage #2: With hydrogenchloride In water | 100% |
With hydrogen; triethylamine; palladium on activated charcoal In methanol at 20℃; for 6h; | 99% |
With ammonium formate In water; isopropyl alcohol at 20℃; for 3h; | 99% |
Conditions | Yield |
---|---|
With hydrogen; triethylamine; palladium on activated charcoal In methanol at 20℃; for 3h; | 100% |
With borane-ammonia complex In water; isopropyl alcohol at 40℃; for 3h; Sealed tube; | 97% |
With 1H-imidazole; copper ammonium sulphate hexahydrate; lithium tert-butoxide In N,N-dimethyl-formamide; isopropyl alcohol for 72h; Irradiation; | 87% |
1-benzoylimidazole
benzoic acid
Conditions | Yield |
---|---|
With morpholine; water at 20℃; for 0.333333h; | 100% |
With 1H-imidazole; potassium chloride In water; acetonitrile at 25 - 50℃; Kinetics; Thermodynamic data; ΔH(excit.), ΔS(excit.), ΔG(excit.); |
Conditions | Yield |
---|---|
With methoxybenzene In toluene for 6h; Heating; | 100% |
With Montmorillonite K-10 clay; toluene for 0.333333h; Dealkylation; Microwave irradiation; | 98% |
With sodium hydrogen sulfate; silica gel In dichloromethane at 20℃; for 5h; | 95% |
A
1,2-bis(3-formyl-4-phenyl)ethane
B
benzoic acid
Conditions | Yield |
---|---|
With iron(II) sulfate In tetrahydrofuran; water at 20℃; for 16h; | A 100% B 95% |
Perbenzoic acid
bis-benzenesulfenyl-amine
A
benzoic acid phenyl ester
B
biphenyl
C
benzoic acid
D
diphenyldisulfane
Conditions | Yield |
---|---|
In benzene Kinetics; Product distribution; Mechanism; isotopic effect, effect of benzoic acid and styrene on the reaction; | A 1.4% B 0.2% C 100% D 50% E n/a |
benzoic acid methoxymethyl ester
benzoic acid
Conditions | Yield |
---|---|
sodium hydrogen sulfate; silica gel In dichloromethane at 20℃; for 1.5h; | 100% |
With bismuth(III) chloride; water In acetonitrile at 50℃; for 2h; | 89% |
benzoic acid
Conditions | Yield |
---|---|
Stage #1: (1-nosyl-5-nitroindol-3-yl)methyl benzoate With 2-(N,N-dimethylamino)ethylthiol hydrochloride; 1,8-diazabicyclo[5.4.0]undec-7-ene In acetonitrile at 20℃; for 0.25h; Inert atmosphere; Stage #2: With hydrogenchloride In diethyl ether; water; acetonitrile Inert atmosphere; | 100% |
A
[(6-Ph2TPA)Ni(O2CPh)]ClO4
B
phenacyl benzoate
C
carbon monoxide
D
benzil
E
benzoic acid
Conditions | Yield |
---|---|
With oxygen | A 100% B n/a C n/a D n/a E n/a |
A
phenacyl benzoate
B
carbon monoxide
D
benzil
E
benzoic acid
Conditions | Yield |
---|---|
With oxygen In acetonitrile at 20℃; | A n/a B n/a C 100% D 12% E 11 mg |
benzoic acid
Conditions | Yield |
---|---|
With hydrogenchloride In water | 100% |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; vanadia In water at 100℃; for 24h; | 100% |
With 2,2'-azinobis(3-ethylbenzthiazolinesulfonate); Trametes versicolor laccase In acetonitrile at 20℃; pH=5; Green chemistry; Enzymatic reaction; | 20% |
Conditions | Yield |
---|---|
With potassium phosphate; tris(2,2-bipyridine)ruthenium(II) hexafluorophosphate; ascorbic acid In water; acetonitrile at 20℃; for 1h; Reagent/catalyst; Irradiation; | 100% |
With 2-H-1,3-di-tert-butyl-1,3,2-diazaphosphorinane; 2,2'-azobis(isobutyronitrile); 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane In toluene at 90℃; for 12h; chemoselective reaction; | 99% |
Conditions | Yield |
---|---|
With poly((divinylbenzene)-0.5 mol-styrenesulfonic acid) In water; toluene at 80℃; for 24h; Schlenk technique; Inert atmosphere; | 100% |
With 10% Pt/activated carbon; oxygen; sodium hydroxide In water at 80℃; for 24h; Green chemistry; chemoselective reaction; | 82% |
cyclohexanone
benzaldehyde
A
hexahydro-2H-oxepin-2-one
B
benzoic acid
Conditions | Yield |
---|---|
With oxygen In 1,2-dichloro-ethane at 50℃; for 5h; Catalytic behavior; Reagent/catalyst; Temperature; Time; | A 100% B 100% |
Conditions | Yield |
---|---|
With dmap; triethylamine In dichloromethane at 20℃; for 4h; | 100% |
With dmap; 2-chloro-1-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)pyridinium trifluoromethanesulfonate; triethylamine In dichloromethane at 20℃; for 4h; | 100% |
With TEA; 1,2-benzisoxazol-3-yl diphenyl phosphate In various solvent(s) for 2h; Ambient temperature; | 99% |
Conditions | Yield |
---|---|
With hydrogenchloride In water for 2h; Heating; | 100% |
With sulfuric acid Fischer-Speier esterification method; Reflux; | 100% |
With tetrachloromethane at 20℃; for 72h; UV-irradiation; | 99% |
Conditions | Yield |
---|---|
With indium(III) bromide In dichloromethane-d2 at 20℃; | 100% |
With palladium diacetate In benzene-d6 for 4h; dehydrocoupling reaction; Heating; | 95% |
With zinc(II) chloride In N,N-dimethyl-formamide at 120℃; for 25h; | 85% |
Conditions | Yield |
---|---|
With bis(5-norbornenyl-2-methyl) azodicarboxylate; polystyrene-supported PPh3 In tetrahydrofuran Esterification; Mitsunobu reaction; | 100% |
With toluene-4-sulfonic acid for 0.05h; Irradiation; | 97% |
With 1-(tert-butyl)-2-(chlorobenzyl) azodicarboxylate; triphenylphosphine In dichloromethane at 0 - 20℃; for 4h; Reagent/catalyst; Mitsunobu Displacement; | 97.9% |
Conditions | Yield |
---|---|
zirconium(IV) oxide at 200℃; var.: 77 deg C, 5 h in liquid-phase; | 100% |
With tetrachloromethane at 20℃; for 72h; UV-irradiation; | 99% |
With alumina methanesulfonic acid at 80℃; for 0.133333h; Microwave irradiation; | 98% |
Conditions | Yield |
---|---|
With TiO(acac)2 In xylene for 36h; Heating; | 100% |
Stage #1: benzoic acid With trifluoroacetic anhydride; indium(III) chloride at 20℃; Stage #2: β-naphthol at 20℃; for 0.166667h; | 98% |
With N,N-bis[2-oxo-3-oxazolidinyl]phosphorodiamidic chloride; triethylamine In dichloromethane for 1h; Ambient temperature; | 91% |
Conditions | Yield |
---|---|
With cyanomethylenetributyl-phosphorane In benzene at 100℃; for 24h; | 100% |
With TiO(acac)2 In xylene for 15h; Heating; | 100% |
With fluorosulfonyl fluoride; N-ethyl-N,N-diisopropylamine In 1,2-dichloro-ethane at 20℃; for 5h; | 99% |
Conditions | Yield |
---|---|
With 1,2,3-Benzotriazole; thionyl chloride In dichloromethane at 20℃; Substitution; | 100% |
With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane at 20℃; for 2h; Reflux; | 100% |
With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane at 35℃; for 1h; | 100% |
Conditions | Yield |
---|---|
With potassium Sodium; polyethylene oxide In tetrahydrofuran at 0℃; 12 ethylene oxide units/M(+); | 100% |
With hydrogen In water at 100℃; under 15001.5 Torr; for 2h; | 100% |
With C33H49ClNRh; hydrogen In 2,2,2-trifluoroethanol at 20℃; under 51005.1 Torr; for 24h; Autoclave; Molecular sieve; | 99% |
Conditions | Yield |
---|---|
With PPE for 15h; Ambient temperature; | 100% |
With TEA; diphenyl (2,3-dihydro-2-thioxo-3-benzoxazolyl)phosphonate In various solvent(s) for 2h; Ambient temperature; | 99% |
With dmap; picryl fluoride In acetonitrile for 3h; Ambient temperature; | 98% |
Conditions | Yield |
---|---|
With 1,1'-carbonyldiimidazole In tetrahydrofuran at 60℃; Inert atmosphere; | 100% |
With benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine In dichloromethane at 0 - 20℃; | 83% |
Stage #1: benzoic acid With chloroformic acid ethyl ester; triethylamine In dichloromethane at 0℃; for 0.5h; Inert atmosphere; Stage #2: 1-amino-2-propene In dichloromethane Inert atmosphere; | 78% |
Conditions | Yield |
---|---|
With TiO(acac)2 In xylene for 15h; Heating; | 100% |
With iron(III)-acetylacetonate In 5,5-dimethyl-1,3-cyclohexadiene for 15h; Inert atmosphere; Reflux; | 97% |
With 4-nitro-diphenylammonium triflate In toluene at 80℃; for 30h; | 95% |
1-hydroxy-pyrrolidine-2,5-dione
benzoic acid
benzoic acid N-hydroxysuccinimide ester
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; for 16h; Inert atmosphere; | 100% |
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide at 20℃; for 0.166667h; | 97% |
With 3-(5-nitro-2-oxo-1,2-dihydro-1-pyridyl)-1,2-benzisothiazole 1,1,-dioxide; triethylamine In dichloromethane -10 deg C -> r.t., overnight; | 93% |
Conditions | Yield |
---|---|
With caesium carbonate In acetonitrile for 0.5h; Heating; | 100% |
With cesium fluoride In acetonitrile for 1.5h; Heating; | 99% |
With potassium fluoride; tetra(n-butyl)ammonium hydrogensulfate In tetrahydrofuran at 20℃; for 3h; | 99% |
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile room temperature, 20 min -> reflux, 50 min; | 100% |
With N-ethyl-N,N-diisopropylamine In acetone | 100% |
With potassium carbonate; 1,4-dimethyl-1,2,4-triazolium iodide In acetonitrile at 40℃; for 3h; Schlenk technique; | 99% |
Conditions | Yield |
---|---|
With tributylphosphine; diamide In benzene at 60℃; for 24h; Product distribution; comparison with Mitsunobu reagent; further secondary alcohols and acids; | 100% |
With tributylphosphine; diamide In benzene at 60℃; for 24h; | 100% |
With tributylphosphine; 1,1'-azodicarbonyl-dipiperidine In benzene at 60℃; for 24h; | 81% |
With 4-nitro-phenol; triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran for 14h; Ambient temperature; | 69% |
With triphenylphosphine; diethylazodicarboxylate |
benzoic acid
α,α-dimethylallyl benzoate
Conditions | Yield |
---|---|
With potassium carbonate; tetrakis(acetonitrile)copper(I)tetrafluoroborate In dichloromethane at 20℃; for 17h; | 100% |
With potassium carbonate; copper(I) bromide In dichloromethane at 20℃; | 92% |
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